41
LAMPIRAN 1. Perhitungan
1.1. Persen Kelarutan Edible Film
Rumus :
Total Berat Awal = Berat kertas saring awal + berat sampel awal
Berat Sisa Sampel akhir = Total berat awal – Total berat akhir
Persen Kelarutan = 𝑩𝒆𝒓𝒂𝒕 𝑺𝒊𝒔𝒂 𝑺𝒂𝒎𝒑𝒆𝒍 𝑨𝒌𝒉𝒊𝒓
𝑩𝒆𝒓𝒂𝒕 𝑺𝒂𝒎𝒑𝒆𝒍 𝑨𝒘𝒂𝒍 𝑥 100%
1.1.1 Edible Film Kontrol pH 4 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5312 0,0513 0,5825 0,5391 0,0434 84,6003
2 0,5912 0,0504 0,6416 0,5994 0,0422 83,7301
3 0,5304 0,0501 0,5805 0,5378 0,0427 85,2295
4 0,5505 0,0442 0,5947 0,5571 0,0376 85,0678
5 0,5045 0,0504 0,5549 0,5107 0,0442 87,6984
1.1.2. Edible Film Kontrol pH 4 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5412 0,0524 0,5936 0,5492 0,0444 84,7328
2 0,5035 0,0429 0,5464 0,5101 0,0363 84,6153
3 0,5221 0,0451 0,5672 0,5283 0,0389 86,2527
4 0,5204 0,0524 0,5728 0,5275 0,0453 86,4503
5 0,4901 0,0521 0,5422 0,4981 0,0441 84,6449
6 0,5111 0,0605 0,5716 0,5202 0,0514 84,9586
1.1.3. Edible Film Kontrol pH 7 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,577 0,0513 0,6283 0,5854 0,0429 83,6257
2 0,4756 0,0611 0,5367 0,4852 0,0515 84,2880
3 0,5443 0,0578 0,6021 0,5549 0,0472 81,6608
4 0,5103 0,0532 0,5635 0,5201 0,0434 81,5789
5 0,5841 0,0512 0,6353 0,5932 0,0421 82,2265
1.1.4. Edible Film Kontrol pH 7 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,59 0,0495 0,6395 0,5991 0,0404 81,6161
2 0,5032 0,0523 0,5555 0,5121 0,0434 82,9827
3 0,5641 0,0545 0,6186 0,5742 0,0444 81,4678
4 0,5023 0,0466 0,5489 0,5101 0,0388 83,2618
5 0,5153 0,0432 0,5585 0,5231 0,0354 81,9444
6 0,5272 0,0477 0,5749 0,5357 0,0392 82,1802
1.1.5. Edible Film Kontrol pH 10 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,505 0,062 0,567 0,5162 0,0508 81,9354
2 0,5123 0,0521 0,5644 0,5221 0,0423 81,1900
3 0,5263 0,056 0,5823 0,5358 0,0465 83,0357
4 0,5307 0,0494 0,5801 0,5381 0,042 85,0202
5 0,5258 0,0591 0,5849 0,5381 0,0468 79,1878
1.1.6. Edible Film Kontrol pH 10 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,523 0,0571 0,5801 0,5307 0,0494 86,5148
2 0,5011 0,0542 0,5553 0,5101 0,0452 83,3948
3 0,5424 0,0495 0,5919 0,5511 0,0408 82,4242
4 0,5601 0,0601 0,6202 0,5702 0,05 83,1946
5 0,5353 0,0491 0,5844 0,5432 0,0412 83,9103
6 0,543 0,0532 0,5962 0,5512 0,045 84,5864
1.1.7. Edible Film Kontrol pH 4 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,4991 0,0571 0,5562 0,5037 0,0525 91,9439
2 0,5421 0,0551 0,5972 0,5465 0,0507 92,0145
3 0,5901 0,0592 0,6493 0,5952 0,0541 91,3851
4 0,5133 0,0601 0,5734 0,5171 0,0563 93,6772
5 0,5112 0,0578 0,569 0,5172 0,0518 89,6193
1.1.8. Edible Film Kontrol pH 4 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5115 0,0523 0,5638 0,5158 0,048 91,7782
2 0,529 0,0486 0,5776 0,5321 0,0455 93,6213
3 0,512 0,0496 0,5616 0,516 0,0456 91,9354
4 0,5461 0,058 0,6041 0,5497 0,0544 93,7931
5 0,5132 0,0542 0,5674 0,5171 0,0503 92,8044
6 0,5111 0,0611 0,5722 0,5165 0,0557 91,1620
1.1.9. Edible Film Kontrol pH 7 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5227 0,0503 0,573 0,5294 0,0436 86,6799
2 0,5711 0,0601 0,6312 0,5761 0,0551 91,6805
3 0,547 0,0537 0,6007 0,5531 0,0476 88,6405
4 0,5557 0,0532 0,6089 0,5613 0,0476 89,4736
5 0,534 0,0515 0,5855 0,5401 0,0454 88,1553
1.1.10.Edible Film Kontrol pH 7 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,545 0,0477 0,5927 0,5495 0,0432 90,5660
2 0,5482 0,0556 0,6038 0,553 0,0508 91,3669
3 0,5931 0,0631 0,6562 0,6001 0,0561 88,9064
4 0,582 0,0494 0,6314 0,5864 0,045 91,0931
5 0,5463 0,0561 0,6024 0,5512 0,0512 91,2655
6 0,5123 0,0513 0,5636 0,5164 0,0472 92,0077
1.1.11.Edible Film Kontrol pH 10 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5901 0,054 0,6441 0,5956 0,0485 89,8148
2 0,5223 0,0571 0,5794 0,5283 0,0511 89,4921
3 0,5321 0,058 0,5901 0,5373 0,0528 91,0344
4 0,5283 0,0593 0,5876 0,5333 0,0543 91,568
5 0,5278 0,0532 0,581 0,5341 0,0469 88,1578
1.1.12.Edible Film Kontrol pH 10 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5014 0,0541 0,5555 0,5065 0,049 90,5730
2 0,5908 0,0495 0,6403 0,5961 0,0442 89,2929
3 0,555 0,0605 0,6155 0,5608 0,0547 90,4132
4 0,6016 0,0473 0,6489 0,6061 0,0428 90,4862
5 0,5445 0,0477 0,5922 0,5493 0,0429 89,9371
6 0,5321 0,0523 0,5844 0,5365 0,0479 91,5869
1.1.13.Edible Film Gliserol pH 4 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,517 0,0521 0,5691 0,5239 0,0452 86,7562
2 0,5231 0,0501 0,5732 0,5306 0,0426 85,0299
3 0,5187 0,0497 0,5684 0,5275 0,0409 82,2937
4 0,5107 0,0661 0,5768 0,5217 0,0551 83,3585
5 0,5452 0,0563 0,6015 0,5521 0,0494 87,7442
1.1.14.Edible Film Gliserol pH 4 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5152 0,053 0,5682 0,5228 0,0454 85,6603
2 0,543 0,0479 0,5909 0,5501 0,0408 85,1774
3 0,5302 0,0465 0,5767 0,5379 0,0388 83,4408
4 0,5142 0,0524 0,5666 0,5208 0,0458 87,4045
5 0,553 0,0549 0,6079 0,5602 0,0477 86,8852
6 0,5202 0,0515 0,5717 0,5268 0,0449 87,1844
1.1.15.Edible Film Gliserol pH 7 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5545 0,0495 0,604 0,5635 0,0405 81,8181
2 0,5017 0,0561 0,5578 0,5101 0,0477 85,0267
3 0,5226 0,0508 0,5734 0,5303 0,0431 84,8425
4 0,5123 0,0532 0,5655 0,5221 0,0434 81,5789
5 0,5874 0,0521 0,6395 0,5978 0,0417 80,0383
1.1.16.Edible Film Gliserol pH 7 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,518 0,0487 0,5667 0,5273 0,0394 80,9034
2 0,5421 0,0433 0,5854 0,5491 0,0363 83,8337
3 0,5011 0,0495 0,5506 0,5101 0,0405 81,8181
4 0,538 0,0498 0,5878 0,5461 0,0417 83,7349
5 0,543 0,0523 0,5953 0,552 0,0433 82,7915
6 0,5281 0,0535 0,5816 0,5381 0,0435 81,3084
1.1.17.Edible Film Gliserol pH 10 Suhu 75oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5657 0,0573 0,623 0,5768 0,0462 80,6282
2 0,5552 0,0543 0,6095 0,5634 0,0461 84,8987
3 0,5212 0,0567 0,5779 0,5322 0,0457 80,5996
4 0,5477 0,0543 0,602 0,5578 0,0442 81,3996
5 0,5322 0,0578 0,59 0,5437 0,0463 80,1038
1.1.18.Edible Film Gliserol pH 10 Suhu 75oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,532 0,0567 0,5887 0,5424 0,0463 81,6578
2 0,5481 0,0404 0,5885 0,5559 0,0326 80,6930
3 0,5523 0,0442 0,5965 0,5594 0,0371 83,9366
4 0,5226 0,0541 0,5767 0,5327 0,044 81,3308
5 0,5391 0,057 0,5961 0,5483 0,0478 83,8596
6 0,5433 0,0497 0,593 0,5524 0,0406 81,6901
1.1.19.Edible Film Gliserol pH 4 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5323 0,0497 0,582 0,5355 0,0465 93,5613
2 0,512 0,0491 0,5611 0,5161 0,045 91,6496
3 0,5211 0,0542 0,5753 0,5242 0,0511 94,2804
4 0,5332 0,0508 0,584 0,5358 0,0482 94,8818
5 0,5012 0,0455 0,5467 0,5038 0,0429 94,2857
1.1.20.Edible Film Gliserol pH 4 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5441 0,0501 0,5942 0,547 0,0472 94,2115
2 0,5361 0,0476 0,5837 0,539 0,0447 93,9075
3 0,5212 0,0487 0,5699 0,524 0,0459 94,2505
4 0,545 0,0541 0,5991 0,5497 0,0494 91,3123
5 0,5291 0,0496 0,5787 0,5323 0,0464 93,5483
6 0,5032 0,0517 0,5549 0,507 0,0479 92,6499
1.1.21.Edible Film Gliserol pH 7 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5867 0,0523 0,639 0,5904 0,0486 92,9254
2 0,5192 0,0517 0,5709 0,5238 0,0471 91,1025
3 0,5231 0,057 0,5801 0,5289 0,0512 89,8245
4 0,5437 0,0493 0,593 0,5471 0,0459 93,1034
5 0,5212 0,0516 0,5728 0,5248 0,048 93,0232
1.1.22.Edible Film Gliserol pH 7 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,537 0,0601 0,5971 0,5434 0,0537 89,3510
2 0,549 0,056 0,605 0,5531 0,0519 92,6785
3 0,5221 0,0423 0,5644 0,527 0,0374 88,4160
4 0,529 0,0591 0,5881 0,5354 0,0527 89,1708
5 0,5471 0,0547 0,6018 0,5523 0,0495 90,4936
6 0,5231 0,0601 0,5832 0,529 0,0542 90,1830
1.1.23.Edible Film Gliserol pH 10 Suhu 100oC dengan Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5116 0,0543 0,5659 0,5164 0,0495 91,1602
2 0,5213 0,0562 0,5775 0,5261 0,0514 91,4590
3 0,5128 0,0537 0,5665 0,5172 0,0493 91,8063
4 0,519 0,0473 0,5663 0,5233 0,043 90,9090
5 0,5281 0,0502 0,5783 0,5327 0,0456 90,8366
1.1.24.Edible Film Gliserol pH 10 Suhu 100oC Tanpa Larutan yang Mengandung Lemak
Ulangan Kertas Saring Awal
(gram)
Sampel Awal (gram)
Total Berat Awal (gram)
Total Berat Akhir (gram)
Sampel Akhir (gram)
Kelarutan (%)
1 0,5354 0,0443 0,5797 0,5402 0,0395 89,1647
2 0,532 0,0405 0,5725 0,5362 0,0363 89,6296
3 0,5311 0,0453 0,5764 0,5348 0,0416 91,8322
4 0,5534 0,0543 0,6077 0,5581 0,0496 91,3443
5 0,5034 0,0535 0,5569 0,5081 0,0488 91,2149
6 0,5302 0,0495 0,5797 0,5352 0,0445 89,8989
1.2. Perhitungan Water Vapour Transmission Rate (WVTR) Edible Film
Nilai WVTR edible film terhadap uap air akan diperoleh menggunakan rumus :
Keterangan simbol:
n : Water lost / air yang berdifusi melewati film (gram) t : Waktu (jam)
37
1.2.1. WVTR Edible Film Kontrol
1.2.1.1 WVTR Edible Film Kontrol Setelah 1 Jam
Batch 1
0,05 0,002375
𝑥
24
1
=
505,3483Batch 2
0,0503 0,002375
𝑥
24
1
=
508,71731.2.1.2 WVTR Edible Film Kontrol Setelah 2 Jam
Batch 1
0,1043 0,002375
𝑥
24
2
=
527,2467Batch 2
0,1086 0,002375
𝑥
24
2
=
549,14511.2.1.3 WVTR Edible Film Kontrol Setelah 3 Jam
Batch 1
0,1042 0,002375
𝑥
24
3
=
478,3964Batch 2
0,1496 0,002375
𝑥
24
3
=
504,22531.2.1.4 WVTR Edible Film Kontrol Setelah 4 Jam
Batch 1
0,1673 0,002375
𝑥
24
4
=
422,8081Rata-rata = 507,0328
Rata-rata = 538,1959
Rata-rata = 491,3108
Batch 2
0,2016 0,002375
𝑥
24
4
=
509,55951.2.1.5 WVTR Edible Film Kontrol Setelah 5 Jam
Batch 1
0,2016 0,002375
𝑥
24
5
=
407,6476Batch 2
0,2496 0,002375
𝑥
24
5
=
504,67451.2.1.6 WVTR Edible Film Kontrol Setelah 6 Jam
Batch 1
0,2443 0,002375
𝑥
24
6
=
411,5781Batch 2
0,249 0,002375
𝑥
24
6
=
495,24131.2.1.7 WVTR Edible Film Kontrol Setelah 7 Jam
Batch 1
0,293 0,002375
𝑥
24
7
=
423,53Batch 2
0,3346 0,002375
𝑥
24
7
=
483,2092Rata-rata = 456,161
Rata-rata = 453,4097
1.2.1.8 WVTR Edible Film Kontrol Setelah 8 Jam
Batch 1
0,3216 0,002375
𝑥
24
8
=
406,3842Batch 2
0,3646 0,002375
𝑥
24
8
=
460,70921.2.1.9 WVTR Edible Film Kontrol Setelah 9 Jam
Batch 1
0,3543 0,002375
𝑥
24
9
=
397,915Batch 2
0,3933 0,002375
𝑥
24
9
=
441,71181.2.1.10 WVTR Edible Film Kontrol Setelah 10 Jam
Batch 1
0,388 0,002375
𝑥
24
10
=
392,1503Batch 2
0,4866 0,002375
𝑥
24
10
=
433,25191.2.1.11 WVTR Edible Film Kontrol Setelah 11 Jam
Batch 1
0,4243 0,002375
𝑥
24
11
=
389,8838Rata-rata = 433,5467
Rata-rata = 419,8134
Rata-rata = 412,7011
Batch 2
0,4656 0,002375
𝑥
24
11
=
441,71181.2.1.12 WVTR Edible Film Kontrol Setelah 12 Jam
Batch 1
0,4586 0,002375
𝑥
24
12
=
386,3107Batch 2
0,5016 0,002375
𝑥
24
12
=
422,52731.2.2. WVTR Edible Film Dengan Penambahan Gliserol
1.2.2.1. WVTR Edible Film Gliserol Setelah 1 Jam
Batch 1
0,118 0,002375
𝑥
24
1
=
1192,622Batch 2
0,113 0,002375
𝑥
24
1
=
1142,0871.2.2.2.WVTR Edible Film Gliserol Setelah 2 Jam
Batch 1
0,192 0,002375
𝑥
24
2
=
970,2687Rata-rata = 404,419
Rata-rata = 1167,355
Batch 2
0,213 0,002375
𝑥
24
2
=
1076,3921.2.2.3.WVTR Edible Film Gliserol Setelah 3 Jam
Batch 1
0,25 0,002375
𝑥
24
3
=
842,2471Batch 2
0,251 0,002375
𝑥
24
3
=
845,61611.2.2.4.WVTR Edible Film Gliserol Setelah 4 Jam
Batch 1
0,285 0,002375
𝑥
24
4
=
720,1213Batch 2
0,292 0,002375
𝑥
24
4
=
737,80851.2.2.5.WVTR Edible Film Gliserol Setelah 5 Jam
Batch 1
0,323 0,002375
𝑥
24
5
=
652,91Batch 2
0,334 0,002375
𝑥
24
5
=
675,14531.2.2.6.WVTR Edible Film Gliserol Setelah 6 Jam
Batch 1
0,366 0,002375
𝑥
24
6
=
616,5249Rata-rata = 843,9316
Rata-rata = 728,9649
Rata-rata = 664,0276
Batch 2
0,349 0,002375
𝑥
24
6
=
587,88851.2.2.7.WVTR Edible Film Gliserol Setelah 7 Jam
Batch 1
0,387 0,002375
𝑥
24
7
=
558,7708Batch 2
0,364 0,002375
𝑥
24
7
=
525,56221.2.2.8.WVTR Edible Film Gliserol Setelah 8 Jam
Batch 1
0,438 0,002375
𝑥
24
8
=
553,3564Batch 2
0,413 0,002375
𝑥
24
8
=
521,77211.2.2.9.WVTR Edible Film Gliserol Setelah 9 Jam
Batch 1
0,498 0,002375
𝑥
24
9
=
559,2521Batch 2
0,453 0,002375
𝑥
24
9
=
508,7173Rata-rata = 542,1665
Rata-rata = 537,5642
1.2.2.10. WVTR Edible Film Gliserol Setelah 10 Jam
Batch 1
0,548 0,002375
𝑥
24
10
=
553,8617Batch 2
0,501 0,002375
𝑥
24
10
=
506,3591.2.2.11.WVTR Edible Film Gliserol Setelah 11 Jam
Batch 1
0,598 0,002375
𝑥
24
11
=
549,4514Batch 2
0,563 0,002375
𝑥
24
11
=
517,29291.2.2.12.WVTR Edible Film Gliserol Setelah 12 Jam
Batch 1
0,638 0,002375
𝑥
24
12
=
537,3537Batch 2
0,618 0,002375
𝑥
24
12
=
520,5087Rata-rata = 530,1103
Rata-rata = 533,3721
LAMPIRAN 2. Output SPSS
2.1. Output SPSS uji One Way Anova, Pos Hoc Duncan
2.1.1. Kelarutan Edible Film yang Dilarutkan pada pH 4 dan Berbagai Suhu (75oC
dan 100oC)
2.1.2. Kelarutan Edible Film yang dilarutkan pada pH 7 dan Berbagai Suhu (75oC
dan 100oC)
ANOVA
kelarutan
690,119 7 98, 588 50, 837 ,000
77, 573 40 1, 939
767,692 47
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 84, 9311
6 84, 9818
6 85, 2758
6 85, 9588
6 91, 9096
6 92, 5158
6 93, 3134
6 93, 4476
,252 ,087
perlakuan
gliserol+lemak 75oC kontrol+lemak 75oC kontrol tanpa lemak 75oC gliserol t anpa lemak 75oC
kontrol+lemak 100oC kontrol tanpa lemak 100oC
gliserol t anpa lemak 100oC
gliserol+lemak100oC Sig.
N 1 2
Subset f or alpha = .05
Means f or groups in homogeneous subsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Tests of Normal ity
,103 48 ,200* ,923 48 ,004
kelarutan1
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
This is a lower bound of t he t rue signif icance. *.
2.1.3. Kelarutan Edible Film yang dilarutkan pada pH 10 dan Berbagai Suhu (75oC
dan 100oC)
Tests of Normal ity
,119 48 ,086 ,907 48 ,001
kelarutan2
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
Lillief ors Signif ic ance Correct ion a.
ANOVA
kelarutan
755,239 7 107,891 51, 480 ,000
83, 831 40 2, 096
839,070 47
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 82, 2422
6 82, 3984
6 82, 7478
6 82, 7730
6 88, 4430
6 90, 0489 90, 0489
6 90, 8677
6 91, 7509
,569 ,062 ,060
perlakuan
kontrol tanpa lemak 75oC gliserol t anpa lemak 75oC
kontrol+lemak 75oC gliserol+lemak 75oC kontrol+lemak 100oC gliserol t anpa lemak 100oC
kontrol tanpa lemak 100oC
gliserol+lemak100oC Sig.
N 1 2 3
Subset f or alpha = .05
Means f or groups in homogeneous subsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Tests of Normali ty
,152 48 ,007 ,913 48 ,002
kelarutansin
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
2.1.4. Kelarutan Edible Film yang dilarutkan pada suhu 75oC dan Berbagai pH
( 4, 7, 10)
ANOVA
kelarutan
700,844 7 100,121 29, 489 ,000
135,807 40 3, 395
836,650 47
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 82, 0994
6 82, 1947
6 83, 4236
6 84, 0042
6 89, 8934
6 90, 3816
6 90, 5142
6 91, 0638
,109 ,324
perlakuan
gliserol+lemak 75oC gliserol t anpa lemak 75oC
kontrol+lemak 75oC kontrol tanpa lemak 75oC kontrol+lemak 100oC kontrol tanpa lemak 100oC
gliserol t anpa lemak 100oC
gliserol+lemak100oC Sig.
N 1 2
Subset f or alpha = .05
Means f or groups in homogeneous subsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Tests of Normal ity
,083 72 ,200* ,978 72 ,230
kelarutan
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
This is a lower bound of t he true signif icance. *.
2.1.5. Kelarutan Edible Film yang dilarutkan pada suhu 100oC dan Berbagai pH
(4,7,10)
ANOVA
kelarutan
127,019 11 11, 547 3, 446 ,001
201,057 60 3, 351
328,077 71
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 82, 0994
6 82, 1947
6 82, 2422
6 82, 3984
6 82, 7478 82, 7478
6 82, 7730 82, 7730
6 83, 4236 83, 4236 83, 4236
6 84, 0042 84, 0042 84, 0042 84, 0042
6 84, 9311 84, 9311 84, 9311
6 84, 9818 84, 9818 84, 9818
6 85, 2758 85, 2758
6 85, 9588
,129 ,067 ,124 ,104
perlakuan
gliserol + lemak pH 10 gliserol t anpa lemak pH10
kontrol tanpa lemak pH7 gliserol t anpa lemak pH7 kontrol+lemak pH 7 gliserol+lemak pH7 kontrol+lemak pH 10 kontrol tanpa lemak pH10 gliserol+lemak pH4 kontrol+lemak pH 4 kontrol tanpa lemak pH4 gliserol t anpa lemak pH4 Sig.
N 1 2 3 4
Subset f or alpha = .05
Means f or groups in homogeneous s ubsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Tests of Normal ity
,072 72 ,200* ,984 72 ,484
kelarutan
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
This is a lower bound of t he true signif icance. *.
2.1.6.Kelarutan Edible Film yang dilarutkan pada Larutan yang Mengandung
Lemak pada Berbagai Suhu (75oC dan 100oC)
ANOVA
kelarutan
143,723 11 13, 066 8, 153 ,000
96, 153 60 1, 603
239,876 71
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 88, 4430
6 89, 8934 89, 8934 6 90, 0489
6 90, 3816 90, 3816
6 90, 5142 90, 5142
6 90, 8677 90, 8677
6 91, 0638 91, 0638 91, 0638
6 91, 7509 91, 7509 91, 7509
6 91, 9096 91, 9096 91, 9096 91, 9096 6 92, 5158 92, 5158 92, 5158
6 93, 3134 93, 3134
6 93, 4476
,052 ,168 ,070 ,073 ,054 ,058 perlakuan
kontrol+lemak pH7 kontrol+lemak pH10 gliserol t anpa lemak pH 7 kontrol tanpa lemak pH10 gliserol t anpa lemak pH10
kontrol tanpa lemak pH7 gliserol + lemak pH 10 gliserol+lemak pH7 kontrol+lemak pH4 kontrol tanpa lemak pH4 gliserol t anpa lemak pH 4 gliserol+lemak pH4 Sig.
N 1 2 3 4 5 6
Subset f or alpha = .05
Means f or groups in homogeneous s ubset s are display ed. Uses Harmonic Mean Sample Size = 6,000.
a.
Tests of Normal ity
,094 72 ,186 ,929 72 ,001
kelarutansinn
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
2.1.7. Kelarutan Edible Film yang dilarutkan pada Larutan Tanpa Lemak pada
Berbagai Suhu (75oC dan 100oC)
ANOVA
kelarutan
1171,943 11 106,540 29, 805 ,000
214,477 60 3, 575
1386,420 71
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 82, 0994
6 82, 7478 82, 7478
6 82, 7730 82, 7730
6 83, 4236 83, 4236
6 84, 9311
6 84, 9818
6 88, 4430
6 89, 8934 89, 8934
6 91, 0638
6 91, 7509 91, 7509
6 91, 9096 91, 9096
6 93, 4476
,276 ,072 ,189 ,096 ,148
perlakuan
gliserol pH10 75oC kontrol pH7 75oC gliserol pH 7 75oC kontro pH 10 75oC gliserol pH 4 75oC kontrol pH4 75oC kontrol pH7 100oC kontrol pH10 100oC gliserol pH 10 100oC gliserol pH 7 100oC kontrol pH4 100oC gliserol pH 4 100oC Sig.
N 1 2 3 4 5
Subset f or alpha = .05
Means f or groups in homogeneous s ubsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Tests of Normali ty
,128 72 ,005 ,918 72 ,000
kelarutansin
Stat is tic df Sig. Stat is tic df Sig.
Kolmogorov -Smirnova Shapiro-Wilk
2.2. Uji SPSS Independent Sampels T-Test
2.2.1. Uji Kuat Tarik (Tensile Strength)
2.2.2. Uji Pemanjangan (Elongasi)
ANOVA
kelarutan
1173,195 11 106,654 77, 348 ,000
82, 733 60 1, 379
1255,929 71
Between Groups Within Groups Tot al
Sum of
Squares df Mean Square F Sig.
kel arutan
Duncana
6 82, 1947
6 82, 2422
6 82, 3984
6 84, 0042
6 85, 2758 85, 2758
6 85, 9588
6 90, 0489
6 90, 3816
6 90, 5142
6 90, 8677
6 92, 5158
6 93, 3134
,780 ,066 ,318 ,279 ,244
perlakuan
gliserol pH10 75oC kontrol pH7 75oC gliserol pH 7 75oC kontro pH 10 75oC kontrol pH4 75oC gliserol pH 4 75oC gliserol pH 7 100oC kontrol pH10 100oC gliserol pH 10 100oC kontrol pH7 100oC kontrol pH4 100oC gliserol pH 4 100oC Sig.
N 1 2 3 4 5
Subset f or alpha = .05
Means f or groups in homogeneous s ubsets are display ed. Uses Harmonic Mean Sample Size = 6, 000.
a.
Independent Samples Test
3, 369 ,096 19, 908 10 ,000 11, 86406 ,59593 10, 53625 13, 19188
19, 908 7, 235 ,000 11, 86406 ,59593 10, 46414 13, 26398 Equal v ariances
ass umed Equal v ariances not as sumed TensileStrength
F Sig. Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
2.2.3. Uji WVTR
2.2.3.1. Uji WVTR Setelah 1 Jam
2.2.3.2. Uji WVTR Setelah 2 Jam
2.2.3.3. Uji WVTR Setelah 3 Jam
Independent Samples Test
3, 333 ,098 -19,174 10 ,000 -57,03447 2, 97460 -63,66229 -50,40665 -19,174 6, 372 ,000 -57,03447 2, 97460 -64,21124 -49,85769 Equal v ariances
ass umed Equal v ariances not as sumed elongasi
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idence
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
3E+017 ,000 -26,075 2 ,001 -660,32174 25, 32350 -769,280 -551,364 -26,075 1, 009 ,024 -660,32174 25, 32350 -975,465 -345,179 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
5E+017 ,000 -8,954 2 ,012 -485,13434 54, 17947 -718,250 -252,019
-8,954 1, 085 ,060 -485,13434 54, 17947 -1058, 31 88, 04043 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
2E+018 ,000 -27,075 2 ,001 -352,62079 13, 02385 -408,658 -296,584
-27,075 1, 034 ,021 -352,62079 13, 02385 -505,778 -199,463 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
2.2.3.4. Uji WVTR Setelah 4 Jam
2.2.3.5. Uji WVTR Setelah 5 Jam
2.2.3.6. Uji WVTR Setelah 6 Jam
2.2.3.7. Uji WVTR Setelah 7 Jam
2.2.3.8. Uji WVTR Setelah 8 Jam
Independent Samples Test
3E+017 ,000 -5,936 2 ,027 -262,78110 44, 26808 -453,251 -72,31093
-5,936 1, 083 ,093 -262,78110 44, 26808 -732,960 207,39809 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
4E+016 ,000 -4,176 2 ,053 -207,86659 49, 77103 -422,014 6, 28088
-4,176 1, 105 ,131 -207,86659 49, 77103 -714,775 299,04155 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
2E+016 ,000 -3,365 2 ,078 -148,79699 44, 21419 -339,035 41, 44130 -3,365 1, 231 ,145 -148,79699 44, 21419 -513,564 215,96980 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
5E+015 ,000 -2,600 2 ,122 -88,79691 34, 14828 -235,725 58, 13129 -2,600 1, 565 ,155 -88,79691 34, 14828 -282,704 105,11030 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
2.2.3.9. Uji WVTR Setelah 9 Jam
2.2.3.10. Uji WVTR Setelah 10 Jam
2.2.3.11. Uji WVTR Setelah 11 Jam
2.2.3.12. Uji WVTR Setelah 12 Jam
Independent Samples Test
2E+017 ,000 -3,311 2 ,080 -104,01752 31, 41960 -239,205 31, 17011 -3,311 1, 607 ,107 -104,01752 31, 41960 -276,438 68, 40275 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
2E+014 ,000 -3,415 2 ,076 -114,17128 33, 43626 -258,036 29, 69332 -3,415 1, 960 ,078 -114,17128 33, 43626 -260,857 32, 51459 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
4E+014 ,000 -3,738 2 ,065 -117,40925 31, 40803 -252,547 17, 72858 -3,738 1, 960 ,067 -117,40925 31, 40803 -255,258 20, 43968 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Interv al of the Dif f erence t-test f or Equality of Means
Independent Samples Test
4E+016 ,000 -4,176 2 ,053 -207,86659 49, 77103 -422,014 6, 28088 -4,176 1, 105 ,131 -207,86659 49, 77103 -714,775 299,04155 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e
Independent Samples Test
9E+015 ,000 -6,235 2 ,025 -124,51220 19, 97120 -210,441 -38,58304 -6,235 1, 413 ,054 -124,51220 19, 97120 -255,556 6, 53127 Equal v ariances
ass umed Equal v ariances not as sumed WVTR
F Sig.
Lev ene's Test f or Equality of Varianc es
t df Sig. (2-t ailed) Mean Dif f erence
Std. Error
Dif f erence Lower Upper 95% Conf idenc e