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Judul Karya Ilmiah (Artikel) : Mesh-Assisted Laser-Induced Plasma Spectroscopy Using Pulse Carbon Dioxide Laser for Analysis of Powder Material by Confining the Powder in a Hole and Employing a Condensation Technique

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LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU PEER REVIEW KARYA ILMIAH : JURNAL ILMIAH

Judul Karya Ilmiah (Artikel) : Mesh-Assisted Laser-Induced Plasma Spectroscopy Using Pulse Carbon Dioxide Laser for Analysis of Powder Material by Confining the Powder in a Hole and Employing a Condensation Technique

Jumlah Penulis Status Pengusul Identitas Jurnal Ilmiah

Kategori Publikasi Jurnal Ilmiah (beri  pada

kategori yang tepat)

Hasil Penilaian Peer Review :

: 5 orang

: Penulis pertama/ Penulis ke- / Penulis Korespondesi **

: a. Nama Jurnal : Indonesian Journal of Chemistry

b. Nomor ISSN : 1411-9420

c. Volume, Nomor, Bulan, Tahun : Vol. 19, No. 3, November 2019

d. Penerbit : Gadjah Mada University

e. DOI artikel (jika ada) : 10.22146/ijc.34778

f. Alamat web jurnal : https://jurnal.ugm.ac.id/ijc/articl e/view/34778

g. Terindeks di Scimagojr/Scopus atau di….**

: Jurnal Ilmiah Internasional / Internasional Bereputasi **

Jurnal Ilmiah Nasional Terakreditasi

Jurnal Ilmiah Nasional/Nasional Terindeks di DOAJ, CABI, COPERNICUS**

Komponen

Nilai Reviewer

Nilai Rata-rata

Yang Dinilai Reviewer I Reviewer II

a. Kelengkapan unsur isi jurnal (10%) 3,3 3,5 3,4

b. Ruang lingkup dan kedalaman pembahasan 11,2 11,4 11,3

(30%)

c. Kecukupan dan kemutahiran data/informasi dan 11,1 11,4 11,25

metodologi (30%)

d. Kelengkapan unsur dan kualitas penerbit (30%) 11,2 11,2 11,2

Total = (100%) 36,8 37,5 37,15

Nilai untuk Pengusul : (60% x 37,15) = 22,29

Semarang, 24 Februari 2021

Reviewer 1 Reviewer 2

Prof. Dr. Suryono, S.Si., M.Si. Dr. Eng. Eko Hidayanto, S.Si., M.Si.

NIP. 197306301998021001 NIP. 197301031998021001

Bidang ilmu/Unit kerja : Fakultas Sains dan Bidang ilmu/Unit kerja : Fakultas Sains dan

Matematika/Fisika Matematika/Fisika

(2)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU PEER REVIEW KARYA ILMIAH : JURNAL ILMIAH

Judul Jurnal Ilmiah (Artikel) : Mesh-Assisted Laser-Induced Plasma Spectroscopy Using Pulse Carbon Dioxide Laser for Analysis of Powder Material by Confining the Powder in a Hole and Employing a Condensation Technique

Nama/ Jumlah Penulis : 5 Orang

Status Pengusul : Penulis pertama/ Penulis ke / Penulis Korespondesi **

Identitas Jurnal Ilmiah : a. Nama Jurnal : Indonesian Journal of Chemistry

b. Nomor ISSN : 1411-9420

c. Vol, No., Bln Thn : Vol. 19, No. 3, November 2019 d. Penerbit : Gadjah Mada University e. DOI artikel (jika ada) : 10.22146/ijc.34778

f. Alamat web jurnal : https://jurnal.ugm.ac.id/ijc/article/view/34778 Alamat Artikel : https://jurnal.ugm.ac.id/ijc/article/view/34778/22720

g. Terindex : Scopus

Kategori Publikasi Jurnal Ilmiah : (beri pada kategori yang tepat)

Hasil Penilaian Peer Review :

Jurnal Ilmiah Internasional/Internasional Bereputasi Jurnal Ilmiah Nasional Terakreditasi Jurnal Ilmiah Nasional Tidak Terakreditasi

Nilai Maksimal Jurnal Ilmiah

Komponen

Nasional Nasional Nilai Akhir

Internasional Terakreditasi Tidak

Yang

Yang Dinilai

Terakreditasi Diperoleh

a. Kelengkapan unsur isi jurnal (10%) 4 3,3

b. Ruang lingkup dan kedalaman 12 11,2

pembahasan (30%)

c. Kecukupan dan kemutahiran 12 11,1

data/informasi dan metodologi (30%)

d. Kelengkapan unsur dan kualitas 12 11,2

terbitan/jurnal (30%)

Total = (100%) 40 36,8

Nilai Pengusul = 60% x 36,8 = 21,72 Catatan Penilaian artikel oleh Reviewer :

1. Kesesuaian dan kelengkapan unsur isi jurnal:

Jurnal ditulis dengan kesesuaian antar bagian, memiliki gap riset yang jelas, jurnal ditulis dengan lengkap dan menenuhi unsur-unsur penulisan jurnal yang baik.

2. Ruang lingkup dan kedalaman pembahasan:

Ruang lingkup jurnal spesifik, pembahasan telah didukung dengan literatur terkini dan memiliki kedalaman yang baik sesuai dengan hasil yang diperoleh dan focus pada gap riset yang dikemukakan.

3. Kecukupan dan kemutakhiran data/informasi dan metodologi:

Jurnal memiliki kecukupan data yang memadai yang diperoleh dari instrument yang baik, menggunakan metodologi riset yang telah sesuai yang didukung dengan referensi jurnal terbaru, sebaiknya dikurangi referensi jurnal yang lebih dari 5 tahun terakhir, jumlah referensi sebaiknya di tambah.

4. Kelengkapan unsur dan kualitas terbitan:

Jurnal telah memiliki kelengkapan unsur yang baik dan kualitas terbitan yang cukup baik, jurnal yang terindek scopus, memiliki indek similaritas yang kecil.

Semarang, 20 April 2021 Reviewer 1

Prof. Dr. Suryono, S.Si., M.Si.

NIP. 197306301998021001 Unit Kerja : Fisika

Bidang Ilmu: Fakultas Sains dan Matematika

(3)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU PEER REVIEW KARYA ILMIAH : JURNAL ILMIAH

Judul Jurnal Ilmiah (Artikel) : Mesh-Assisted Laser-Induced Plasma Spectroscopy Using Pulse Carbon Dioxide Laser for Analysis of Powder Material by Confining the Powder in a Hole and Employing a Condensation Technique

Nama/ Jumlah Penulis : 5 Orang

Status Pengusul : Penulis pertama/ Penulis ke / Penulis Korespondesi **

Identitas Jurnal Ilmiah : a. Nama Jurnal : Indonesian Journal of Chemistry

b. Nomor ISSN : 1411-9420

c. Vol, No., Bln Thn : Vol. 19, No. 3, November 2019 d. Penerbit : Gadjah Mada University e. DOI artikel (jika ada) : 10.22146/ijc.34778

f. Alamat web jurnal : https://jurnal.ugm.ac.id/ijc/article/view/34778 Alamat Artikel : https://jurnal.ugm.ac.id/ijc/article/view/34778

g. Terindex : Scopus

Kategori Publikasi Jurnal Ilmiah : (beri pada kategori yang tepat)

Hasil Penilaian Peer Review :

Jurnal Ilmiah Internasional/Internasional Bereputasi Jurnal Ilmiah Nasional Terakreditasi Jurnal Ilmiah Nasional Tidak Terakreditasi

Nilai Maksimal Jurnal Ilmiah

Komponen Nasional Nasional Nilai Akhir

Internasional Terakreditasi Tidak Yang

Yang Dinilai Terakreditasi Diperoleh

a. Kelengkapan unsur isi jurnal (10%) 4 3,5

b. Ruang lingkup dan kedalaman 12 11,4

pembahasan (30%)

c. Kecukupan dan kemutahiran 12 11,4

data/informasi dan metodologi (30%)

d. Kelengkapan unsur dan kualitas 12 11,2

terbitan/jurnal (30%)

Total = (100%) 40 37,5

Nilai Pengusul = 60% x 37,5 = 22,50

Catatan Penilaian artikel oleh Reviewer : 1. Kesesuaian dan kelengkapan unsur isi jurnal:

Sangat sesuai dan lengkap mulai dari abstrak, pendahuluan, prosedur eksperimen, hasil dan pembahasan, sampai pada kesimpulan dan dafar pustaka yang digunakan.

2. Ruang lingkup dan kedalaman pembahasan:

Paper ini membahas tentang Analisis pengotor dalam sampel bubuk telah dibuat dengan menggunakan spektroskopi plasma yang diinduksi laser berbantuan logam menggunakan laser CO2 pulsa.

3. Kecukupan dan kemutakhiran data/informasi dan metodologi:

Data-data hasil yang diperoleh dalam penelitian mutakhir dengan didukung metodologi yang tepat.

4. Kelengkapan unsur dan kualitas terbitan:

Karya ini diterbitkan dalam jurnal berkualitas Q3 dengan SJR 0,27 oleh Gadjah Mada University dengan unsur-unsur yang lengkap serta kualitas yang baik.

Semarang, 03 Juli 2021 Reviewer 2

Dr. Eng. Eko Hidayanto, S.Si., M.Si.

NIP. 197301031998021001 Unit Kerja : Fisika

Bidang Ilmu: Fakultas Sains dan Matematika

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Indonesian Journal of Chemistry

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Mesh-assisted laser-induced plasma spectroscopy using pulse carbon dioxide laser for analysis of powder material by confining the powder in a hole and employing a condensation technique

Khumaeni A.

,

Wardaya A.Y.

,

Sugito H.

,

Idris N.

,

Kagawa K.

Save all to author list

a a a b c

Department of Physics, Faculty of Science and Mathematics, Diponegoro University, Jl. Prof. Soedharto, SH., Tembalang, 50275, Semarang, Indonesia

Department of Physics, Faculty of Mathematics and Natural Sciences, Syiah Kuala University, Darussalam, Banda Aceh, 23111, Aceh, Indonesia

Fukui Science Education Academy, Takagi Chuo 2 chome, Fukui, 910-0804, Japan

a

b

c

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Abstract Author keywords Reaxys Chemistry database information SciVal Topics Metrics Funding details

Abstract

Analysis of impurity in powder samples has been made by using metal-assisted laser-induced plasma spectroscopy utilizing a pulsed CO laser. Various powders including food powder, supplement powder, baby powder, and medicine powder were employed as sample materials. Experimentally, the powder sample was tightly put in a hole made on a metal plate and a metal mesh was placed on the powder surface. A pulse CO laser (10.6

μ

m, 1500 mJ) was irradiated on the powder surface passing through the metal mesh. Luminous plasma was induced by mesh just above the mesh when a part of laser energy attacked the mesh. The other part of laser energy impinged the powders and ablated fine particles of powder to the plasma to be atomized and excited. Identification and analysis of elements in powder were successfully conducted. A linear calibration curve of Cu in baby powder has been demonstrated with an intercept zero, certifying that the present technique was a high possibility to be employed for semi-quantitative analysis of elements in powder material. It was proved that by applying the present technique and employing a condensation technique, the detection sensitivity of Cr impurity in the powder sample increased about twenty times compared to the case without condensation. The limit of detection of Cr in rice powder sample was 25 mg/kg. The proposed method was very convenient for

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9/15/21, 3:53 PM Editorial Team

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Home > About the Journal > Editorial Team

Editorial Team

Editor-in-Chief

Nuryono Nuryono, Laboratory of Inorganic Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia

Managing Editor

Dwi Siswanta, Laboratory of Analytical Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia

Editorial Board

Dr. Tran Anh Vy, Department of Chemical and Biochemical Engineering Gachon University, Republic of Korea, Korea, Republic of Dr. Hendrik Oktendy Lintang, Indonesia

Dr. Charles Edwin Raja Gabriel, University of Notre Dame, Notre Dame, Indiana, United States

Assoc. Prof. Dr. Roswanira Abdul Wahab, Department of Chemistry, Universiti Teknologi Malaysia, Malaysia Mudasir Mudasir, Laboratory of Analytical Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia Hideaki Hisamoto, Department of Applied Chemistry, Osaka Prefecture University, Japan

Prof. Joe da Costa, Department of Chemical Engineering, University of Queensland, Australia Dr. Maurizio Barbieri , Department of Earth Science, Sapienza University, Italy

Ming Cai, Tongji University, China

Muhammad Idham Darussalam Mardjan, Laboratory of Organic Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia Pornthep Sompornpisut, Department of Chemistry, Chulalongkorn University, Thailand

Prof. Dr. Taghreed Hashim Al-Noor, Ibn-Al-Haitham Education College /University of Baghdad, Iraq Praveen Kumar Sharma, Department of Chemistry, Lovely Professional University, Punjab, India Akhmad Syou an, Laboratory of Physical Chemistry, Department of Chemistry, Universitas Gadjah Mada Tri Joko Raharjo, Department of Chemistry, Universitas Gadjah Mada, Indonesia

Dr. Saprizal Hadisaputra, Chemistry Education Division, Faculty of Science and Education, University of Mataram, Indonesia Satya Candra Wibawa Sakti, Laboratory of Inorganic Chemistry, Department of Chemistry, Universitas Airlangga, Indonesia Winifred Uduak Anake, Department of Chemistry, College of Science and Technology, Covenant University, Nigeria Aulia Sukma Hutama, Laboratory of Physical Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia Dr. Adhi Dwi Hatmanto, Universitas Gadjah Mada, Indonesia

Administration Support

Djoko Prihandono, Department of Chemistry, Universitas Gadjah Mada, Indonesia

Aulia Sukma Hutama, Laboratory of Physical Chemistry, Department of Chemistry, Universitas Gadjah Mada, Indonesia Aulia Ratri Hapsari, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Indonesia

 

Indonesian Journal of Chemistry (ISSN 1411-9420 / 2460-1578) - Chemistry Department, Universitas Gadjah Mada, Indonesia.

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9/15/21, 3:54 PM Vol 19, No 3 (2019)

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Home > Archives > Vol 19, No 3 (2019)

Vol 19, No 3 (2019)

Accredited by RISTEKDIKTI No : 21/E/KPT/2018 Date : 9 July 2018

Table of Contents

Articles

Thermal and Dynamics Mechanical Analysis of Polypropylene Blown Films with Crude Palm Oil as Plasticizer Siti Hasnah Kamarudin, Emiliana Rose Jusoh, Luqman Chuah Abdullah, Mohd Halim Shah Ismail, Min Min Aung, Chantara Thevy Ratnam

10.22146/ijc.30460 Abstract views : 1981 | views : 2176

545-555

Synthesis and Characterization of Molybdenum Phthalocyanine as Target Material for High Speci c Activity Molybdenum-99 Production

Muhamad Basit Febrian, Duyeh Setiawan, Hilda Hidayati 10.22146/ijc.33218 Abstract views : 2135 | views : 1920

556-564

Three Dimensional Structural Modelling of Lipase Encoding Gene from Soil Bacterium Alcaligenes sp. JG3 Using Automated Protein Homology Analysis

Dilin Rahayu Nataningtyas, Tri Joko Raharjo, Endang Astuti 10.22146/ijc.34152 Abstract views : 1682 | views : 1803

565-574

Synthesis of Mesoporous Carbon from Merbau Wood (Intsia spp.) by Microwave Method as Ni Catalyst Support for α-Cellulose Hydrocracking

Andaru Dena Prasiwi, Wega Trisunaryanti, Triyono Triyono, Iip Izul Falah, Darma Santi, Muhammad Fajar Marsuki

10.22146/ijc.34189 Abstract views : 2362 | views : 2025

575-582

Microwave Assisted Synthesis and Evaluation of Toxicity and Antioxidant Activity of Pyrazoline Derivatives Jasril Jasril, Hilwan Yuda Teruna, Aisyah Aisyah, Nurlaili Nurlaili, Rudi Hendra

10.22146/ijc.34285 Abstract views : 2672 | views : 2118

583-591

Effect of Free Fatty Acid Pretreatment to Yield, Composition and Activation Energy in Chemical Synthesis of Fatty Acid Methyl Ester

Nor Saadah Mohd Alias, Harumi Veny, Fazlena Hamzah, Noorhaliza Aziz

592-598

Home About Login Register Search Current Archives Announcements Statistics Indexing & Abstracting Journal History Contact

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9/15/21, 3:54 PM Vol 19, No 3 (2019)

https://jurnal.ugm.ac.id/ijc/issue/view/3613 2/3

KEYWORDS

FTIRHPLCQSARTiO2

adsorption

antioxidantcatalyst characterization

chitosan

eugenolextractionheavy metalsimmobilization kinetics methylene blue molecular docking photocatalyst silica synthesis transesteri cation zeolite

Indones. J. Chem.

indexed by:

 

 

 

CURRENT ISSUE 10.22146/ijc.34492 Abstract views : 2478 | views : 1943

Estimating Factors Determining Emulsi cation Capability of Surfactant-Like Peptide with Coarse-Grained Molecular Dynamics Simulation

Tegar Wijaya, Rukman Hertadi

10.22146/ijc.34547 Abstract views : 1811 | views : 1839

599-605

Mesh-Assisted Laser-Induced Plasma Spectroscopy Using Pulse Carbon Dioxide Laser for Analysis of Powder Material by Con ning the Powder in a Hole and Employing a Condensation Technique

Ali Khumaeni, Asep Yoyo Wardaya, Heri Sugito, Nasrullah Idris, Kiichiro Kagawa 10.22146/ijc.34778 Abstract views : 1645 | views : 1706

606-614

Effect of Salinity and Oxygen Condition on Phosphate Release from Marine Sediment Measured Using Diffusive Gradient in Thin Film (DGT) Technique

Askal Maimulyanti, Budiawan Budiawan, Asep Saefumillah, Heny Suseno 10.22146/ijc.35233 Abstract views : 1786 | views : 1662

615-625

Congo Red Azo Dye Removal and Study of Its Kinetics by Aloe Vera Mediated Copper Oxide Nanoparticles Madiha Batool, Muhammad Zahid Qureshi, Farwa Hashmi, Nida Mehboob, Abdul Salam Shah 10.22146/ijc.35626 Abstract views : 2619 | views : 2014

626-637

A Simple Pre-concentration Method for the Determination of Nickel(II) in Urine Samples Using UV-Vis Spectrophotometry and Flame Atomic Absorption Spectrometry Techniques

Ahmed Fadhil Khudhair, Mouyed Khudhair Hassan, Hasan F. Alesary, Ahmed S. Abbas 10.22146/ijc.35681 Abstract views : 3383 | views : 2921

638-649

P84/Zeolite-Carbon Composite Mixed Matrix Membrane for CO2/CH4 Separation

Triyanda Gunawan, Retno Puji Rahayu, Rika Wijiyanti, Wan Norharyati Wan Salleh, Nurul Widiastuti 10.22146/ijc.35727 Abstract views : 2358 | views : 2308

650-659

Preparation and Characterization of a Novel Cocrystal of Atorvastatin Calcium with Succinic Acid Coformer Yudi Wicaksono, Dwi Setyawan, Siswandono Siswandono, Tri Agus Siswoyo

10.22146/ijc.35801 Abstract views : 3455 | views : 2914

660-667

Fast Analytical Method for Authentication of Chili Powder from Synthetic Dyes Using UV-Vis Spectroscopy in Combination with Chemometrics

Eti Rohaeti, Khoirotul Muzayanah, Dewi Anggraeni Septaningsih, Mohamad Ra 10.22146/ijc.36297 Abstract views : 3363 | views : 2324

668-674

Synthesis, Characterization and Catalytic Activity of NiO-CoO-MgO Nano-Composite Catalyst Salih Hadi Kadhim, Tariq Hussein Mgheer, Hussein Idrees Ismael, Khudheyer Jawad Kadem, Ahmed Saadon Abbas, Abbas Jasim Atiyah, Iman Jassim Mohamad

10.22146/ijc.38119 Abstract views : 1632 | views : 1622

675-683

Alginate-Graphene Oxide Biocomposite Sorbent for Rapid and Selective Extraction of Non-Steroidal Anti- In ammatory Drugs Using Micro-Solid Phase Extraction

Mohammad Salim Tabish, Nor Suhaila Mohamad Hanapi, Wan Nazihah Wan Ibrahim, Nor’ashikin Saim, Noorfatimah Yahaya

10.22146/ijc.38168 Abstract views : 2797 | views : 2454

684-695

Combustion Synthesis Ironmaking: Investigation on Required Carbon Amount in Raw Material from the Viewpoint of Adiabatic Flame Temperature Calculation

Keisuke Abe, Ade Kurniawan, Masafumi Sanada, Takahiro Nomura, Tomohiro Akiyama 10.22146/ijc.38359 Abstract views : 2521 | views : 1577

696-702

Valuable Chemicals Derived from Pyrolysis Liquid Products of Spirulina platensis Residue Siti Jamilatun, Budhijanto Budhijanto, Rochmadi Rochmadi, Avido Yuliestyan, Arief Budiman 10.22146/ijc.38532 Abstract views : 2022 | views : 2044

703-711

Pyrolusite Bioleaching by an Indigenous Acidithiobacillus sp KL3 Isolated from an Indonesian Sulfurous River Sediment

Endah Retnaningrum, Wahyu Wilopo

10.22146/ijc.38898 Abstract views : 1772 | views : 1657

712-719

Development and Validation of a Four-Tier Diagnostic Instrument for Chemical Kinetics (FTDICK) Habiddin Habiddin, Elizabeth Mary Page

10 22146/ij 39218 Ab i 4937 | i 2896 | i 1305

720-736

(9)

9/15/21, 3:54 PM Vol 19, No 3 (2019)

https://jurnal.ugm.ac.id/ijc/issue/view/3613 3/3

10.22146/ijc.39218 Abstract views : 4937 | views : 2896 | views : 1305

Effect of Key Parameters on Jacalin Extraction from Aqueous Phase into Anionic Reverse Micelles Sharifah Fathiyah Sy Mohamad, Farhan Mohd Said, Mimi Sakinah Abdul Munaim, Shahril Mohamad 10.22146/ijc.39705 Abstract views : 1915 | views : 1684

737-746

Corrosion Inhibition of Carbon Steel Using Palm Oil Leaves Extract Nor Insyirah Hairul Salleh, Arman Abdullah

10.22146/ijc.39707 Abstract views : 2927 | views : 2431

747-752

Effect of Torrefaction Temperature, Residence Time and Particle Size on the Properties of Torre ed Food Waste

Ruwaida Abdul Rasid, Thye Mei Chin, Mazni Ismail, Nahsya Nur Udzaifah Abdul Rahman 10.22146/ijc.39718 Abstract views : 1689 | views : 1730

753-760

Synthesis and Characterization of Cu-Doped Zirconium Titanate as A Potential Visible-Light Responsive Photocatalyst

Katarina Rachma Andita, Rian Kurniawan, Akhmad Syou an 10.22146/ijc.39778 Abstract views : 2257 | views : 1812

761-766

Effect of Immobilization Method on the Growth of Chlorella vulgaris and Fatty Acid Pro le for Biodiesel Production

Nur Hanani Rushan, Nur Hidayah Mat Yasin, Noor Raihana Abu Sepian, Farhan Mohd Said, Nura fah Izzati Shafei

10.22146/ijc.39800 Abstract views : 2163 | views : 1913

767-776

Docking of New Designed Compounds Derived from 1,6-Dihydro-1,3,5-triazine-2,4-diamine Toward Quadruple Mutant Plasmodium Dihydrofolate Reductase

Imam Siswanto, Harno Dwi Pranowo, Mudasir Mudasir 10.22146/ijc.39943 Abstract views : 1916 | views : 1914

777-785

Inhibitive Determination of Hg(II) in Aqueous Solution Using Urease Amperometric Biosensor Dhony Hermanto, Bambang Kuswandi, Dwi Siswanta, Mudasir Mudasir

10.22146/ijc.40617 Abstract views : 1753 | views : 2008

786-795

Extraction of Phytosterol Concentration in Different Legume Pods by Using Microwave-Assisted Hydrodistillation

Noormazlinah Noormazlinah, Norlaili Hashim, Abdurahman Hamid Nour, Mimi Sakinah Abdul Munaim, Maria Pilar Almajano, Nurul Bahirah

10.22146/ijc.40865 Abstract views : 2477 | views : 2183

796-803

The Potentials of an Integrated Ultrasonic Membrane Anaerobic System (IUMAS) in Treating Sugar Cane Wastewater

Abdurahman Hamid Nour, Yasmeen Ha z Zaki, Hybat Salih Mohamed, Hesham Hussein Rassem 10.22146/ijc.40866 Abstract views : 1828 | views : 1666

804-810

Statistical Modelling of Ultrasonic-Aided Extraction of Elaeis guineensis Leaves for Better-Quality Yield and Total Phenolic Content

Nissha Bharrathi Romes, Mariani Abdul Hamid, Siti Ernieyanti Hashim, Roswanira Abdul Wahab 10.22146/ijc.41603 Abstract views : 2184 | views : 1698

811-826

 

Indonesian Journal of Chemistry (ISSN 1411-9420 / 2460-1578) - Chemistry Department, Universitas Gadjah Mada, Indonesia.

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9/15/21, 3:57 PM Thermal and Dynamics Mechanical Analysis of Polypropylene Blown Films with Crude Palm Oil as Plasticizer | Kamarudin | I…

https://jurnal.ugm.ac.id/ijc/article/view/30460 1/3

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ABOUT THE AUTHORS Siti Hasnah Kamarudin Institute of Tropical Forestry and Forest Products, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

Malaysia

Institute of Tropical Forestry and Forest Products Emiliana Rose Jusoh

* Corresponding Author Department of Chemical and Environmental Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

Malaysia

Department of Chemical and Environmental Engineering Luqman Chuah Abdullah Department of Chemical and Environmental Engineering, Home About Login Register Search Current Archives Announcements Statistics Indexing & Abstracting Journal History Contact Home > Vol 19, No 3 (2019) > Kamarudin

Thermal and Dynamics Mechanical Analysis of Polypropylene Blown Films with Crude Palm Oil as Plasticizer

https://doi.org/10.22146/ijc.30460

Siti Hasnah Kamarudin(1), Emiliana Rose Jusoh(2*), Luqman Chuah Abdullah(3), Mohd Halim Shah Ismail(4), Min Min Aung(5), Chantara Thevy Ratnam(6)

(1) Institute of Tropical Forestry and Forest Products, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

(2) Department of Chemical and Environmental Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

(3) Department of Chemical and Environmental Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

(4) Department of Chemical and Environmental Engineering, Faculty of Engineering, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

(5) Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia (6) Radiation Processing Technology Division, Malaysian Nuclear Agency, 43000, Bangi, Malaysia

(*) Corresponding Author

Abstract

This research aims to investigate the effect of crude palm oil (CPO) as a plasticizer in polypropylene blown lm on thermal and dynamic mechanical properties. Polypropylene (PP) was blended with 1, 3, and 5% of CPO using a twin screw extruder. The extruded samples were blown using the blown thin lm technique. The samples were analyzed using dynamic mechanical analysis (DMA), differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). From the dynamic mechanical analysis, the storage modulus and loss modulus for PP presented decreasing pattern about 3–5% due to the action of CPO as plasticizer which introduced free volume and enabled the polyole ns chains to deform more easily. The glass transition temperatures (Tg) of PP were found being shifted to lower temperature from 10 to 1 °C with the increasing CPO content. The fraction of crystallization was determined using DSC. The thermogravimetric analysis (TGA) results showed that the incorporation of CPO as plasticizer showed a small increased effect in the thermal stability for PP. These ndings have contributed new knowledge to the additives area and give important implications for designing and manufacturing polymer packaging materials.

Keywords

crude palm oil; polypropylene; plasticizer; thermal properties

Full Text:

References

[1] Karian, H.G., 2003, Handbook of Polypropylene and Polypropylene Composites, 2nd ed., Marcel Dekker, Canada, 57–68.

[2] Ho, C.H., Wang, C.H., Lin, C.I., and Lee, Y.D., 2008, Synthesis and characterization of TPO-PLA copolymer and its behavior as compatibilizer for PLA/TPO blends, Polymer, 49 (18), 3902–3910.

[3] Liao, H.T., and Wu, C.S., 2009, Preparation and characterization of ternary blends composed of polylactide, poly(ɛ-craptolactone) and starch, Mater. Sci. Eng., A, 515 (1-2), 207–214.

[4] Marcilla, A., and Beltran, M., 2004, “Mechanisms of Plasticizers Action” in Handbook of Plasticizers, Eds. Wypych, G., ChemTec Publishing, Toronto, Canada, 107–120.

[5] Wilson A 1995Plasticizers Principles and Practice 1sted The Institute of Materials London 45–50

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9/15/21, 4:00 PM Development and Validation of a Four-Tier Diagnostic Instrument for Chemical Kinetics (FTDICK) | Habiddin | Indonesian Jou…

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ABOUT THE AUTHORS Habiddin Habiddin

* Corresponding Author orcid

https://scholar.google.co.id/cita user=lbc_OagAAAAJ&hl=en

Department of Chemistry, Faculty of Mathematics and Science, Universitas Negeri Malang, Jl. Semarang No. 5, Malang 65145, East Java, Indonesia

Indonesia

Elizabeth Mary Page Department of Chemistry, University of Reading, Whiteknights Park, Reading RG6 6AD, United Kingdom United Kingdom

ARTICLE TOOLS Print this article Home About Login Register Search Current Archives Announcements Statistics Indexing & Abstracting Journal History Contact Home > Vol 19, No 3 (2019) > Habiddin

Development and Validation of a Four-Tier Diagnostic Instrument for Chemical Kinetics (FTDICK)

https://doi.org/10.22146/ijc.39218 Habiddin Habiddin(1*), Elizabeth Mary Page(2)

(1) Department of Chemistry, Faculty of Mathematics and Science, Universitas Negeri Malang, Jl. Semarang No. 5, Malang 65145, East Java, Indonesia

(2) Department of Chemistry, University of Reading, Whiteknights Park, Reading RG6 6AD, United Kingdom (*) Corresponding Author

Abstract

The present study outlines the development and validation of a four-tier diagnostic instrument to explore rst year undergraduate students’

understanding of chemical kinetics (FTDICK). The four-tier instrument is a recent format and has been applied only sparsely in a limited number of subject areas, not including chemical kinetics. This study con rms the importance of a four-tier approach in fully investigating students’ poor knowledge and understanding. The FTDICK described here involves 20 questions with a con dence level linked to both the question tier and the reason tier. The development of the instrument followed the procedure used for the two-tier instrument developed by Treagust and involves (1) testing & interviewing, (2) identifying & collecting students’ unscienti c ideas, (3) developing the prototype FTDICK, (4) validating the prototype FTDICK, and (5) developing the nal FTDICK. The initial steps revealed a number of areas of misconceptions to be explored in the nal instrument. The instrument has been developed and the prototype tested using international cohorts of students from the University of Reading, UK and two Indonesian Universities. Comprehensive item analysis on the results showed the instrument to be valid and reliable and suitable for identifying students’ understanding of chemical kinetics. This study con rms the importance of a four-tier approach for investigating students’ prior knowledge and understanding.

Keywords

validation; four-tier instrument; Four-Tier Diagnostic Instrument for Chemical Kinetics (FTDICK)

Full Text:

References

[1] Hailikari, T.K., and Nevgi, A., 2010, How to diagnose at-risk students in chemistry: The case of prior knowledge assessment, Int. J. Sci.

Educ., 32, 2079–2095.

[2] Seery, M.K., 2009, The role of prior knowledge and student aptitude in undergraduate performance in chemistry: a correlation-prediction study, Chem. Educ. Res. Pract., 10 (3), 227–232.

[3] Bennett, J.M., and Sozbilir, M., 2007, A study of Turkish chemistry undergraduates’ understandings of entropy, J. Chem. Educ., 84 (7), 1204–1208.

[4] Caleon, I., and Subramaniam, R., 2010, Development and application of a three-tier diagnostic test to assess secondary students’

understanding of waves, Int. J. Sci. Educ., 32 (7), 939–961.

[5] Carson, E.M., and Watson, J.R., 2002, Undergraduate students’ understanding of entropy and gibbs free energy, Univ. Chem. Educ., 6, 4–

12.

[6] Treagust, D.F., 2002, “Teaching and Learning About Chemical Compounds” in Chemical Education: Towards Research-based Practice, Eds., Gilbert, J.K., De Jong, O., Justi, R., Treagust, D.F., and Van Driel, J.H., Springer, Netherlands, 187–188.

[7] Taştan, Ö., Yalçinkaya, E., and Boz, Y., 2010, Pre-service chemistry teachers’ idea about reaction mechanism, J. Turk. Sci. Educ., 7 (1), 47–

60.

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