Meinaa Jaber Dalal and Athraa Hameed Mekky
Supplementary Data
This supplementary data is a part of a paper entitled “Synthesis, Characterization and Antioxidant Evaluation of Some Tetrazole Derivatives”.
Fig S1. FTIR spectrum of compound S1
Fig S2. 1H-NMR spectrum of compound S1
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
2
Fig S3. 13C-NMR spectrum of compound S1
Fig S4. FTIR spectrum of compound S2
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S5. 1H-NMR spectrum of compound S2
Fig S6. 13C-NMR spectrum of compound S2
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
4
Fig S7. FTIR spectrum of compound S3
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 9.5 10.5 11.5
12.5 f1 (ppm)
-100 0 100 200 300 400 500 600 700 800 900 1000 1100 1200
1.171.041.092.112.071.10
1.09
1.00 2.50
3.35
7.167.517.708.108.128.158.178.69
10.23
12.00
Fig S8. 1H-NMR spectrum of compound S3
Meinaa Jaber Dalal and Athraa Hameed Mekky
0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 80
-5E+05 0 5E+05 1E+06 2E+06 2E+06 2E+06 3E+06 4E+06 4E+06 4E+06 5E+06 6E+06 6E+06 6E+06 7E+06 8E+06
39.3339.5439.7539.9640.1740.3840.59
121.35124.52128.41129.72129.97131.80134.57136.41139.41142.89143.94
162.16
Fig S9. 13C-NMR spectrum of compound S3
Fig S10. FTIR spectrum of compound S4
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
6
Fig S11. 1H-NMR spectrum of compound S4
Fig S12. FTIR spectrum of compound S5
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S13. FTIR spectrum of compound S6
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 9.5
0.0 f1 (ppm)
-20 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320
3.00
2.071.83
5.16 1.161.181.19
2.50
3.32
4.114.134.144.154.29
7.657.667.677.677.677.687.687.687.69
Fig S14. 1H-NMR spectrum of compound S6
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
8
Fig S15. 13C-NMR spectrum of compound S6
Fig S16. FTIR spectrum of compound S7
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S17. 1H-NNMR spectrum of compound S7
Fig S18. 13C-NMR spectrum of compound S7
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
10
Fig S19. FTIR spectrum of compound S8
0 .0 0 .5 1 .0 1 .5 2 .0 2 .5 3 .0 3 .5 4 .0 4 .5 5 .0 5 .5 6 .0 6 .5 7 .0 7 .5 8 .0 8 .5 9.0 9 .5 1 0 .0 1 0 .5 1 1 .0 1 1 .5 1 2 .0 1 2 .5 1 3 .0 1 3 .5
4 .0 f1 (p p m )
-1 0 0 1 0 2 0 3 0 4 0 5 0 6 0 7 0 8 0 9 0 1 0 0
1.06
2.09
3.830.951.991.090.961.24
1.07 2.50 dmso
3.35 HDO
4.30
4.73
7.497.507.517.527.667.677.697.707.727.738.03
11.84
Fig S20a. 1H-NMR spectrum of compound S8 with solvent impure DMSO-d6
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S20b. 1H-NMR spectrum of compound S8 without solvent
Fig S21. 13C-NMR spectrum of compound C8
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
12
Fig S22. FTIR spectrum of compound S9
0.5 1.5 2.5 3.5 4.5 5.5 6.5 7.0 7.5 8.5 9.5 10.5 11.5
12.5 f1 (ppm)
0 50 100 150 200 250 300 350 400 450 500
0.952.00
1.010.961.065.041.03
0.96 2.50
4.284.64
7.137.457.487.698.22
11.76
Fig 23. 1H-NMR spectrum of compound C9 with solvent in impure DMSO-d6
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S24. 13C-NMR spectrum of compound S9
Fig S25. FTIR spectrum of compound S10
Indones. J. Chem., 2022, 22 (6), 1596 - 1604
Suppl.
Meinaa Jaber Dalal and Athraa Hameed Mekky
14
Fig S26a. 1H-NMR spectrum of compound S10 with impure solvent DMSO-d6
Fig S26b. 1H-NMR spectrum of compound without solvent S10
Meinaa Jaber Dalal and Athraa Hameed Mekky
Fig S27. 13C-NMR spectrum of compound S10
