SURAT KETERANGAN HASIL SURVEILAN
DALAM RANGKA PENERBITAN HC
Petugas Penerima Contoh
(...) PETUNJUK TEKNIS PENGAMBILAN CONTOH
DALAM RANGKA PENERBITAN HC
Edisi / Revisi : 1/0 Halaman : 1 dari 1
Berita Acara Serah Terima Contoh No. Dokumen : Form 2
57
JUMLAH CONTOH BERDASARKAN SATUAN KEMASAN TERKECIL PRODUK PERIKANAN BESARNYA LOT (SATUAN KEMASAN
TERKECIL) JUMLAH CONTOH UJI
≤ 2400 6
2401 - 15000 8
15001 - 24000 10
24001 - 42000 15
≥ 42001 24
JUMLAH CONTOH IKAN HIDUP BERDASARKAN SATUAN TERKECIL EKOR
JUMLAH IKAN (EKOR) JUMLAH CONTOH UJI
≤ 8000 3
8001 - 14000 5
14001 - 24000 8
24001 - 40000 14
≥ 40000 21
PETUNJUK TEKNIS PENGAMBILAN CONTOH DALAM RANGKA PENERBITAN HC
Edisi / Revisi : 1/0 Halaman : 1 dari 1
Jumlah Sampel Uji Organoleptik dalam rangka End Product Testing
No. Dokumen : Form 3 Validasi Tanggal : 23 Mei 2016
58
1. UNI EROPA
Berdasarkan Commission Regulation (EC) No. 1881/2006 tanggal 19 Desember 2006 tentang Setting Maximum Level for Certain Contaminants in Foodstuffs
No. Parameter Satuan Batas maksimal
A Logam Berat 1) Merkuri (Hg)
a.
b.
Anglerfish (Lophius species) Atlantic catfish (Anarhichas lupus) Bonito (Sarda sarda),
Eel (Anguilla species),
Emperor, orange, roughly, rosy soldierfish (Hoplostethus species)
Grenadier (Coryphaenoides rupestris) Halibut (Hippoglossus hippoglossus) Kingklip (Genypterus capensis) Marlin (Makaira species ), Megrim (Lepidorhombus species) Mullet (Mullus species)
Pink cusk eel (Genypterus blacodes) Pike (Esox lucius)
Plain bonito ( Orcynopsis unicolor) Poor cod (Tricopterus minutes)
Portuguese dogfish (Centroscymnus coelolepis) Rays (Raja species)
Redfish (Seabastes marinus, S. mentella, S. viviparus),
Sail fish (Istiophorus platypterus)
scabbard fish ( Lepidopus caudatus, Aphanopus carbo)
Seabream, pandora (Pagellus species) Shark (semua spesies),
Snacke Mackerel atau butterfish (Lepidocybium flavobrunneum, Ruvettus pretiosus, Gempylus serpens),
Sturgeon ( Acipenser species) Swordfisfh (Xiphias gladius),
Tuna (Thunnus species, Euthynnus species, Katsuwonus pelamis)
Produk perikanan selain (a), crustacea tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster, dan crustacea besar (Nephropidae dan Palinuridae)
mg/kg
mg/kg
1,00
0,50 PETUNJUK TEKNIS PENGAMBILAN CONTOH
DALAM RANGKA PENERBITAN HC
Edisi / Revisi : 1/0 Halaman : 1 dari 20
Standar Pengujian Negara Mitra No. Dokumen : Form 4
59
2) Cadmium (Cd)
a. Eel (Anguilla anguilla), bonito (Sarda sarda), grey mullet (Mugil labrosus labrosus), horse mackerel atau scad (Trachurus species), louvar or louvar (Luvarus imperialis), mackerel (Scomber species), sardin ( Sardine pilchardus), sardinop (Sardinops species) common two-banded seabream (Diplodus vulgaris), tuna (Thunus species, Euthynnus species dan Katsuwonus pelamis), wedge sole (Dicologoglossa cuneata)
mg/kg 0,10
b. Produk perikanan selain (a) mg/kg 0,05
Bullet tuna (Auxis species) mg/kg 0,20
c. Anchovy (Engraulis species) Swordfish/Meka (Xiphias gladius)
mg/kg 0,30
d. Crustacea tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster, dan crustacea besar (Nephropidae dan Palinuridae).
mg/kg 0,50
e. Bivalve Molluscs mg/kg 1,0
f. Cephalopoda (tanpa jeroan) mg/kg 1,0
3) Timbal (Pb)
a. Daging ikan mg/kg 0,30
b. Crustacea tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster dan crustacea besat (Nephropidae dan Palinuridae)
mg/kg 0,50
c. Bivalve Molluscs mg/kg 1,5
d. Cephalopoda (tanpa jeroan) mg/kg 1,0
4) Arsenik (As)
a. Udang beku, udang kupas mentah beku, ikan beku, ikan segar, tuna segar, tuna loin beku, ikan
kemasan dalam kaleng, surimi, ikan asap
mg/kg 0,1
b. Tuna slice beku, tuna ground meat beku, belut beku dan agar-gar kertas
mg/kg 0.25
c. Semi refind carragenan mg/kg 3,0
B Pestisida
1) Organochlorin termasuk PCBs, Organophosphat*
a. Semua produk perikanan kecuali eel. Crustacea tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster dan crustacea besat (Nephropidae dan Palinuridae)
pg/g berat basah
8,0
b. Eel (Anguilla Anguilla )dan produk yang berasal dari eel
pg/g berat basah
12,0
c. Minyak ikan (minyak dari daging, hati, dan bagian lain dari produk perikanan untuk konsumsi manusia)
pg/g lemak 10,0
2) Dioksin*
a. Semua produk perikanan kecuali eel . pg/g berat basah
4,0
b. Eel (Anguilla Anguilla )dan produk yang berasal dari eel
pg/g berat basah
60 c. Minyak ikan (minyak dari daging, hati, dan bagian
lain dari produk perikanan untuk konsumsi manusia)
pg/g lemak 2,0
3) Polycyclic aromatic hydrocarbons (PAH)
- Benzopyrene)*
a Daging ikan dari ikan asap dan produk perikanan yang diasap kecuali bivalve molluscs. Crustaceans asap tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster dan crustacea besat (Nephropidae dan Palinuridae)
µg/kg berat basah
5,0
b Daging ikan selain yang diasap µg/kg berat basah
2,0
c Crustaceans, cephalopods selain asap. Crustaceans tidak termasuk daging coklat dari crab dan daging kepala serta thorax dari lobster dan crustacea besat (Nephropidae dan Palinuridae)
µg/kg berat basah
5,0
d. Bivalve Molluscs µg/kg berat
basah
10,0
C Tin: Timah ( inorganik)
produk ikan kaleng
mg/kg 200
Berdasarkan Commission Regulation (EC) No. 2073/2005 tanggal 15 November 2005 tentang On Microbial Criteria for Foodstuffs
61
2. KANADA
Bacteriological Guidelines for Fish and Fish Products (end product)
Table of bacteriological levels with organism, product and acceptance numbers
Test Organism1 Product Type Number of sample units Acceptance number (c)2 m/g2 M/g2 Criteria for action
Escherichia coli Cooked or
ready-to-eat products 5 1 4 40 Reject if 2 or more units exceed m, or if any unit exceeds M Raw bivalve molluscs 5 1 230/100g 330/100g Reject if 2 or more units exceed m, or if any unit exceeds M All other types 5 2 4 40 Reject if 3 or more units exceed m, or if
62 any unit exceeds M Coagulase-PositiveStaphyloco cci
All types 5 1 1000 10000 Reject if 2 or more units exceed m, or if any unit exceeds M
Salmonella spp. All types 5 Absent in
each 25 g sample or in pooled samples of 125g. - - Reject if Salmonellas pp is detected
Vibrio cholerae Cooked or
ready-to-eat products 5 Absent in each 25 g sample or in pooled samples of 125g - - Reject if Vibrio cholerae is detected. Vibrio parahaemolyticus7
Raw Oyster 5 1 100 10000 Reject if 2 or more units exceed m, or if any unit exceeds M
Listeria monocytogenes
Policy on Listeria monocytogenes in Ready-to-Eat Foods
Product Type / Category 3 Laboratory method
to be applied
Action Level
RTE Fish products in which the growth of L. monocytogenes can occur and could exceed 100 CFU/g before the end of the stated shelf-life.
Includes all products that do not fall in either below-mentioned product types.
(Equivalent to Category 1 foods in the HC Listeria policy)*
Presence/absence in 125g (MFHPB-30 6) on 5 sample units of 25 g each Detected
RTE Fish products in which the growth of L. monocytogenes can occur but is limited to levels no greater than 100 CFU/g over the course of their stated shelf-life.
RTE products that have a refrigerated shelf-life of 5 days or less fall under this category.
Other products require validation data 4 demonstrating growth cannot exceed 100 CFU/g 5.
(Equivalent to Category 2A foods in the HC Listeria policy*)
Enumeration in 50 g
(MFLP-74 6) on 5 sample units of 10 g each
> 100CFU/g 5
RTE Fish products in which growth of L. monocytogenes can not occur over the course of the stated shelf-life.
Products with the following characteristics fall under this category: Enumeration in 50 g(MFLP-74 6) on 5 sample units of 10 g each > 100CFU/g 5
63 products that are frozen, or
have a pH < 4.4 regardless of the aw, or have an aw < 0.92 regardless of the pH, or have a pH < 5.0 and an aw < 0.94
For products that don't meet the above characteristics, validation data 4 demonstrating the absence of growth is required.
(Equivalent to Category 2B foods in the HC Listeria policy*)
Notes:
1 The analysis of all fish or fishery products shall be conducted in accordance with approved methods 2 m - number of bacteria per gram separating acceptable from marginally acceptable samples, c - number of samples that may exceed this number of bacteria per gram, M - no sample can exceed this number of bacteria per gram
3 For further guidance on the determination of a product category, see Figure 1 Classification Of Ready-to Eat Foods in the Health Canada document Validation of Ready-to-Eat Foods for Changing the Classification of a Category 1 into a Category 2A or 2B Food - in relation to Health
Canada's Policy on Listeria monocytogenes in Ready-to-Eat Foods (2011)
4 See HC's guide on "Listeria monocytogenes Challenge Testing of Ready-to-Eat Refrigerated Foods" for information on challenge testing as part of validation.
5 Counts between 5 and 100 CFU/g can be an indication of a possible loss of control and should prompt the processor to verify and/or re-evaluate his process controls.
6 Or any other method published in the Health Canada's Compendium of Analytical
Methods for Listeria monocytogenes in which the "application" section is appropriate for the intended purpose (e.g., MFHPB-methods and MFLP-methods).
7An interim adjustment to the bacteriological guideline (end-product) for Vp apply to British Columbia oysters intended for raw consumption. The updated guideline is found in the Notice to Industry - Enhancement to the management of the risks ofVibrio parahaemolyticus in Raw Oysters. * Health Canada's "Policy on Listeria monocytogenes in Ready-to-Eat Foods" will be referred to as the "HC ListeriaPolicy" validation.
64
Cemaran
Note:
Sampling: Samples to consist of a minimum of 5 units representative of the lot. Analysis may be
carried out on a composite of all sample units.
Criteria for Action: A lot of fish will be considered reject if the sample value exceeds the
action level. Fish or fish products exceeding these guidelines may be permitted for export if they do not violate regulations of the importing country.
65
Toxin
Keterangan tambahan:
2Histamine
Samples are collected according to Sampling Plan 1 (AQL 6.5) for initial inspection and Sampling Plan 2 (AQL 6.5) for reinspection. See the Sampling Policy and Procedures. Any sample exceeding 50 mg/100 g will result in the lot being rejected with no right to
reinspection. The acceptance number is that corresponding to the number for decomposition.
3PSP, ASP and DSP (Paralytic Shellfish Poisoning, Amnesic Shellfish Poisoning – Diarrhetic Shellfish Poisoning)
Procedures for closure of shellfish areas, and possible recall of product due to samples of shellfish containing toxin levels equal to or greater than the above action levels can be found in Chapter 11 of the Canadian Shellfish Sanitation program.
The minimum acceptable sample is that which when shucked will produce 100 g of drained meats from 5 pooled sub-samples. Depending on the size of animals, the total number of shellfish required varies from 3 (geoduck) to 25 (pink scallops).
66
Additive
Keterangan:
4The compounds listed in this table are food additives; however some background levels may occur naturally in some foods. See Division 16 of the Food and Drug Regulations.
5See Division 21 of the Food and Drug Regulations.
6When the additive is not permitted, then the action level is the background level or detection limit; when the additive is permitted, then the action level is the background level or detection limit plus the permitted amount.
7Marine mammals, including seals are included in the definition of "fish" as per the Canadian Food and Drug Regulations. Sodium nitrite is permitted in marine mammal meats at the maximum level of 200 ppm.
8Calculated as sulphur dioxide.
67
3. CHINA
Maximum Level of Contaminants in Fish and Fishery Product
No Cemaran dan Jenis Produk Maximum Level
Lead Calculated as Pb (mg/kg)
1. Fresh and frozen aquatic animals (excluding fish, crustacean, bivalves)
a. Fish, crustacean b. Bivalves
Aquatic products (excluding jellyfish products) a. Jellyfish products 1.0 (eviscerated) 0.5 1.5 1.0 2.0 Cadmium Calculated as Cd (mg/kg)
2. Fresh and frozen aquatic animals a. Fish
b. Crustaceans
c. Bivalves, gastropods, cephalopods, echinoderms Aquatic products
a. Canned fish (excluding canned anchovies, swordfish)
b. Canned anchovies, swordfish
c. Other fish products (except anchovy and swordfish products)
d. Anchovy and swordfish products
0.1 0.5 2.0 (eviscerated) 0.2 0.3 0.1 0.3 Mercury Calculated as Hg (mg/kg)
Total Mercury Methyl Mercury 3. Aquatic animals and their products (excluding predatory
fish and their products)
a. Predatory fish and their products
- -
0.5 1.0
Arsenic Calculated as As (mg/kg)
Total Arsenic Inorganic Arsenic 4. Aquatic animals and their products (excluding fish and
their products)
a. Fish and their products
- -
0.5 0.1
Chromium Calculated as Cr (mg/kg)
5. Aquatic animals and their products 2.0
Benzo(a)pyrene Maximum level (µg/kg)
6. Aquatic animals and their products
a. Barbecued or grilled aquatic products 5.0
N-nitrosamines Maximum level (µg/kg)
7. Aquatic animals and their products
a. Aquatic products (excluding canned aquatic products)
4.0
Polychlorinated Biphenyls Maximum levela (mg/kg)
8. Aquatic animals and their products 0.5
aPolychlorinated biphenyls are calculated as the sum of PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180
68
4. RUSIA
STANDAR MUTU RUSIA UNTUK PRODUK IKAN, NON IKAN DAN PRODUK OLAHANNYA
Nama Produk Parameter Maks level mg/kg, Keterangan Tuna, swordfish, meka, beluga, mackerel segar/beku, Kimia Timbal (Pb) 2.0 Kadmium (Cd) 0.2 Arsen (As) 5.0 * Merkuri (Hg) 1.0 Histamin 100.0 nitrosamines: jumlah nitrosomethylamine dan nitrosodiethylamine 0.003 *
Dioxins 0.000004 *diuji bila ada kecurigaan yang cukup tentang kemungkinan adanya pada bahan baku Mikrobiologi
Bakteri aerob mesofilik dan fakultatif anaerob, CFU/g
1х105 CGB (coliforms), dalam 0.001g Tidak diperbolehkan Termasuk E,coli
S. aureus, dalam 0.01g Tidak
diperbolehkan Bakteri pathogen termasuk
salmonella dan
L.monocytogenes, dalam 25 g
Tidak
diperbolehkan
Bakteri pathogen lain sesuaikan dengan SNI Tuna
V. parahaemolyticus, CFU/g, 100 sulfite-reducing clostridia
dalam 1.0g
Produk dalam kemasan vacuum
Pesticida**: HCCH (α, β, γ - isomers) 0.2 DDT dan metabolitnya 0.2 Polychlorinated biphenyls 2.0 Radionuklida: Cesium-137, Bq/kg(l) 130 Strontium-90, Bq/kg(l) 100 Parasit Anisakis Tidak diperbolehkan visual
Ikan laut lainnya Kimia
Timbal (Pb) 1.0
Arsen (As) 5.0 Bila memungkinkan Kadmium (Cd) 0.2 Merkuri (Hg) 0.5 nitrosamines: jumlah nitrosomethylamine dan nitrosodiethylamine 0.003
Dioxins 0.000004 diuji bila ada kecurigaan yang cukup tentang kemungkinan adanya pada bahan baku Pesticida**:
HCCH (α, β, γ - isomers) 0.2 DDT dan metabolitnya 0.2 Polychlorinated biphenyls 2.0 Radionuklida:
69 Cesium-137, Bq/kg(l) 130
Strontium-90, Bq/kg(l) 100 Mikrobiologi
Bakteri aerob mesofilik dan fakultatif anaerob, CFU/g
1х105 CGB (coliforms), dalam 0.001g Tidak diperbolehkan Termasuk E,coli
S. aureus, dalam 0.01g Tidak
diperbolehkan Bakteri patogen termasuk
salmonella dan
L.monocytogenes, dalam 25 g
Tidak
diperbolehkan
Bakteri pathogen lain sesuaikan dengan SNI produk
V. parahaemolyticus, CFU/g, 100 ikan laut sulfite-reducing clostridia
dalam 1.0g
Produk dalam kemasan vacuum Parasit Scombroidae, octopus, scallops : Anisakis Tidak diperbolehkan visual Ikan hasil budidaya Antibiotik: Grup tetrasiklin <0.01 mg/kg Ikan kaleng (Tuna, beluga, swordfish, mackerel salmon, herring) Kimia Timbal (Pb) 2.0
Arsen (As) 5.0 Bila memungkinkan Kadmium (Cd) 0.2
Merkuri (Hg) 1.0
stannum 200 prefabricated tin tare
chrome 0.5 chromium-plated tare
Histamin 100.0
Nitrosamines: jumlah nitrosomethylamine dan nitrosodiethylamine
0.003
benzapyrene 0.005 Ikan asap
Dioxins*** 0.000004 diuji bila ada kecurigaan yang cukup tentang kemungkinan adanya pada bahan baku Pesticida**: HCCH (α, β, γ - isomers) 0.2 DDT dan metabolitnya 0.2 Polychlorinated biphenyls 2.0 Radionuklida: Cesium-137,Bq/kg(l) 130 Strontium-90, Bq/kg(l) 100 Mikrobiologi:
Bakteri aerob mesofilik dan fakultatif anaerob, CFU/g
5 х 104
CGB (coliforms) dalam 1.0g Tidak
diperbolehkan
Termasuk E,coli
S. aureus, dalam 1.0g Tidak
diperbolehkan sulfite-reducing clostridia
dalam 1.0g
Tidak
diperbolehkan Bakteri patogen termasuk
salmonella dan
L.monocytogenes, dalam 25 g
Tidak
diperbolehkan
Bakteri pathogen lain sesuaikan dengan SNI produk
Ikan kaleng (gelas, aluminium dan tin)
Harus memenuhi persyaratan sterilisasi komersil untuk produk kaleng Group A sesuai Annex 1 Bagian 1 Bab II Persyaratan sanitary dan epidemiologi serta hygiene untuk produk yang dikenakan pengawasan Sanitary dan epidemiologi
70 pasteurisasi
dalam wadah gelas
Harus memenuhi persyaratan sterilisasi komersil untuk produk kaleng Group E sesuai Annex 1 Bagian 1 Bab II Persyaratan sanitary dan epidemiologi serta hygiene untuk produk yang dikenakan pengawasan Sanitary dan epidemiologi
Ikan Kering Kimia: (bahan baku dan produk akhir) Timbal (Pb) 1.0
Arsen (As) 5.0 Bila memungkinkan Kadmium (Cd) 0.2 Merkuri (Hg) 0.5 Nitrosamine:jumlah dari nitrosomethylamine dan nitrosodiethylamine 0.003
Dioxins 0.000004 (diuji bila ada kecurigaan yang cukup tentang kemungkinan adanya pada bahan baku) Radionuklida: Cesium-137, Bq/kg(l) 130 Strontium-90, Bq/kg(l) 100 Pesticida**: HCCH (α, β, γ - isomers) 0.2 DDT dan metabolitnya 0.4
2.0 fillet ikan, herring benzapyrene 0.005 ikan asap
Polychlorinated biphenyls 2.0 (bahan baku dan produk akhir) Mikrobiologi:
Bakteri aerob mesofilik dan fakultatif anaerob, CFU/g
5х104
CGB (coliforms) dalam 0.1g Tidak
diperbolehkan sulfite-reducing clostridia
dalam 1.0g
Tidak
diperbolehkan Bakteri pathogen termasuk
salmonella dalam 25g
Tidak
diperbolehkan
Bakteri pathogen lain sesuaikan dengan SNI produk
Kapang, CFU/g, 50 Ragi, CFU/g, 100 non ikan: moluska, krustasea dan invertebrate lain, algae dan grass- wracks) dan produk olahannya:
Indikator Parasit:
Indikator keamanan Parasit untuk ikan, krustasea, moluska, ampibi, reptile dan produk olahannya harus memenuhi persyaratan pada Bagian 1 Bab II Annex 2 Persyaratan sanitary dan epidemiologi serta hygiene untuk produk yang dikenakan pengawasan Sanitary dan epidemiologi
- moluska, krustacea dan invertebrate lain Bahan beracun: Timbal (Pb) Arsen (As) Kadmium (Cd) merkuri (Hg) 10.0 5.0 2.0 0.2
- algae and grass-wracks Bahan beracun Timbal (Pb) 0.5 Arsen (As) 5.0 Kadmium (Cd) 1.0 merkuri (Hg) 0.1 Antibiotik (untuk ikan hasil budidaya): Grup tetrasiklin Tidak
diperbolehkan <0.01 mg/kg - moluska dan krustasea Phycotoxin paralyzant of mollusks (saxitoxin) 0.8 Moluska
71 amnesic poison of mollusks
(domoic acid)
20 Moluska
30 Crab internals diarrheal poison of mollusks
(okadaic acid)
0.16 moluska
non ikan – clams (mussels, oysters, scallop dll.): dingin, beku
CGB (coliforms) dalam 0.1g Tidak
diperbolehkan S. aureus, dalam 0.1g Tidak
diperbolehkan Bakteri patogen,termasuk salmonella dan L.monocytogenes dalam 25g Tidak diperbolehkan
V. parahaemolyticus, CFU/g, 100 – ikan laut Bakteri aerob mesofilik dan
fakultatif anaerob, CFU/g
2х104 Telur ikan terbang (other fish caviar ) Bahan beracun lead 1.0 arsen 1.0 Kadmium 1.0 mercury 0.2 Pesticida**: HCCH (α, β, γ - isomers) 0.2 DDT dan metabolitnya 2.0 Polychlorinated biphenyls 2.0 Mikrobiologi
Bakteri aerob mesofilik dan fakultatif anaerob, CFU/g
1х105 CGB (coliforms) in 0.1g Tidak diperbolehkan sulfite-reducing clostridia dalam 1.0g Tidak diperbolehkan Bakteri patogen,termasuk salmonella dalam 25g Tidak diperbolehkan Kapang, CFU/g, 50 Ragi, CFU/g, 300
72
76
78
KEPALA BADAN KARANTINA IKAN,
PENGENDALIAN MUTU DAN KEAMANAN HASIL PERIKANAN,
ttd.
RINA
Lembar Pengesahan
No. Nama Pejabat Paraf 1 Sekretaris BKIPM
2 Kepala Pusat Sertifikasi Mutu dan KHP
3 Kepala Bagian Hukum, Humas dan Informasi
4 Kepala Subbag Hukum
Salinan sesuai dengan aslinya Kepala Bagian Hukum,
Humas dan Informasi,