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Structural characterization of hydrothermally synthesized MnO nanorods

(Conference Paper) (Open Access)

, , , , , ,

Department of Physics, Faculty of Science and Mathematics, Diponegoro University, Jl. Prof. Soedarto, Tembalang, Semarang City, 50275, Indonesia

Abstract

We prepared the hydrothermal method to synthesize MnO nanorods with controlled structure. KMnO and HCl with the various molar ratio (1:2,1:6,1:8) reacted at 160°C for three hours to form MnO nanorods. The study found that changing the molar ratio can control the structure and morphology of MnO . The result revealed that MnO formed in nanorod microstructures with different crystallographic structure and phase composition of each molar ratio. The diffraction peaks observed at 2θ values of 28.9°, 37.8°, 40.9°, 49.7° and 60.5° respectively indexed to (110), (101), (200), (411) and (521) plane reflections of a tetragonal phase of β-MnO and α-MnO . The characterization of the

morphology showed that the diameters of nanorod microstructures of MnO ranging from 30 to 145 nm with length ranging from 0.5 to 3 μm. These MnO nanorods product would be potentially used in energy storage devices. © Published under licence by IOP Publishing Ltd.

SciVal Topic Prominence

Topic:

Prominence percentile: 99.994

Indexed keywords

Engineering controlled terms:

Chlorine compounds Microstructure Nanorods Potash

Engineering uncontrolled terms

Controlled structures Crystallographic structure Diffraction peaks Hydrothermal methods Hydrothermally synthesized Structural characterization Structure and morphology Tetragonal phase

Engineering main heading:

Manganese compounds

Funding details

Funding sponsor Funding number Acronym

Ministry of Science Research and Technology

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Journal of Physics: Conference Series

Volume 909, Issue 1, 27 November 2017, Article number 012004

International Conference on Science and Applied Science 2017, ICSAS 2017; Lorin Solo HotelSurakarta; Indonesia; 29 July 2017 through ; Code 132300

2 A'Yuni, D.Q.  Alkian, I. Sya'Diyah, F.K. Kadarisman Darari, A. Gunawan, V. Subagio, A.

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Capacitance | Nanosheets | Asymmetric supercapacitors

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Funding text

We would like thank to Diponegoro University, Ministry of Research Technology and the Higher Education Republic of Indonesia for funding our research from Program KreativitasMahasiswa (PKM). We are also indebted to Mr.

Chasbullah Hindratmo for his valuable assistance in Laboratory Nanotechnology, Diponegoro University.

Wu, J., Huang, H., Yu, L., Hu, J.

(2013) Advances in Materials Physics and Chemistry, 3 (3), p. 201.  . 3

 

Darari, A., Ardiansah, H.R., Arifin, A., Rismaningsih, N., Ningrum, A.N., Subagio, A.

(Open Access) (2016) AIP Conference Proceedings, 1725, art. no. 020012.  . ISBN: 978-073541372-6

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(2006) European Journal of Inorganic Chemistry, (11), pp. 2313-2317.  . doi: 10.1002/ejic.200500983

ISSN: 17426588

Source Type: Conference Proceeding Original language: English

DOI: 10.1088/1742-6596/909/1/012004 Document Type: Conference Paper Volume Editors: Suparmi,Anwar F.

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The Interna onal Conference on Science and Applied Science (ICSAS) 2017 conference is aimed to bring together scholars, leading researchers and experts from diverse backgrounds and applica ons areas in Science. Special emphasis is placed on promo ng interac on between the science theore cal, experimental, and Educa on Sciences, engineering so that a high level exchange in new and emerging areas within Mathema cs, Chemistry, Physics, and Biology, all areas of sciences and applied mathema cs and sciences is achieved.

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3. Prof. Drs. Cari, M.A., M.Sc, Ph.D, Physics department, Graduate Program, Sebelas Maret University

4. Dr. Jaya Murjaya, M.Si, Indonesian Agency for Meteorological, Climatological, and Geophysics

*under confirmation

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Journal of Physics: Conference Series

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International Conference on Science and Applied Science 2017

To cite this article: 2017 J. Phys.: Conf. Ser. 909 011001

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International Conference on Science and Applied Science 2017 IOP Publishing IOP Conf. Series: Journal of Physics: Conf. Series 909 (2017) 011001 doi :10.1088/1742-6596/909/1/011001

International Conference on Science and Applied Science 2017

(ICSAS 2017)

Lorin Solo Hotel Surakarta, Indonesia

29 July 2017

Preface

International Conference on Science and Applied Science 2017 (ICSAS 2017) was held at the Lorin Solo Hotel, Surakarta, Indonesia on 29 July 2017. The ICSAS 2017 conference is aimed to bring together scholars, leading researchers and experts from diverse backgrounds and applications areas in Science. Special emphasis is placed on promoting interaction between the science theoretical, experimental, and education sciences, engineering so that a high level exchange in new and emerging areas within Mathematics, Chemistry, Physics and Biology, all areas of sciences and applied mathematics and sciences is achieved.

In ICSAS 2017, there are eight parallel sessions and four keynote speakers. It is an honour to present this volume of Journal of Physics: Conference Series (JPCS) and we deeply thank the authors for their enthusiastic and high-grade contribution. From the review results, there are 93 papers which will be published in JPCS. We would like to express our sincere gratitude to all in the Programming Committee who have reviewed the papers and developed a very interesting Conference Program, as well as thanking the invited and plenary speakers. Finally, we would like to thank the conference chairman, the members of the steering committee, the organizing committee, the organizing secretariat and the financial support from the Sebelas Maret University that allowed ICSAS 2017 to be a success.

The Editor of the ICSAS 2017 Proceedings:

Prof. Dra. Suparmi, M.A.,Ph.D.

Dr. Fuad Anwar, S.Si., M.Si.

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