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Factors screening to statistical experimental design of racemic atenolol kinetic resolution via transesterification reaction in organic solvent using free Pseudomonas fluorescens lipase

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Academic year: 2019

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FIGURE 1Flow chart of the study
TABLE 1The experimental factors and their levels
FIGURE 2Comparison of enzymes performance [155 rpm, 40°C,lipoprotein: 3200 U, PFL30.04 mM racemic atenolol in THF (PFL18.8 mM racemic atenolol in THF (lipoprotein, PFL‐Sigma) or‐Fluka); 2.4 molar ratio,‐Fluka: 800 U, PFL‐Sigma: 3200 U]
FIGURE 3Enzymatic transesterification in phosphate buffers
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Factors screening to statistical experimental design of racemic atenolol kinetic resolution via transesterification reaction in organic solvent using free Pseudomonas fluorescens lipase

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