KARYA ILMIAH : JURNAL ILMIAH

(1)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU

PEER REVIEW

KARYA ILMIAH : JURNAL ILMIAH

Judul Jurnal Ilmiah (Artikel) : Shock wave plasma generation in low pressure ambient gas from powder sample using subtarget supported micro mesh as a sample holder and its potential applications for sensitive analysis of powder samples

Nama/ Jumlah Penulis : 19 Orang

Status Pengusul : Penulis pertama/ Penulis ke 6 / Penulis Korespondesi **

Identitas Jurnal Ilmiah : a. Nama Jurnal :

Microchemical Journal

b. Nomor ISSN : 0026-265X

c. Vol, No., Bln Thn : Vol. 142, No.-, November 2018

d. Penerbit : Elsevier

e. DOI artikel (jika ada) : 10.1016/j.microc.2018.06.022

f. Alamat web jurnal : https://www.elsevier.com/locate/microc

Alamat Artikel : https://www.sciencedirect.com/science/article/abs/pii/S0 026265X18305605

g. Terindex : Scopus

Kategori Publikasi Jurnal Ilmiah :

^√

Jurnal Ilmiah Internasional/Internasional Bereputasi (beri pada kategori yang tepat) Jurnal Ilmiah Nasional Terakreditasi

Jurnal Ilmiah Nasional Tidak Terakreditasi

Hasil Penilaian

Peer Review

:

Komponen Yang Dinilai

Nilai Maksimal Jurnal Ilmiah

Nilai Akhir Yang Diperoleh Internasional Nasional

Terakreditasi Nasional Tidak Terakreditasi

a. Kelengkapan unsur isi jurnal (10%) 4 3,5

b. Ruang lingkup dan kedalaman pembahasan (30%)

12 11,6

c. Kecukupan dan kemutahiran

data/informasi dan metodologi (30%)

12 11,7

d. Kelengkapan unsur dan kualitas terbitan/jurnal (30%)

12 11,7

Total = (100%) 40 38,5

Nilai Pengusul = 20% x 38,5/18 =0,43 Catatan Penilaian artikel oleh Reviewer :

1. Kesesuaian dan kelengkapan unsur isi jurnal:

Subtansi kesesuaian antar bagian, gap riset yang jelas, jurnal ditulis dengan lengkap dan unsur-unsur penulisan jurnal terpenuhi dengan baik.

2. Ruang lingkup dan kedalaman pembahasan:

Ruang lingkup sesuai, pembahasan didukung dengan literatur terkini dan memiliki kedalaman yang baik sesuai dengan hasil yang diperoleh dan dikdukun dengan literatur.

3. Kecukupan dan kemutakhiran data/informasi dan metodologi:

Jurnal memiliki kecukupan data yang layak, menggunakan metodologi riset yang baik 4. Kelengkapan unsur dan kualitas terbitan:

Jurnal telah memiliki kelengkapan unsur yang baik dan kualitas terbitan yang cukup baik, jurnal yang terindek scopus, memiliki indek similaritas yang kecil.

Semarang, 20 April 2021 Reviewer 1

Prof. Dr. Suryono, S.Si., M.Si.

NIP. 197306301998021001 Unit Kerja : Fisika

Bidang Ilmu: Fakultas Sains dan Matematika

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(2)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU

PEER REVIEW

KARYA ILMIAH : JURNAL ILMIAH

Judul Jurnal Ilmiah (Artikel) : Shock wave plasma generation in low pressure ambient gas from powder sample using subtarget supported micro mesh as a sample holder and its potential applications for sensitive analysis of powder samples

Nama/ Jumlah Penulis : 19 Orang

Status Pengusul : Penulis pertama/ Penulis ke 6 / Penulis Korespondesi **

Identitas Jurnal Ilmiah : a. Nama Jurnal :

Microchemical Journal

b. Nomor ISSN : 0026-265X

c. Vol, No., Bln Thn : Vol. 142, No.-, November 2018

d. Penerbit : Elsevier

e. DOI artikel (jika ada) : 10.1016/j.microc.2018.06.022

f. Alamat web jurnal : https://www.elsevier.com/locate/microc

Alamat Artikel : https://www.sciencedirect.com/science/article/abs/pii/S0 026265X18305605

g. Terindex : Scopus

Kategori Publikasi Jurnal Ilmiah :

^√

Jurnal Ilmiah Internasional/Internasional Bereputasi (beri pada kategori yang tepat) Jurnal Ilmiah Nasional Terakreditasi

Jurnal Ilmiah Nasional Tidak Terakreditasi

Hasil Penilaian

Peer Review

:

Komponen Yang Dinilai

Nilai Maksimal Jurnal Ilmiah

Nilai Akhir Yang Diperoleh Internasional Nasional

Terakreditasi Nasional Tidak Terakreditasi

a. Kelengkapan unsur isi jurnal (10%) 4 3,5

b. Ruang lingkup dan kedalaman pembahasan (30%)

12 11,7

c. Kecukupan dan kemutahiran

data/informasi dan metodologi (30%)

12 11,5

d. Kelengkapan unsur dan kualitas terbitan/jurnal (30%)

12 11,8

Total = (100%) 40 38,5

Nilai Pengusul = 20% x ( 38,5/18 ) = 0,43 Catatan Penilaian artikel oleh Reviewer :

1. Kesesuaian dan kelengkapan unsur isi jurnal:

Isi jurnal sangat sesuai dan lengkap dari komponen-komponen yang ada abstrak, pendahuluan, prosedur eksperimen, hasil dan pembahasan, lalu kesimpulan dan daftar pustaka yang digunakan.

2. Ruang lingkup dan kedalaman pembahasan:

Paper ini membahas tentang studi eksperimental pada analisis spektrokimia sampel bubuk menggunakan pemegang sampel subtarget yang didukung micro mesh (SSMM) dalam gas ambien bertekanan rendah.

3. Kecukupan dan kemutakhiran data/informasi dan metodologi:

Data-data/informasi serta metodologi yang digunakan sangat mutakhir.

4. Kelengkapan unsur dan kualitas terbitan:

Karya ini diterbitkan dalam jurnal berkualitas Q2 dengan SJR 0,75 oleh Elsevier Inc. dengan unsur-unsur yang lengkap serta kualitas yang sangat baik.

Semarang, 04 Juli 2021 Reviewer 2

Dr. Eng. Eko Hidayanto, S.Si., M.Si.

NIP. 197301031998021001 Unit Kerja : Fisika

Bidang Ilmu: Fakultas Sains dan Matematika

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(3)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU PEER REVIEW KARYA ILMIAH : JURNAL ILMIAH

Hasil Penilaian Peer Review :

Komponen Yang Dinilai

Nilai Reviewer

Nilai Rata-rata Reviewer I Reviewer II

a. Kelengkapan unsur isi jurnal (10%) ^3,5 ^3,5 3,5

b. Ruang lingkup dan kedalaman pembahasan (30%)

11,6 11,7 11,65

c. Kecukupan dan kemutahiran data/informasi dan metodologi (30%)

11,7 11,5 11,6

d. Kelengkapan unsur dan kualitas penerbit (30%) ^11,7 ^11,8 11,75

Total = (100%) 38,5

Nilai untuk Pengusul : 20% x (38,5/18) = 0,43

Reviewer 1

Prof. Dr. Suryono, S.Si., M.Si.

NIP. 197306301998021001

Bidang ilmu/Unit kerja : Fakultas Sains dan Matematika/Fisika

Semarang, 24 Februari 2021 Reviewer 2

Dr. Eng. Eko Hidayanto, S.Si., M.Si.

NIP. 197301031998021001

Bidang ilmu/Unit kerja : Fakultas Sains dan Matematika/Fisika

Judul Karya Ilmiah (Artikel) : Shock wave plasma generation in low pressure ambient gas from powder sample using subtarget supported micro mesh as a sample holder and its potential applications for sensitive analysis of powder samples

Jumlah Penulis : 19 Orang

Status Pengusul : Penulis pertama/ Penulis ke 6/ Penulis Korespondesi **

Identitas Jurnal Ilmiah : a. Nama Jurnal : Microchemical Journal

b. Nomor ISSN : 0026-265X

c. Volume, Nomor, Bulan, Tahun : Vol. 142, No.-, November 2018

d. Penerbit : Elsevier

e. DOI artikel (jika ada) : 10.1016/j.microc.2018.06.022 f. Alamat web jurnal : https://www.elsevier.com/locate/mi

croc g. Terindeks di Scimagojr/Scopus atau

di….**

Kategori Publikasi Jurnal Ilmiah (beri pada kategori yang tepat)

: Jurnal Ilmiah Internasional / Internasional Bereputasi **

Jurnal Ilmiah Nasional Terakreditasi

Jurnal Ilmiah Nasional/Nasional Terindeks di DOAJ, CABI, COPERNICUS**

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Microchemical Journal • Open Access • Volume , Pages - • November

Shock wave plasma generation in low pressure ambient gas from powder sample using subtarget supported micro mesh as a sample holder and its potential applications for sensitive analysis of powder samples

Iqbal J., Pardede M., Jobiliong E., Hedwig R., Ramli M., Khumaeni A., Budi W.S., Idris N., Abdulmadjid S.N., Lahna K., Marpaung M.A., Karnadi I.

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a b b c d e e d

d d f g

Department of Physics, University of Azad, Jammu & Kashmir, Muzaﬀarabad, Pakistan

University of Pelita Harapan, 1100 M.H. Thamrin Boulevard, Lippo Village, Tangerang, 15811, Indonesia Department of Computer Engineering, Bina Nusantara University, 9 K.H. Syahdan, Jakarta, 14810, Indonesia Faculty of Mathematics and Natural Sciences, Syiah Kuala University, Darussalam, Banda Aceh, 23111, Indonesia View additional aﬃliations

a b c d

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Abstract Author keywords SciVal Topics Metrics Funding details

Abstract

We present in this report the results of experimental study on the spectrochemical analysis of powder samples using subtarget supported micro mesh (SSMM) sample holder in low pressure ambient gases.

The study is substantiated by establishing the analyte excitation mechanism with the evidence of shock wave plasma generation and the high temperature induced subsequently required for the thermal excitation and emission of the ablated atoms. The application of SSMM sample holder using Cu subtarget and stainless steel micro mesh to a number of powder samples in low pressure ambient gases are shown to produce generally sharp emission lines with low background, without suffering from intensity reduction and matrix effect commonly found in the use of pelletized powder samples.

The same excellent spectral quality is demonstrated by its application to the analysis of rice samples which is the major staple diets in a large number of countries. In particular the analysis of Zn in rice is shown to exhibit a linear calibration line with extrapolated zero intercept and a detection limit of <0.87 μg/g which is promising for quantitative analysis. © 2018

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Author keywords

LIBS; Low pressure; Shock wave plasma; Spectrochemical analysis of powder samples; Subtarget supported micro mesh sample holder; Zn in rice

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(11)

1 of 1 Abstract Author keywords SciVal Topics Metrics Funding details

Kurniawan, K.H., Pardede, M., Hedwig, R., Lie, Z.S., Lie, T.J., Kurniawan, D.P., Ramli, M., (...), Tjia, M.O.

(2007) Analytical Chemistry, 79 (7), pp. 2703-2707. . doi: 10.1021/ac061713o

Khumaeni, A., Ramli, M., Deguchi, Y., Lee, Y., Idris, N., Kurniawan, K.H., Lie, T.J.J., (...), Kagawa, K.

Khumaeni, A., Lie, Z.S., Niki, H., Kurniawan, K.H., Tjoeng, E., Lee, Y.I., Kurihara, K., (...), Kagawa, K.

.

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Sedov, L.I.

Similarity and Dimensional Methods in Mechanics

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9/15/21, 4:09 PM Editorial Board - Microchemical Journal - Journal - Elsevier

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University of Valencia, Valencia, Spain

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Fabiana Arduini

University of Rome Tor Vergata Department of Chemical Sciences and Technologies, Roma, Italy

Xiandeng (Dan) Hou

Sichuan University Analytical and Testing Center, Chengdu, China

Yong-Ill Lee

Changwon National University, Changwon, South Korea

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National University of Rosario, Rosario, Argentina

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Gangfeng Ouyang, PhD

Sun Yat-sen University School of Chemistry, Guangzhou, China View more

Justyna Płotka-Wasylka

Gdańsk University of Technology, Gdansk, Poland

Rawi Ramautar, PhD

Leiden University, Leiden, Netherlands View more

Paloma Yáñez-Sedeño Orive, PhD

Complutense University of Madrid Faculty of Chemical Sciences, Madrid, Spain

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9/15/21, 4:20 PM Microchemical Journal | Vol 142, Pages 1-412 (November 2018) | ScienceDirect.com by Elsevier

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Larrea divaricata volatilome and antimicrobial activity against Monilinia fructicola

Joana Boiteux, Carolina Monardez, María de los Ángeles Fernández, Magdalena Espino, ... María Fernanda Silva Pages 1-8

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Deﬁning a standard method to measure the total and bioavailable concentration of ﬂuorine in New Zealand soils

Thangavelautham Geretharan, Paramsothy Jeyakumar, Michael Bretherton, Christopher W.N. Anderson Pages 94-101

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Eco-friendly environmental trace analysis of thorium using a new supramolecular solvent-based liquid-liquid microextraction combined with spectrophotometry

Ayman A. Gouda, Manal S. Elmasry, Hisham Hashem, Heba M. EL-Sayed Pages 102-107

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Shock wave plasma generation in low pressure ambient gas from powder sample using subtarget supported micro mesh as a sample holder and its potential applications for sensitive analysis of powder samples Javed Iqbal, Marincan Pardede, Eric Jobiliong, Rinda Hedwig, ... May On Tjia

Pages 108-116 Abstract

Abstract

The concentration of fluorine (F) in New Zealand pastoral soils is increasing as a consequence of Phosphorus (P) fertiliser application, and there is concern over the long-term impact of this F on animal and soil microbiological health. Ongoing soil F monitoring to underpin comprehensive soil F management practices requires an accurate and simple test to quantify both the total and bioavailable concentration of F in soil. In this study, soils were collected from various locations across New Zealand, representing different soil orders and land uses. The total soil F concentration was measured using an ion specific electrode following extraction with four different concentrations of NaOH (4 mol L , 8 mol L , 12 mol L and 16 mol L ), or fusion with NaOH (the conventional method used to analyse total soil F). We concluded that NaOH extraction gave an acceptable level of accuracy for organic matter and volcanic parent material derived soils Agreement was however less strong for recent and pallic soils The extraction method was subsequently

−1

−1 −1 −1

Abstract

A novel green supramolecular solvent-based liquid-liquid microextraction (SsLLME) method was developed and validated for preconcentration of thorium(IV) in various environmental samples. The presented preconcentration method was based on using 1-decanol/THF as supramolecular solvent phase and quinalizarin as a chelating agent. Thorium(IV)- quinalizarin hydrophobic complex was obtained at pH 6.0, extracted into the supramolecular solvent phase, centrifuged and then the absorbance was measured spectrophotometrically at 590 nm. The impact of some variables on the efficiency of microextraction; pH, amount of quinalizarin, and supramolecular solvent type, ratio and volume, ultrasonication and centrifugation time, sample volume and influence of matrix ions; was optimized. Linearity ranged from 2.0 to 100 μg L with a limit of detection (LOD) of 0.40 μg L . The preconcentration factor (PF) was found to be 40. The precision of the method was confirmed with its low RSD% (1 4) The developed method was applied to the analysis of real water and soil

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Application of gas chromatography coupled with tandem mass spectrometry for the assessment of PAH levels in non industrial indoor air

Florentina Villanueva, Gema Sevilla, Sonia Lara, Pilar Martín, ... Beatriz Cabañas Pages 117-125

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An analytical hierarchy process for selection of the optimal procedure for resveratrol determination in wine samples

Magdalena Fabjanowicz, Marta Bystrzanowska, Jacek Namieśnik, Marek Tobiszewski, Justyna Płotka-Wasylka Pages 126-134

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Abstract

We present in this report the results of experimental study on the spectrochemical analysis of powder samples using subtarget supported micro mesh (SSMM) sample holder in low pressure ambient gases. The study is substantiated by establishing the analyte excitation mechanism with the evidence of shock wave plasma generation and the high temperature induced subsequently required for the thermal excitation and emission of the ablated atoms. The

application of SSMM sample holder using Cu subtarget and stainless steel micro mesh to a number of powder samples in low pressure ambient gases are shown to produce generally sharp emission lines with low background, without suﬀering from intensity reduction and matrix eﬀect commonly found in the use of pelletized powder samples. The same excellent spectral quality is demonstrated by its application to the analysis of rice samples which is the major staple diets in a large number of countries In particular the analysis of Zn in rice is shown to exhibit a linear calibration line with extrapolated

Abstract

A gas chromatographic coupled to a triple quadrupole tandem mass spectrometric (GC–MS/MS) method was optimized in order to measure the levels of polycyclic aromatic hydrocarbons (PAHs) in diﬀerent non industrial indoor

environments using active (filter + XAD-2) and passive (polyurethane, PUF) samplers. Ultrasonic and soxhlet extractions were used for active and passive samplers, respectively. The precision and accuracy of the analytical methods used were tested by spiking PUF, filters and XAD-2 with different working standards containing all analyzed PAH compounds. The proposed methods were applied to the analysis of real samples collected in the urban area of Ciudad Real, Spain.

Nineteen PAHs were investigated in homes and workplaces such as petrol station stores (PSS), an underground parking oﬃce and the oﬃce of a periodic technical inspection of vehicles (PTI). The range of individual concentrations of PAH collected with the active sampler was from non detected to 144 ng m at home from <LOD to 595 ng m at PSS from

⁻³ ⁻³

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Microchemical Journal 142 (2018) 17-23

ELSEVIER

Contents lists available at ScienceDirect

Microchemical Journal

journal homepage: www.elsevier.com/locate/microc

NiMn0

₃

nanoparticles anchored on graphene quantum dot: Application in sensitive electroanalysis of dobutamine

Foroozan Hasanpour":", Mohsen Nekoeinia", Abolfazl Semnani", Sahar Shojaei"

·• Department of Cnemtstry, Payame Noor University, 19395-4697 Tehran, Iran

b Department of Cnemtstry, Faculty of Science, Shahrekord University, P.O. Box 115, Shahrekord, Iran

ARTICLE INFO Keywords:

Dobutamine Graphene quantum dot NiMn03 nanopartides Modified carbon paste electrode Electroanalysis

ABSTRACT

Simple hydrothermal route was developed for synthesis of NiMn03 in the presence of graphene quantum dot.

The structure and morphological aspect of nano-hybrid were approved using FE-SEM, XRO and FT-IR. Theo, these nano-particles were chosen as a modifier in carbon paste electrode, which produces noticeable catalytic effect for electro-oxidation of dobutamine. The oxidation mechanism of the drug was also studied using cyclic voltammetry. After variable optimization, a linear regression function was found in the range of 0.08-40.0 µM with the detection limit of 0.02 µM between the concentration of doburamine and its anodic signal. The utility of the modified electrode was assessed by measuring the concentration of dobutamine in serum samples.

I. Introduction

Dobutamine (DB) is a member of catecholamine drugs used in treating coronary heart disease and cardiogenic shock [1]. It is used to improve heart rate or cardiac output in congestive heart failure [2]. DB must be used with caution in some diseases such as atrial fibrillation because it can increase the atrioventricular conduction [3]. The structure of DB contains three functional groups consisting of a catechol, secondary amine and phenol ring with great potential for participating in redox reactions [ 4]. ln recent years, chemically modified electrodes have found significant applications in electrochemical techniques [5, 6]. Surface modification of electrodes causes some improvements in sensitivity and reproducibility of detection and in some cases increases selectivity to analyte by immobilizing functional groups. The advent of nano-materials-based sensing systems offers a sensitive, fast and low-cost method in electrochemical detection [7-12]. Gra- phene quantum dots (GQDs), as a novel class of carbon-based material, have found many applications in electrode modification [13, 14]. They are a kind of OD material [15, 16] with size diameter smaller than 20 run. The quantum confinement effects of GQDs result in large surface area and high conductivity, which can be used as a good sensing material for construction of electrochemical sensors. Recently, metal oxide nano-particles have been applied as an efficient electrode modifier material, which mediates the electron transfers between the analyte and the electrode [17]. Mostly used electrode materials were transition metal oxides like Ru02, Co304 and MnO, which suffer limitation of poor electrical conductivity [18]. The use of binary metal oxides such as NiCo204 and Zn2Sn04 can lessen this restriction [19, 20]. NiMn0₃is one of the binary metal oxides with good electrical

• Corresponding author.

E-mail address: [email protected] (F. Hasanpour).

https:/ /doi.org/10.1016/j.microc.2018.06.014

Received 9 January 2018; Received in revised form 8 June 2018; Accepted 8 June 2018 Available online 09 June 2018

conductivity, which can adapt itself to Ilmenite crystal type [21]. Zhu et al.

synthesized the nickel manganese ilmenite-type (NiMn0³⁾ with some characteristics such as excellent capacitance characteristics, good electric conductivity and low cost [22]. NiMn03 has a rhombohedral structure and both cations (Ni²⁺and Mn⁴⁺⁾occupy octahedral positions. Giri et al.

prepared N-doped graphene/Nistno, to use in supercapacitors [23]. Then- systems and carboxyl/hydroxyl groups on the surface of graphene can simply interact with transition metal ions [24]; and in a similar manner, incorporation of NiMn0₃with GQDs would be superior if the presence of GQDs results in better conductivity or smaller size of GQDs/NiMn03 nano- hybrid. In this study, nitrogen-doped GQDs were synthesized using a reac- tion between citric acid and urea. Then, GQDs/NiMn03 nano-hybrid was prepared via a one-step hydrothermal method. The synthesized nano-com- posite was used as a modifier in carbon paste electrode (CPE), which causes facilitation of electron transfer process in DB oxidation and enhances sensitivity for the determination of this drug. The proposed modified electrode provides accurate analysis of DB in serum samples. To the best of our knowledge, there has been no report on the application of GQDs/NiMn03

nano-hybrid in electrochemical sensing field.

2. Experimental

2.1. Apparatus and chemicals

Electroanalysis was performed using Metrohm Autolab PGSTATlOI equipped with NOVA software (Ecochernie, Utrecht, the Netherlands), and the three-electrode system contained a platinum counter electrode,

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Microchemical Journal 142 (2018) 187-194

ELSEVIER

Contents lists available at ScienceDirect

Microchemical Journal

journal homepage: www.elsevier.com/locate/microc

Impact of selected parameters of the fermentation process of wine and wine itself on the biogenic amines content: Evaluation by application of

chemometric tools

Justyna Plotka-Wasylka

²

·•·1, Vasil Simeonov'Y, Calum Morrison'v', Jacek Narniesnik=!

·• Department of Analytical Chemi5try, Faculty of Chemi5try, Gda.risk University of Technology, Gdaiisk, Poland

b Faculty of Chemi5try and Phannacy, University of Sofia, Sofia 1126, Bulgaria

c Forensic Medicine and Science, School of Medicine, Denti5try and Nursing, College of Medical, Veterinary and Life Sciences, University of Glasgow, United Kingdom

ARTICLE INFO Keywords:

Wine Biogenic amines Food analysis Correlations SPME Cluster analysis

ABSTRACT

The demand for safer foods has promoted more research into biogenic amines (BAs) over the past few years, however, there are still some questions that remain unanswered. Despite the fact that BAs are present in wine and can cause toxic effect to the body, a shared regulation limiting the amounts of BAs in wine is still lacking. A detailed understanding of their presence in wine is also important for the food trade sector. Therefore, the aim of this work was to determine the level of selected BAs in wine samples origin from Poland. Thereafter, the evaluation of correlation between concentration of BAs and selected parameters including pH, alcohol content and fermentation temperature by application of chemometric analysis was carried out. The BAs were determined by application of previously developed SPME-GC-MS methodology characterized by low detection limits ranged from 0.009 µg/L (tyramine) to 0.155 µg/L (histamine). Data obtained in this study show that none of the wine samples surpassed the toxic levels reported for BAs in the literature (the total BAs content was ranged from 7 to 2174 µg/L), therefore, these wines appear to be safe as regards the risk associated with the intake of potentially toxic BAs. Moreover, several correlations between occurrence, concentration of biogenic amines, important factors of winemaking process as well as physico-chemical parameters of wine were indicated. Even though infonnation on BAs is currently not included in wine composition databases, information on their existence, distribution, concentration and knowledge of existing relationships between BAs and other wine parameters is crucial and may be useful for the food industry, health professionals and consumers.

I. Introduction

The occurrence of biogenic amines (BA) in wine is becoming in- creasingly important to both consumers and producers due to the potential threat of toxicity to humans and trade implications. Considering the fact that concentration levels of BA can increase (cadaverine, putrescine and tyramine), decrease (spermine and spermidine) or remain constant during the processing and storage of some food products (including wine) their amounts and ratios have been proposed as an index of the hygienic conditions of raw material and/or manufacturing practices [1]. Thus, BA have the potential to be used as indicators of food spoilage as well as authenticity [2].

Biogenic amines are naturally present in wine and it is very difficult, or even impossible, to obtain a wine that does not contain any biogenic

• Corresponding author.

E-mail address: [email protected] (J. Plotka-Wasylka).

I Current address: 11/12 Narulowicza Street, 80-233 Gdati.sk, Poland.

2 Current address: I James Bourchier Blvd., Sofia 1126, Bulgaria.

3 Current address: Glasgow Gl2 SQQ, United Kingdom.

hllps:/ /doi.org/10.1016/j.microc.2018.06.038

Received 11 May 2018; Received in revised fonn 25 June 2018; Accepted 27 June 2018 Available online 30 June 2018

amines [3]. The occurrence of BAs in wine may have many different sources: amino acid content at the initial and final phases of alcoholic fermentation, time of wine contact with yeast, but also the type and degree of ripeness of the grapes, the climate and soil of the viticulture area, and the vinification techniques can contribute to the biogenic amines content in wine. Additionally, biogenic amines can be produced during ageing or storage when wine is exposed to the activity of dee- arboxylase positive microorganisms [4].

The main BA's associated with wine include histamine, putrescine, tyramine and cadaverine, followed by 2-phenylethylarnine, tryptamine, agmatine, sperrnidine, and spermine [S]. Some polyamines such as putrcscine may be present in grape skin. They are mainly produced by grape vines in response to stress factors including salt, heat, and water deficiency. Putrescine and cadaverinc are also normally associated with