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YBCO次世代超電導線材のMO磁束観察法による特性評価

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(1)

YBCO

線材の

MO

法による評価

低温工学協会 九州・西日本支部研究会 2006 July 20-22

Photograph of core part

Core part of RTR-MOI

MO

装置 開発

MO

装置

開発

(2)

R1 R2 R3 R4 R5 R6

#1 20 6.5 10 0.13 - 2.5

#2 20 6.4 10 0.14 - 2.5

#3 20 6.7 10 0.12 - 2.5

#4 20 6.9 10 0.11 - 2.5

QuickTime˛ Ç∆

TIFFÅià≥èkǻǵÅj êLí£ÉvÉçÉOÉâÉÄ

ǙDZÇÃÉsÉNÉ`ÉÉÇ å©ÇÈÇΩÇflÇ…ÇÕïKóvÇ≈Ç∑ÅB

QuickTime˛ Ç∆

TIFFÅiLZWÅj êLí£ÉvÉçÉOÉâÉÄ

ǙDZÇÃÉsÉNÉ`ÉÉÇ å©ÇÈÇΩÇflÇ…ÇÕïKóvÇ≈Ç∑ÅB

Low defect density ! A lot of defects !

MOI に用いる磁気光学膜の作製

The indicator films are necessary to observe MO images.

MO

装置 開発

MO

装置

開発

We obtain high quality MO indicator films !

(3)

YBCO

線材の

MO

法による評価

低温工学協会 九州・西日本支部研究会 2006 July 20-22

初期の IBAD/PLD 線材の磁束侵入の様子

IBAD/PLD

素線評価 素線評価

Defects

Fujikura #106880 40K ZFC

10mT 20mT 30mT 40mT 50mT 60mT

70mT 80mT 90mT 100mT Remanent

10mm

IBAD/PLD 線材への磁束侵入は左右均一

Dendritic な磁束侵入が µm オーダで折れ曲がっ

バッファ層の粒界の細かさを反映している ている

(4)

conductors in USA Flux penetration into

RABiTS tape

D. M. Feldmann (Polyanskii group) et al.

Appl. Phys. Lett. 77 (2000)2906.

YBCO(PLD)/CeO2/YSZ/CeO2/Ni

15K 600 Oe

Grain boundaries are connected each other with small angles, and magnetic flux penetrates along grain boundaries.

Rolling aligned Ni has a large grain (~ 100µm).

(5)

YBCO

線材の

MO

法による評価

低温工学協会 九州・西日本支部研究会 2006 July 20-22

RTR-MOI 装置による MO 観察結果

IBAD/PLD (Total length 1.5m) ZFC 40K 80 mT [NCCC]

This tape has only a few defects. Magnetic flux penetration is uniform for both width and length directions.

150 mm

I

c

~250A

10 mm

素線評価 素線評価

(6)

Movie of the observation result by RTR-MOI Movie of the observation result by RTR-MOI

IBAD/PLD (Total length 1.5m) IBAD/PLD (Total length 1.5m)

ZFC 40K 50 mT ZFC 40K 50 mT [NCCC]

[NCCC]

I

c

~250A I

c

~250A

10 mm (width) 10 mm (width)

Tape edge Tape edge

Tape edge Tape edge

Shooting time ~ 1 hour

Shooting time ~ 1 hour

素線評価 素線評価

(7)

YBCO

線材の

MO

法による評価

低温工学協会 九州・西日本支部研究会 2006 July 20-22

RTR-MOI

Hall sensor array (Tapestar@THEVA)

Both Hall sensor array equipment (tapestar@THEVA) and our new RTR- MOI can visualize 2D-image of flux distribution.

Using same sample : TFA-MOD (I

c

~100A) [SRL, early stage specimen]

40K, 50mT

77K, 20mT

10 mm (width)

MOI has a higher spatial resolution !

There are many defects in this sample.

Hall sensors array can detect same defect.

1µm - 10µm

Spatial resolution of RTR-MOI equipment

素線評価 素線評価

(8)

1μμ 10μμ 100 μμ 1μμ 10μμ 100μμ

1μ 1μ 10μ 100μ

Comparison with other characterization methods Spatial resolution

Measuring speed(m/h)

RTR MOI

Hall sensor array system

RTR I-V meas.

V I

Hall sensor array(Tapestar@THEVA)

RTR I-V measurement

coated conductor

Field

Moving

We must choose measuring method by the purpose!

Referensi

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