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Synthesis of zinc oxide whiskers with hydrothermal method for composite absorbent material of microwave of ZnOw/MWCNT/ epoxy

(Article) (Open Access)

, , , ,

Department of Physics, Faculty of Science and Mathematics, Diponegoro University, UNDIP, Semarang, 50275, Indonesia

Research and Development Center, Ministry of Defence, Republic of Indonesia, PUSLITBANG IPTEKHAN, Jakarta, 12450, Indonesia

Abstract

The MWCNT/ZnOw/epoxy composites have great potential as microwave absorbing material. The synthesis of ZnO whiskers (ZnOw) was carried out using precursors ZnSO and Na CO via hydrothermal method with temperatures of 120°C, 160°C, 200°C, and 240°C. X-ray diﬀraction (XRD) and scanning electron microscope (SEM) were applied to ﬁnd out the morphology and structure of ZnOw powder. The best results of the XRD and SEM-EDX at hydrothermal temperature of 160°C showed the best crystallinity of ZnO compound, that is at 2θ values of 31.7°, 32.2°, 34.3°, 36.1°, 37.9°, 56.5°, 62.8°, 67.8°, 76.8° and 89.5° with a Miller index of 111, 100, 002, 101, 102, 110, 103, 112, 202 and 203, respectively. At 160°C, ZnO whiskers had a size of 97.7 nm, with a purity level of 72.6%. By adding 4% MWCNT, the result of synthesis via spray pyrolysis method (purity 90%) and 4% of epoxy, the ZnOw synthesised by hydrothermal method formed MWCNT/ ZnOw/epoxy composites. To determine the composite's microwave absorption capability, a vector network analyser was administered at hydrothermal temperatures of 160°C and 200°C. The

MWCNT/ZnOw/epoxy composites had a reﬂection loss of -11.9 dB. This value exceeds the standard for microwave absorbing material which is -11.9 dB. Therefore, the composite has great potential as a microwave absorbing material.

SciVal Topic Prominence

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Author keywords

Composites Hydrothermal MWCNT Zinc oxide whiskers ZnOw

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Volume 29, 2018, Pages 257-264

Ristiawan, M.W.â  Priyonoâ Subagio, A.â Kholil, A.M.A.â Ajiesastra, A.^b 

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4 2 3

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Zinc oxide | Nanorods | Seed layers



Chemistry database information 

Substances

⤢

Zn O

⤢

Fe C C H HH HH

HH HHH

⤢

H₂O

S

O O

O Zn O 7

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O O

O 2 Na

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References (17)

Engineering controlled terms:

Composite materials II-VI semiconductors Microwaves

Multiwalled carbon nanotubes (MWCN) Scanning electron microscopy Sodium Carbonate Sodium compounds Spray pyrolysis X ray diﬀraction Zinc oxide

Engineering uncontrolled terms

Hydrothermal Hydrothermal temperature Microwave absorbing materials

Morphology and structures MWCNT Spray pyrolysis method Zinc oxide whisker ZnOw

Engineering main heading:

Hydrothermal synthesis

Funding details

Funding text

The authors thank all parties which have been supporting this research work. The authors also would like to thank Diponegoro University and The Ministry of Research, Technology and Higher Education, Indonesia for ﬁnancial support. They are also indebted to Mr. Chasbullah Hindratmo for his valuable assistance in Laboratory Nanotechnology, Diponegoro University.

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ISSN: 16753402 Source Type: Journal Original language: English

DOI: 10.21315/jps2018.29.s2.20 Document Type: Article

Publisher: Penerbit Universiti Sains Malaysia

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Electromagnetic properties of Si-C-N based ceramics and composites

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Synthesis and optical properties of tetrapod-like zinc oxide nanorods

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Preparation of ZnO cluster and rod-like whiskers through hydrothermal methods

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Organic molecule-assisted hydrothermal self-assembly of size-controlled tubular ZnO nanostructures

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Synthesis of ZnO whiskers via hydrothermal decomposition route

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Enhanced electromagnetic absorption properties of carbon nanotubes and zinc oxide whisker microwave absorber

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Selected-Control Synthesis of ZnO Nanowires and Nanorods via a PEG-Assisted Route

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The Journal of Physical Science (ISSN 1675-3402) is a refereed journal published by Penerbit Universiti Sains Malaysia (USM Press). It is abstracted by Chemical Abstracts Service and indexed in Scopus, ProQuest, Ebsco, Directory of Open Access Journals (DOAJ), ASEAN Citation Index (ACI), Directory of Open Access Scholarly Resources (ROAD), Information Matrix for the Analysis of Journals, MyCite and Genamics JournalSeek.

Aims and Scope

The aim of the journal is to disseminate latest scientific ideas and findings in the field of physical sciences among scientists in Malaysia and international regions.

This journal is devoted to the publication of articles dealing with research works in Chemistry, Physics and Engineering. Review articles will also be considered.

Manuscripts must be of scientific value and will be submitted to independent referees for review. Contributions must be written in English and must not have been published elsewhere.

Journal of Physical Science is a multiple award-winning academic journal.

Accolades received by the journal in the recent years include being a recipient of the

Ministry of Education’s CREAM Awards for three consecutive years (2016, 2017 and

2018), and Best Article for Science, Technology and Medicine category in the

Malaysian Scholarly Publishing Council-Ministry of Higher Education (MAPIM-KPT)

Awards 2016.

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Beginning 2016, Journal of Physical Science publishes three issues annually: April, August and November (previously, the journal published biannually).

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Editorial Board

Editor-in-Chief

Prof. Dr. Abdul Latif Ahmad (Universiti Sains Malaysia) Editorial Board

Prof. Dr. Ahmad Fauzi Mohd. Noor (Universiti Sains Malaysia)

Prof. Dr. Atsunori Matsuda (Toyohashi University of Technology, Japan) Prof. Dr. Eiichiro Matsubara (Kyoto University, Japan)

Prof. Dato’ Dr. Hasnah Osman (Universiti Sains Malaysia) Prof. Dr. Hanafi Ismail (Universiti Sains Malaysia)

Prof. Ulung Datuk Dr. Harith Ahmad (University of Malaya, Malaysia) Prof. Dr. Hong-Wei Yen (Tunghai University, Taiwan)

Prof. Mark C. Bagley (University of Sussex, United Kingdom) Prof. Dr. Mohd. Zubir Mat Jafri (Universiti Sains Malaysia) Prof. Nicolas Brosse (University of Lorraine, France)

Prof. Dr. Norli Ismail (Universiti Sains Malaysia)

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1/16/2020 Vol. 29, Supp. 2 (2018) - Journal of Physical Science

jps.usm.my/vol-29-supp-2-2018/ 1/3

Vol. 29, Supp. 2 (2018)

Download EPUB for this issue

Editorial Notes, by Adhi Kusumastuti

1. Thermal Characteristics of Microwave Reactor for Pyrolysis of Food Waste, by Samsudin Anis, Yanuar Adi Kurniawan, Wirawan Sumbodo, Rais Alhakim and Suprayoga Edi Lestari

2. Wear Analysis of Spherical Graphite Cast Iron Using Pin-on Disc Tribotester, by Muchammad, Imam Syafa’at, Fuad Hilmy, Mohammad Tauviqirrahman and Jamari

3. Particle and Crystallite Size Characterisation of Lead Titanate Derived from Solid- state Reaction Method, by Dony Hidayat Al-Janan, Rahmat Doni Widodo,

Rusiyanto and Leonardus Dimas Bima Saputra

4. Study of Thermal Heating of Waste Engine Oil in a Microwave Pyrolysis Reactor, by Moh. Arif Budianto, Samsudin Anis and Wirawan Sumbodo

5. Production of Liquid Oil from Thermolysis of Electrical and Electronic Wastes (E- waste) under Microwave Irradiation, by Samsudin Anis, Suprayoga Edi Lestari, Wahyudi and Karnowo

6. A New Hybrid of Photovoltaic-thermoelectric Generator with Hot Mirror as Spectrum Splitter, by Mustofa, Zuryati Djafar, Syafaruddin and Wahyu Haryadi Piarah

7. Behaviour of Over-reinforced Concrete Beams with Double Helix and Double Square Confinements Related to Ultimate Bending and Shear Strength, by Horng Hean Tee, Kousay Al-Sanjery and Je rey Choong Luin Chiang

8. Seismic Performance of the King Cross Steel Profile in Interior Reinforced

Concrete Beam-column Joint, by Rahmani Kadarningsih, Iman Satyarno, Muslikh

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and Andreas Triwiyono

9. Improving the Masonry Brick Ductility using Mortar Bed Joint from Rubber Tire Crumbs: A Review, by Restu Faizah, Iman Satyarno, Henricus Priyosulistyo and Akhmad Aminullah

10. Shear Strength Behaviour of Steel Truss Embedded in Flexural Plastic Hinge Zone of Reinforced Concrete Beam Subjected to Reversed Cyclic Loading, by Fatmawati Amir, Iman Satyarno and Djoko Sulistyo

11. The Implementation of Fuzzy Expert Systems on Concrete Bridge Investigation with Octave, by Setiono, Wibowo and Sofa Marwoto

12. E ect of Water Content and Water Type on the Physical Properties of Concrete, by Elviana, Ashar Saputra and Djoko Sulistyo

13. Emulsion Liquid Membrane for Textile Dyes Removal: Extraction Process, by Adhi Kusumastuti, Samsudin Anis, Rodia Syamwil and Abdul Latif Ahmad

14. Physical Properties of Edible Sorgum Starch Film Added with Carboxymethyl Cellulose, by Rr. Dewi Artanti Putri, Aji Setiawan and Puji Diah Anggraini

15. Extraction of Phenol from Bio-oil Produced by Pyrolysis of Coconut Shell, by Dewi Selvia Fardyanti, Megawati, Heri Istanto, Muhammad Khusni Anajib, Prayogo and Ummi Habibah

16. Design and Construction of Chem-E-Car SMARTTRONS Powered by

Thermoelectric Generator Utilising Temperature Gradient of Two Reactors, by Dhoni Hartanto, Waliyuddin Sammadikun, Akhmad Sutrisno, Abdul Basit, Ade Surya Siladryanto, Bayu Triwibowo, Haniif Prasetiawan, Widi Astuti, Megawati, Achmad Chafidz, Wara Dyah Pita Rengga, Ratna Dewi Kusumaningtyas and Ianatul Khoiroh

17. Esterification of Non-edible Oil Mixture in Reactive Distillation Column over Solid Acid Catalyst: Experimental and Simulation Study, by Ratna Dewi

Kusumaningtyas, Haniif Prasetiawan, Brylian Rizky Pratama, Dani Prasetya and Anwaruddin Hisyam

18. Emulsion Liquid Membrane for Cadmium Removal: Determination of Liquid Membrane Components, by Adhi Kusumastuti, Nur Qudus, Samsudin Anis and Abdul Latif Ahmad

19. Modelling of Adsorptive-distillation of Ethanol-water Using Natural and Synthetic Zeolites as Adsorbent, by Megawati, Wara Dyah Pita Rengga, Dewi Selvia

Fardhyanti, Afiati Estrina Akhir and Wahyudi Budi Sendiawan

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20. Synthesis of Zinc Oxide Whiskers with Hydrothermal Method for Composite

Absorbent Material of Microwave of ZnOw/MWCNT/Epoxy, by Mohammad Wahyu Ristiawan, Priyono, Agus Subagio, Arifin Muhammad Abdul Kholil and Andhika Ajiesastra

21. Process Evaluation of Biodiesel Production from Nyamplung (Calophyllum

inophyllum) Oil Enhanced by Ionic Liquid + NaOH Catalyst and Microwave Heating System, by Prima Astuti Handayani, Abdullah and Hadiyanto

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Vol. 29, Supp. 2 (2018)

Download EPUB for this issue Editorial Notes, by Adhi Kusumastuti

1. Thermal Characteristics of Microwave Reactor for Pyrolysis of Food Waste, by Samsudin Anis, Yanuar Adi Kurniawan, Wirawan Sumbodo, Rais Alhakim and Suprayoga Edi Lestari

2. Wear Analysis of Spherical Graphite Cast Iron Using Pin-on Disc Tribotester, by Muchammad, Imam Syafa’at, Fuad Hilmy, Mohammad Tauviqirrahman and Jamari

3. Particle and Crystallite Size Characterisation of Lead Titanate Derived from Solid-state Reaction Method, by Dony Hidayat Al-Janan, Rahmat Doni Widodo, Rusiyanto and Leonardus Dimas Bima Saputra

4. Study of Thermal Heating of Waste Engine Oil in a Microwave Pyrolysis Reactor, by Moh. Arif Budianto, Samsudin Anis and Wirawan Sumbodo

5. Production of Liquid Oil from Thermolysis of Electrical and Electronic Wastes (E-waste) under Microwave Irradiation, by Samsudin Anis, Suprayoga Edi Lestari, Wahyudi and Karnowo

6. A New Hybrid of Photovoltaic-thermoelectric Generator with Hot Mirror as Spectrum Splitter, by Mustofa, Zuryati Djafar, Syafaruddin and Wahyu Haryadi Piarah

7. Behaviour of Over-reinforced Concrete Beams with Double Helix and Double Square Confinements Related to Ultimate Bending and Shear Strength, by Horng Hean Tee, Kousay Al-Sanjery and Je rey Choong Luin Chiang

8. Seismic Performance of the King Cross Steel Profile in Interior Reinforced Concrete Beam-column Joint, by Rahmani Kadarningsih, Iman Satyarno, Muslikh and Andreas Triwiyono

9. Improving the Masonry Brick Ductility using Mortar Bed Joint from Rubber Tire Crumbs: A Review, by Restu Faizah, Iman Satyarno, Henricus Priyosulistyo and Akhmad Aminullah

10. Shear Strength Behaviour of Steel Truss Embedded in Flexural Plastic Hinge Zone of Reinforced Concrete Beam Subjected to Reversed Cyclic Loading, by Fatmawati Amir, Iman Satyarno and Djoko Sulistyo

11. The Implementation of Fuzzy Expert Systems on Concrete Bridge Investigation with Octave, by Setiono, Wibowo and Sofa Marwoto

12. E ect of Water Content and Water Type on the Physical Properties of Concrete, by Elviana, Ashar Saputra and Djoko Sulistyo

13. Emulsion Liquid Membrane for Textile Dyes Removal: Extraction Process, by Adhi Kusumastuti,

Samsudin Anis, Rodia Syamwil and Abdul Latif Ahmad

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14. Physical Properties of Edible Sorgum Starch Film Added with Carboxymethyl Cellulose, by Rr. Dewi Artanti Putri, Aji Setiawan and Puji Diah Anggraini

15. Extraction of Phenol from Bio-oil Produced by Pyrolysis of Coconut Shell, by Dewi Selvia Fardyanti, Megawati, Heri Istanto, Muhammad Khusni Anajib, Prayogo and Ummi Habibah

16. Design and Construction of Chem-E-Car SMARTTRONS Powered by Thermoelectric Generator Utilising Temperature Gradient of Two Reactors, by Dhoni Hartanto, Waliyuddin Sammadikun, Akhmad

Sutrisno, Abdul Basit, Ade Surya Siladryanto, Bayu Triwibowo, Haniif Prasetiawan, Widi Astuti,

Megawati, Achmad Chafidz, Wara Dyah Pita Rengga, Ratna Dewi Kusumaningtyas and Ianatul Khoiroh 17. Esterification of Non-edible Oil Mixture in Reactive Distillation Column over Solid Acid Catalyst:

Experimental and Simulation Study, by Ratna Dewi Kusumaningtyas, Haniif Prasetiawan, Brylian Rizky Pratama, Dani Prasetya and Anwaruddin Hisyam

18. Emulsion Liquid Membrane for Cadmium Removal: Determination of Liquid Membrane Components, by Adhi Kusumastuti, Nur Qudus, Samsudin Anis and Abdul Latif Ahmad

19. Modelling of Adsorptive-distillation of Ethanol-water Using Natural and Synthetic Zeolites as Adsorbent, by Megawati, Wara Dyah Pita Rengga, Dewi Selvia Fardhyanti, Afiati Estrina Akhir and Wahyudi Budi Sendiawan

20. Synthesis of Zinc Oxide Whiskers with Hydrothermal Method for Composite Absorbent Material of Microwave of ZnOw/MWCNT/Epoxy, by Mohammad Wahyu Ristiawan, Priyono, Agus Subagio, Arifin Muhammad Abdul Kholil and Andhika Ajiesastra

21. Process Evaluation of Biodiesel Production from Nyamplung (Calophyllum inophyllum) Oil Enhanced by Ionic Liquid + NaOH Catalyst and Microwave Heating System, by Prima Astuti Handayani, Abdullah and Hadiyanto

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