6. DAFTAR PUSTAKA - 12.70.0152 Yeremia Adi Wijaya LAMPIRAN

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Lampiran 1. Karakteristik Laju Transmisi Uap Air Beberapa Lapisan Film

No Bahan Polimer WVTR

(g/m2.hari)

Referensi 1 Cellulose Acetate (CA) 2920 Shogren (1997)

2 Polylactic Acid (PLA) 130 - 180 Alemayehu et al (2012) & Shogren (1997)

3 Karagenan + 0,5% Gly 400 - 600 Handoko (2015)

4 Chitosan 1100 - 1200 Saleh (2009)

5 Pati - Chitosan 750 - 1300 Saleh (2009)

6 Protein Zein 179 Alemayehu et al (2012)

7 Isolat Protein Whey 145 Schmid (2013)

8 Isolat Protein Whey-45 110 Coughlan et al (2004) 9 Isolat protein kedelai 89.04 - 96.96 Reis (2002)

10 Kacang hijau + 30% Gly 120 - 130 Wittaya (2013) 11 Gelatin + 30% Srb 909 - 1040 Shakila et al (2012) 12 Gelatin : Chitosan + 30% Srb 843 - 913 Shakila et al (2012) 13 Low Density Polyethylene

(LDPE)

0.92 Ralston (2010)

14 Polipropilen (PP) 0.2 - 0.4 Woishnis (1995) dalam Oymaci (2014)

15 Polietilen Terepthalat (PET) 0.5 - 2 Woishnis (1995) dalam Oymaci (2014)

16 Polietilen (PE) 0.5 - 2 Woishnis (1995) dalam Oymaci (2014)

17 Polistiren (PS) 6.4 Barrie (1968) dalam Aldana et al (2014)

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Lampiran 2. Perbandingan Karakteristik Laju Transmisi Uap Air Beberapa Lapisan Film

0 200 400 600 800 1000 1200

g

/m

2.h

ar

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Lampiran 3. Karakteristik Mekanik Beberapa Lapisan Film

No. Polimer TS (Mpa) E (%) Referensi

1. Cellulose Acetate (CA) 65,6 30 Cuq et al (1998) 2. Methyl Cellulose (MC) 12,9 500 Cuq et al (1998) 3. Karagenan + 0,5% Gly 8,98 61,3 Handoko (2015)

4. Karagenan + Pati 20 - 50 20 - 60 Abdou & Sorour (2014) 5. Chitosan + 0,1 % Gly 11,58 69,84 Bourbon et al (2011)

6. Zein Protein 0,4 - Cuq et al (1998)

7. Isolat Protein Whey 13,9 30,8 Cuq et al (1998) 8. Protein Myofibril 17,1 22,7 Cuq et al (1998) 9. Isolat protein kedelai (0,1 mm) 4,0 – 4,3 11 - 12 Soliman (2007) 10. Mung Bean + 30% Gly 30 - 40 15 - 17 Wittaya (2013) 11. Low Density Polyethylene

(LDPE)

12,9 500 Cuq et al (1998)

12. Polietilen (PE) 29,9 56,5 Shimadzu (2015)

13. Polipropilen (PP) 38,2 28,4 Shimadzu (2015) 14 Polietilen Terepthalat (PET) 55 125 Matweb (1996) 15. Orientated Polypropylene

(OPP)

165 60 Krochta & De Mulder-Johnston (1997)

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Lampiran 4. Komposisi Asam Amino Fraksi 7S Globulins dan Subunit 7S Globulin (β-Konglisinin & Basic 7S Globulin) Asam Amino

(AA)

Sifat Asam Amino

β-Konglisinin Basic 7S globulin

(BG) (Total AA) (%)4

Total AA 7S Globulins (Total AA) (%)

α'

(Total AA) (%)1

α

(Total AA) (%)2

β

(Total AA) (%)3

Triptofan (Trp) Hidrofobik (3 AA) 0,5 (2 AA) 0,3 (0 AA) 0 (3 AA) 0.7 (8 AA) 0,4 Threonin (Thr) Hidrofilik (14 AA) 2,2 (11 AA) 1,8 (11 AA) 2,5 (30 AA) 7.0 (66 AA) 3,1

Isoleusin (Ile) Hidrofobik (29 AA) 4,5 (31 AA) 5,1 (26 AA) 5,9 (17 AA) 4.0 (103 AA) 4,9 Leusin(Leu) Hidrofobik (49 AA) 7,7 (54 AA) 8,9 (47 AA) 10,7 (45 AA) 10.5 (195 AA) 9,2 Lisin (Lys) Hidrofilik (42 AA) 6,6 (35 AA) 5,8 (21 AA) 4,8 (12 AA) 2.8 (110 AA) 5,2 Metionin (Met) Hidrofobik (6 AA) 0,9 (3 AA) 0,5 (2 AA) 0,5 (10 AA) 2.3 (21 AA) 1,0

Sistein (Cys) Hidrofilik (5 AA) 0,8 (5 AA) 0,8 (1 AA) 0,2 (13 AA) 3.0 (24 AA) 1,1 Phenilalanin

(Phe) Hidrofobik (32 AA) 5,0 (30 AA) 5,0 (30 AA) 6,8 (23 AA) 5.4 (115 AA) 5,4 Tirosin (Tyr) Hidrofilik (15 AA) 2,2 (15 AA) 2,5 (12 AA) 2,7 (7 AA) 1.6 (49 AA) 2,3

Valin (Val) Hidrofobik (32 AA) 5 (27 AA) 4,5 (29 AA) 6,6 (32 AA) 7.5 (120 AA) 5,7 Arginin (Arg) Hidrofilik (43 AA) 6,7 (48 AA) 7,9 (31 AA) 7,1 (14 AA) 3.3 (136 AA) 6,4 Histidin (His) Hidrofilik (22 AA) 3,4 (8 AA) 1,3 (8 AA) 1,8 (14 AA) 3.3 (52 AA) 2,5

Alanin (Ala) Hidrofobik (28 AA) 4,4 (28 AA) 4,6 (23 AA) 5,2 (28 AA) 6.6 (107 AA) 5,1 Aspartat (Asp) Hidrofilik (29 AA) 4,5 (28 AA) 4,6 (21 AA) 4,8 (12 AA) 2.8 (90 AA) 4,3 Asparagin (Asn) Hidrofilik (42 AA) 6,6 (42 AA) 6,9 (33 AA) 7,5 (26 AA) 6,1 (143 AA) 6,8

Glutamin (Gln) Hidrofilik (54 AA) 8,5 (47 AA) 7,8 (33 AA) 7,5 (36 AA) 8.4 (170 AA) 8,0 Glutamat (Glu) Hidrofilik (81 AA) 12,7 (80 AA) 13,2 (37 AA) 8,4 (8 AA) 1.9 (206 AA) 9,7 Glisin (Gly) Hidrofobik (31 AA) 4,9 (26 AA) 4,4 (19 AA) 4,3 (31 AA) 7.3 (107 AA) 5,1 Prolin (Pro) Hidrofobik (35 AA) 5,5 (40 AA) 6,7 (22 AA) 5,0 (27 AA) 6.3 (124 AA) 5,9 Serin (Ser) Hidrofilik (47 AA) 7,4 (45 AA) 7,4 (33 AA) 7,5 (43 AA) 8.3 (168 AA) 8,0

Total (639 AA) 100% (605 AA) 100% (439 AA) 100% (427 AA) 100% (2114 AA) 100% Sifat Asam Amino 38,4% Hidrofobik

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Lampiran 5. Komposisi Asam Amino Fraksi Glisinin (11S) dan Subunit Penyusunnnya (G1 – G5) Asam Amino (AA) Sifat Asam Amino G1 (Total AA) (%)1

G2 (Total AA) (%)2

G3 (Total AA) (%)3

G4 (Total AA) (%)4

G5 (Total AA) (%)5

Total AA Fraksi 11S (%) Triptofan (Trp) Hidrofobik (4 AA) 0,8 (4 AA) 0,8 (3 AA) 0,6 (6 AA) 1,1 (4 AA) 0.8 (21 AA) 0,8 Threonin (Thr) Hidrofilik (20 AA) 4,0 (18 AA) 3,7 (18 AA) 3,7 (21 AA) 3,7 ( 21 AA) 4.1 (98 AA) 3,9 Isoleusin (Ile) Hidrofobik (26 AA) 5,3 (23 AA) 4,7 (24 AA) 5,0 (21 AA) 3,7 (17 AA) 3.3 (111 AA) 4,4

Leusin(Leu) Hidrofobik (37 AA) 7,5 (38 AA) 7,8 (36 AA) 7,5 (44 AA) 7,8 (41 AA) 7.9 (196 AA) 7,7 Lisin (Lys) Hidrofilik (25 AA) 5,1 (19 AA) 3,9 (19 AA) 4,0 (28 AA) 5,0 (19 AA) 3.7 (110 AA) 4,3 Metionin (Met) Hidrofobik (7 AA) 1,4 (8 AA) 1,6 (6 AA) 1,2 (3 AA) 0,5 (5 AA) 1,0 (29 AA) 1,1

Sistein (Cys) Hidrofilik (11 AA) 2,2 (10 AA) 2,1 (11 AA) 2,3 (8 AA) 1,4 (8 AA) 1.6 (48 AA) 1,9 Phenilalanin

(Phe) Hidrofobik (24 AA) 4,8 (22 AA) 4,5 (29 AA) 6,0 (16 AA) 2,8 (18 AA) 3.5 (109 AA) 4,3 Tirosin (Tyr) Hidrofilik (11 AA) 2,2 (11 AA) 2,3 (10 AA) 2,1 (15 AA) 2,7 (15 AA) 2.9 (62 AA) 2,4

Valin (Val) Hidrofobik (24 AA) 4,8 (27 AA) 5,6 (26 AA) 5,4 (35 AA) 6,2 (34 AA) 6.6 (146 AA) 5,8 Arginin (Arg) Hidrofilik (27 AA) 5,5 (29 AA) 6,0 (29 AA) 6,0 (36 AA) 6,4 (33 AA) 6.4 (154 AA) 6,1 Histidin (His) Hidrofilik (8 AA) 1,6 (4 AA) 0,8 (6 AA) 1,2 (15 AA) 2,7 (15 AA) 2.9 (48 AA) 1,9

Alanin (Ala) Hidrofobik (29 AA) 5,9 (33 AA) 6,8 (30 AA) 6,2 (24 AA) 4,3 (20 AA) 3.9 (136 AA) 5,4 Aspartat (Asp) Hidrofilik (17 AA) 3,4 (18 AA) 3,7 (16 AA) 3,3 (30 AA) 5,3 (24 AA) 4.7 (105 AA) 4,1 Asparagin (Asn) Hidrofilik (37 AA) 7,5 (40 AA) 8,2 (36 AA) 7,5 (33 AA) 5,9 (33 AA) 6,4 (179 AA) 7,1 Glutamin (Gln) Hidrofilik (48 AA) 9,7 (51 AA) 10,5 (49 AA) 10,2 (48 AA) 8,5 (45 AA) 8.7 (241 AA) 9,5 Glutamat (Glu) Hidrofilik (41 AA) 8,3 (37 AA) 7,6 (38 AA) 7,9 (55 AA) 9,8 (42 AA) 8,1 (213 AA) 8,4 Glisin (Gly) Hidrofobik (36 AA) 7,3 (35 AA) 7,2 (32 AA) 6,7 (38 AA) 6,8 (41 AA) 7.9 (182 AA) 7,2 Prolin (Pro) Hidrofobik (29 AA) 5,9 (26 AA) 5,4 (29 AA) 6,0 (38 AA) 6,8 (38 AA) 7,4 (160 AA) 6,3 Serin (Ser) Hidrofilik (34 AA) 6,9 (32 AA) 6,6 (34 AA) 7,1 (48 AA) 8,5 (43 AA) 8,3 (191 AA) 7,5

Total (495 AA)

100% (485 AA) 100% (481 AA) 100% (562 AA) 100% (516 AA) 100% (2539 AA) 100% Sifat Asam Amino

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Lampiran 6. Perhitungan Laju Transmisi Uap Air

Rumus perhitungan laju transmisi uap air / water vapour transmission rate (WVTR) (ASTM E96, 1995)

Keterangan :

n : Perubahan berat (gram) t : Waktu (jam)

A : Luas permukaan (m2₎

 WVTR Edible Film 100% IPK Setelah 1 Jam Batch 1

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 1 𝑥 24 = 157.7650}0.024

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 1 𝑥 24 = 133.4344}0.022

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 1 𝑥 24 = 159.1800}0.022

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 2 𝑥 24 = 118,3237}0.036

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 2 𝑥 24 = 136,4670}0.045

Batch 3

𝑊𝑉𝑇𝑅 = _{𝑡. 𝐴}𝑛 𝑊𝑉𝑇𝑅 𝐾𝑜𝑛𝑣𝑒𝑟𝑠𝑖 = 𝑡.𝐴𝑛 x 24

Rata – rata = 150,1265

(13)

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 2 𝑥 24 = 126,6204}0.035

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 3 𝑥 24 = 109,559}0.05

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 3 𝑥 24 = 139,4496}0.069

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 3 𝑥 24 = 115,7673}0.048

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 4 𝑥 24 = 116,6804}0.071

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 4 𝑥 24 = 139,4996}0.092

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 4 𝑥 24 = 119,385}0.066

𝑊𝑉𝑇𝑅 = 0.087

0.03651 𝑥 5 𝑥 24 = 114,3796

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 5 𝑥 24 = 145,5648}0.120

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 5 𝑥 24 = 120,1085}0.083

Rata – rata = 121,6086

Rata – rata = 125,1883

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𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 6 𝑥 24 = 115,0370}0.105

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 6 𝑥 24 = 140,5105}0.139

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 6 𝑥 24 = 120,5905}0.100

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 7 𝑥 24 = 116,4456}0.124

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 7 𝑥 24 = 136,0338}0.157

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 7 𝑥 24 = 124,0363}0.120

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 8 𝑥 24 = 115,0370}0.140

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 8 𝑥 24 = 136,4670}0.180

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 8 𝑥 24 = 120,2894}0.133

Rata – rata = 125,3795

Rata – rata = 125,5052

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𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 9 𝑥 24 = 115,4022}0.158

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 9 𝑥 24 = 137,4779}0.204

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 9 𝑥 24 = 118,9830}0.148

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 10 𝑥 24 = 117,6664}0.179

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 10 𝑥 24 = 132,8279}0.219

Batch 3

𝑊𝑉𝑇𝑅 = 0.164

0.03317 𝑥 10 𝑥 24 = 118,6614

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 11 𝑥 24 = 115,3358}0.193

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 11 𝑥 24 = 136,7427}0.284

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 11 𝑥 24 = 117,7406}0.179

Rata – rata = 123,9544

Rata – rata = 123,0319

(16)

𝑊𝑉𝑇𝑅 = _{0.03651 𝑥 12 𝑥 24 = 110,6546}0.202

Batch 2

𝑊𝑉𝑇𝑅 = _{0.03957 𝑥 12 𝑥 24 = 135,4562}0.268

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 12 𝑥 24 = 115,1643}0.191

 WVTR Edible Film 75% Protein : 25% Karagenan

 WVTR Edible Film 75% Protein : 25% Karagenan Setelah 1 Jam Batch 1

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 1 𝑥 24 = 159,1800}0.022

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 1 𝑥 24 = 311,1245}0.043

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 1 𝑥 24 = 173,6509}0.024

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 2 𝑥 24 = 155,5623}0.043

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 2 𝑥 24 = 231,5345}0.064

Batch 3

Rata – rata = 120,425

Rata – rata = 214,6518

(17)

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 2 𝑥 24 = 141,0913}0.039

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 3 𝑥 24 = 159,1800}0.066

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 3 𝑥 24 = 202,5927}0.084

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 3 𝑥 24 = 127,8263}0.053

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 4 𝑥 24 = 151,9445}0.084

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 4 𝑥 24 = 191,7395}0.106

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 4 𝑥 24 = 123,0027}0.068

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 5 𝑥 24 = 149,0503}0.103

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 5 𝑥 24 = 164,9683}0.114

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 5 𝑥 24 = 130,2382}0.09

Rata – rata = 163,1997

Rata – rata = 155,5623

(18)

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 6 𝑥 24 = 139,8854}0.116

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 6 𝑥 24 = 148,3268}0.123

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 6 𝑥 24 = 136,2677}0.113

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 7 𝑥 24 = 139,5409}0.135

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 7 𝑥 24 = 148,8436}0.144

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 7 𝑥 24 = 139,5409}0.135

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 8 𝑥 24 = 144,7091}0.160

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 8 𝑥 24 = 146,5179}0.162

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 8 𝑥 24 = 138,3781}0.153

Rata – rata = 141,4933

Rata – rata = 142,6418

(19)

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 9 𝑥 24 = 151,9445}0.189

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 9 𝑥 24 = 145,513}0.181

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 9 𝑥 24 = 141,4933}0.176

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 10 𝑥 24 = 149,0503}0.206

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 10 𝑥 24 = 142,5384}0.197

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 10 𝑥 24 = 145,4326}0.201

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 11 𝑥 24 = 153,2601}0.233

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 11 𝑥 24 = 143,3935}0.218

Batch 3

𝑊𝑉𝑇𝑅 = 0.213

0.03317 𝑥 11 𝑥 24 = 140,1047

Rata – rata = 146,3170

Rata – rata = 145,6738

(20)

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 12 𝑥 24 = 153,7534}0.255

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 12 𝑥 24 = 144,7091}0.240

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 12 𝑥 24 = 127,8263}0.212

𝑊𝑉𝑇𝑅 = _{0.001431 𝑥 1 𝑥 24 = 536,5816}0.032

Batch 2

𝑊𝑉𝑇𝑅 = _{0.001231 𝑥 1 𝑥 24 = 350,9326}0.018

Batch 3

𝑊𝑉𝑇𝑅 = _{0.001994 𝑥 1 𝑥 24 = 373,1146}0.031

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 2 𝑥 24 = 385,6681}0.043

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 2 𝑥 24 = 282,6957}0.064

Batch 3

𝑊𝑉𝑇𝑅 = 0.039

0.03317 𝑥 2 𝑥 24 = 330,9887

Rata – rata = 142,0963

Rata – rata = 420,2096

(21)

𝑊𝑉𝑇𝑅 = _{0.001431 𝑥 3 𝑥 24 = 324,1847}0.058

Batch 2

𝑊𝑉𝑇𝑅 = _{0.001231 𝑥 3 𝑥 24 = 266,4488}0.041

Batch 3

𝑊𝑉𝑇𝑅 = _{0.001994 𝑥 3 𝑥 24 = 292,8749}0.073

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 4 𝑥 24 = 280,8670}0.067

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 4 𝑥 24 = 282,6957}0.058

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 4 𝑥 24 = 297,8899}0.099

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 5 𝑥 24 = 258,2299}0.077

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 5 𝑥 24 = 265,1491}0.068

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 5 𝑥 24 = 305,7132}0.127

Rata – rata = 294,5028

Rata – rata = 287,1508

(22)

𝑊𝑉𝑇𝑅 = _{0.001431 𝑥 6 𝑥 24 = 226,3704}0.081

Batch 2

𝑊𝑉𝑇𝑅 = _{0.001231 𝑥 6 𝑥 24 = 266,4488}0.082

Batch 3

𝑊𝑉𝑇𝑅 = _{0.001994 𝑥 6 𝑥 24 = 300,8988}0.150

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 7 𝑥 24 = 229,9636}0.096

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 7 𝑥 24 = 272,9476}0.098

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 7 𝑥 24 = 306,0571}0.178

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 8 𝑥 24 = 220,0823}0.105

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 8 𝑥 24 = 272,9476}0.112

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 8 𝑥 24 = 306,0571}0.203

Rata – rata = 264,5727

Rata – rata = 269,6561

(23)

𝑊𝑉𝑇𝑅 = _{0.001431 𝑥 9 𝑥 24 = 212,3969}0.114

Batch 2

𝑊𝑉𝑇𝑅 = _{0.001231 𝑥 9 𝑥 24 = 266,4488}0.123

Batch 3

𝑊𝑉𝑇𝑅 = _{0.001994 𝑥 9 𝑥 24 = 302,2362}0.226

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 10 𝑥 24 = 211,2790}0.126

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 10 𝑥 24 = 255,4010}0.131

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 10 𝑥 24 = 302,1040}0.251

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 11 𝑥 24 = 214,9375}0.141

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 11 𝑥 24 = 248,1342}0.140

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 11 𝑥 24 = 295,4280}0.270

Rata – rata = 260,3606

Rata – rata = 256,2608

(24)

𝑊𝑉𝑇𝑅 = _{0.003317 𝑥 12 𝑥 24 = 213,7942}0.153

Batch 2

𝑊𝑉𝑇𝑅 = _{0.00317 𝑥 12 𝑥 24 = 235,5798}0.145

Batch 3

𝑊𝑉𝑇𝑅 = _{0.03317 𝑥 12 𝑥 24 = 293,8779}0.293

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 1 𝑥 24 = 653,5801}0.052

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 1 𝑥 24 = 564,1145}0.077

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 1 𝑥 24 = 630,050}0.086

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 2 𝑥 24 = 515,3227}0.082

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 2 𝑥 24 = 388,2866}0.106

Batch 3

Rata – rata = 247,7506

Rata – rata = 615,9149

(25)

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 2 𝑥 24 = 498,1791}0.136

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 3 𝑥 24 = 452,4785}0.108

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 3 𝑥 24 = 327,2353}0.134

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 3 𝑥 24 = 427,3595}0.175

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 4 𝑥 24 = 436,7674}0.139

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 4 𝑥 24 = 300,3727}0.164

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 4 𝑥 24 = 375,4658}0.205

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 5 𝑥 24 = 429,8546}0.171

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 5 𝑥 24 = 300,3727}0.205

Batch 3

Rata – rata = 402,3577

Rata – rata = 370,8686

(26)

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 5 𝑥 24 = 348,7253}0.238

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 6 𝑥 24 = 427,3408}0.204

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 6 𝑥 24 = 307,6988}0.252

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 6 𝑥 24 = 323,5722}0.265

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 7 𝑥 24 = 409,3853}0.228

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 7 𝑥 24 = 335,9569}0.321

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 7 𝑥 24 = 321,3046}0.307

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 8 𝑥 24 = 411,6297}0.262

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 8 𝑥 24 = 335,1719}0.366

Rata – rata = 352,8706

Rata – rata = 355,5489

(27)

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 8 𝑥 24 = 318,6881}0.348

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 9 𝑥 24 = 411,9789}0.295

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 9 𝑥 24 = 323,9792}0.398

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 9 𝑥 24 = 318,2811}0.391

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 10 𝑥 24 = 404,7169}0.322

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 10 𝑥 24 = 321,6185}0.439

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 10 𝑥 24 = 307,6988}0.420

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 11 𝑥 24 = 397,6326}0.348

Batch 2

Rata – rata = 351,4130

Rata – rata = 344,6781

(28)

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 11 𝑥 24 = 311,6949}0.468

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 11 𝑥 24 = 298,3746}0.448

𝑊𝑉𝑇𝑅 = _{0.001909 𝑥 12 𝑥 24 = 386,4921}0.369

Batch 2

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 12 𝑥 24 = 300,3727}0.492

Batch 3

𝑊𝑉𝑇𝑅 = _{0.003276 𝑥 12 𝑥 24 = 289,3834}0.474

 WVTR Edible Film 100% Karagenan

 WVTR Edible Film 100% Karagenan Setelah 1 Jam Batch 1

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 1 𝑥 24 = 764,1796}0.126

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 1 𝑥 24 = 1027,261}0.189

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 1 𝑥 24 = 1054,437}0.194

Rata – rata = 325,416

(29)

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 2 𝑥 24 = 645,9137}0.213

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 2 𝑥 24 = 760,9342}0.280

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 2 𝑥 24 = 861,4862}0.317

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 3 𝑥 24 = 638,838}0.316

Batch 2

𝑊𝑉𝑇𝑅 = 0.359

0.004416 𝑥 3 𝑥 24 = 650,4176

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 3 𝑥 24 = 728,3227}0.402

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 4 𝑥 24 = 623,1703}0.411

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 4 𝑥 24 = 610,1062}0.449

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 4 𝑥 24 = 668,535}0.492

Rata – rata = 756,1114

Rata – rata = 672,5261

(30)

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 5 𝑥 24 = 588,297}0.485

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 5 𝑥 24 = 547,8726}0.504

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 5 𝑥 24 = 613,0955}0.564

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 6 𝑥 24 = 574,1455}0.568

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 6 𝑥 24 = 536,2774}0.592

Batch 3

𝑊𝑉𝑇𝑅 = 0.631

0.004416 𝑥 6 𝑥 24 = 571,6065

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 7 𝑥 24 = 575,3007}0.664

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 7 𝑥 24 = 530,3245}0.683

Batch 3

𝑊𝑉𝑇𝑅 = 0.710

0.004416 𝑥 7 𝑥 24 = 551,2891

 WVTR Edible Film 100% Karagenan Setelah 8 Jam

Rata – rata = 583,0884

Rata – rata = 672,5261

(31)

Batch 1

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 8 𝑥 24 = 574,6509}0.758

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 8 𝑥 24 = 512,9512}0.755

Batch 3

𝑊𝑉𝑇𝑅 = 0.827

0.004416 𝑥 8 𝑥 24 = 561,8684

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 9 𝑥 24 = 599,0791}0.889

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 9 𝑥 24 = 516,9521}0.856

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 9 𝑥 24 = 550,7714}0.912

𝑊𝑉𝑇𝑅 = 0.952

0.003957 𝑥 10 𝑥 24 = 577,3801

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 10 𝑥 24 = 508,7389}0.936

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 10 𝑥 24 = 546,7856}1,006

Rata – rata = 549,8235

Rata – rata = 555,6009

(32)

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 11 𝑥 24 = 549,7021}0.997

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 11 𝑥 24 = 499,5483}1,011

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 11 𝑥 24 = 540,0656}1,093

𝑊𝑉𝑇𝑅 = _{0.003957 𝑥 12 𝑥 24 = 525,1208}1,039

Batch 2

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 12 𝑥 24 = 505,0248}1,115

Batch 3

𝑊𝑉𝑇𝑅 = _{0.004416 𝑥 12 𝑥 24 = 518,6129}1145

Rata – rata = 529,772

(33)

Lampiran 7. Output SPSS Kuat Tarik dan Pemanjangan (Uji One Way Anova, Pos Hoc Duncan)

Tests of Normality

.297 5 .170 .869 5 .263

Tensile_Strength

Statistic df Sig. Statistic df Sig.

Kolmogorov-Smirnova Shapiro-Wilk

Lilliefors Significance Correction a.

Tests of Normality

.208 5 .200* .868 5 .259

Elongasi

This is a lower bound of the true significance. *.

Lilliefors Significance Correction a.

ANOVA

1746.219 4 436.555 1214.508 .000

30.553 85 .359

1776.772 89

250830.4 4 62707.595 1130.395 .000

4715.295 85 55.474

255545.7 89

Between Groups Within Groups Total

Between Groups Within Groups Total Tensile_Strength

Elongasi

Sum of

(34)

Lampiran 8. Output SPSS Laju Transmisi Uap Air (Uji One Way Anova, Pos Hoc Duncan)

Tensile_Strength

Duncana

18 2.1029

18 2.4923

18 3.3792

18 9.8511

18 12.9234

.055 1.000 1.000 1.000

Perlakuan 100% Karagenan Komn 25:75 Komb 50:50 Komb 75:25 100% Protein Sig.

N 1 2 3 4

Subset for alpha = .05

Means for groups in homogeneous subsets are displayed. Uses Harmonic Mean Sample Size = 18.000.

a.

Elongasi

Duncana

18 12.1117

18 14.3948

18 41.2457

18 76.4428

18 154.5522

.360 1.000 1.000 1.000

Perlakuan 100% Protein Komb 75:25 Komb 50:50 Komn 25:75 100% Karagenan Sig.

N 1 2 3 4

(35)

Tests of Normality

.184 5 .200* .937 5 .644

.180 5 .200* .930 5 .595

.176 5 .200* .921 5 .537

.191 5 .200* .911 5 .473

.192 5 .200* .914 5 .494

.196 5 .200* .912 5 .479

.199 5 .200* .918 5 .517

.196 5 .200* .920 5 .530

.189 5 .200* .917 5 .512

.188 5 .200* .918 5 .515

.188 5 .200* .918 5 .517

.188 5 .200* .918 5 .514

WVTR_Jam_1 WVTR_Jam_2 WVTR_Jam_3 WVTR_Jam_4 WVTR_Jam_5 WVTR_Jam_6 WVTR_Jam_7 WVTR_Jam_8 WVTR_Jam_9 WVTR_Jam_10 WVTR_Jam_11 WVTR_Jam_12

This is a lower bound of the true significance. *.

(36)

ANOVA

1261125 4 315281.135 34.743 .000

90745.571 10 9074.557

1351870 14

727654.9 4 181913.715 34.775 .000

52312.072 10 5231.207

779966.9 14

585196.8 4 146299.197 79.051 .000

18506.842 10 1850.684

603703.6 14

501196.8 4 125299.202 88.979 .000

14081.870 10 1408.187

515278.7 14

412094.1 4 103023.530 78.041 .000

13201.148 10 1320.115

425295.3 14

381042.5 4 95260.622 75.851 .000

12558.853 10 1255.885

393601.3 14

366850.6 4 91712.640 106.247 .000

8632.002 10 863.200

375482.6 14

364273.6 4 91068.388 82.522 .000

11035.628 10 1103.563

375309.2 14

370138.0 4 92534.489 69.296 .000

13353.439 10 1335.344

383491.4 14

351717.9 4 87929.486 72.313 .000

12159.629 10 1215.963

363877.6 14

326542.5 4 81635.623 75.151 .000

10862.851 10 1086.285

337405.3 14

308813.1 4 77203.275 77.278 .000

9990.384 10 999.038

318803.5 14 Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total Between Groups Within Groups Total WVTR_Jam_1 WVTR_Jam_2 WVTR_Jam_3 WVTR_Jam_4 WVTR_Jam_5 WVTR_Jam_6 WVTR_Jam_7 WVTR_Jam_8 WVTR_Jam_9 WVTR_Jam_10 WVTR_Jam_11 WVTR_Jam_12 Sum of

(37)

WVTR_Jam_1

Duncana

3 150.1265

3 214.6518

3 420.2096

3 615.9149

3 948.6260

.426 1.000 1.000 1.000

Perlakuan 100% Protein 75 Protein : 25 Karagenan 50 Protein : 50 Karagenan 25 Protein : 75 Karagenan 100% Karagenan Sig.

N 1 2 3 4

a.

WVTR_Jam_2

Duncana

3 127.1371

3 214.6518 214.6518

3 333.1175

3 467.2628

3 756.1114

.169 .073 1.000 1.000

N 1 2 3 4

(38)

WVTR_Jam_3

Duncana

3 121.6086

3 163.1997

3 294.5028

3 402.3577

3 672.5261

.264 1.000 1.000 1.000

N 1 2 3 4

a.

WVTR_Jam_4

Duncana

3 125.1883

3 155.5623

3 287.1508

3 370.8686

3 633.9371

.345 1.000 1.000 1.000

N 1 2 3 4

(39)

WVTR_Jam_5

Duncana

3 126.6843

3 148.0856

3 276.3641

3 359.6509

3 583.0884

.487 1.000 1.000 1.000

N 1 2 3 4

a.

WVTR_Jam_6

Duncana

3 125.3795

3 141.4933

3 264.5727

3 352.8706

3 560.6765

.590 1.000 1.000 1.000

N 1 2 3 4

(40)

WVTR_Jam_7

Duncana

3 125.5052

3 142.6418

3 269.6561

3 355.5489

3 552.3048

.491 1.000 1.000 1.000

N 1 2 3 4

a.

WVTR_Jam_8

Duncana

3 123.9311

3 143.2017

3 266.1474

3 355.1633

3 549.8235

.494 1.000 1.000 1.000

N 1 2 3 4

(41)

WVTR_Jam_9

Duncana

3 123.9544

3 146.3170

3 260.3606

3 351.4130

3 555.6009

.471 1.000 1.000 1.000

N 1 2 3 4

a.

WVTR_Jam_10

Duncana

3 123.0519

3 145.6738

3 256.2608

3 344.6781

3 544.3015

.445 1.000 1.000 1.000

N 1 2 3 4

(42)

WVTR_Jam_11

Duncana

3 123.2730

3 145.5861

3 252.8332

3 335.9007

3 529.7720

.426 1.000 1.000 1.000

N 1 2 3 4

a.

WVTR_Jam_12

Duncana

3 120.4250

3 142.0963

3 247.7506

3 325.4160

3 516.2528

.421 1.000 1.000 1.000

N 1 2 3 4