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Microwave-Assisted and Thermal Synthesis of Calix[4]arene Derivatives
By:Al-Douh, MH (Al-Douh, M. H.)[ 1 ] ; Ali, Y (Ali, Y.)[ 2 ] ; Abd Hamid, S (Abd Hamid, S.)[ 3 ] RUSSIAN JOURNAL OF ORGANIC CHEMISTRY
Volume: 56 Issue: 7 Pages: 1251-1257 DOI: 10.1134/S1070428020070209 Published: JUL 2020
Document Type: Article View Journal Impact
Abstract
Sometert-butylcalix[4]arene derivatives were synthesized by thermal and microwave methods. The microwave method was conducted in two ways: (1) all the reactants were added in one batch and (2) the reactants were added in two batches under different conditions. Tetrabutylammonium iodide (TBAI) was used in both methods, and its effect on the reaction rate was studied. In general, the duration of the microwave-assisted reactions in the presence of TBAI, especially in the two-batch method, was shorter, and the yields were higher, than in the thermal reaction. The highest yield of (S)-glycidyl calixarene derivative by the thermal method was obtained by using K(2)CO(3)as a base with MeCN as a solvent in the presence of TBAI, while the lowest yield of the same compound was observed when using acetone in the absence of TBAI. All the synthesized calix[4]arene derivatives were characterized by(1)H and(13)C NMR experiments.
Keywords
Author Keywords:microwave synthesis; calix[4]arenes; tetrabutylammonium iodide
Author Information
Reprint Address:
Sarhad Univ Sci & Informat Technol, Dept Chem, Peshawar 25000, Pakistan.
International Islamic University Malaysia Int Islamic Univ Malaysia, Kulliyyah Sci, Kuantan 25200, Pahang, Malaysia.
Corresponding Address: Ali, Y (corresponding author)
Sarhad Univ Sci & Informat Technol, Dept Chem, Peshawar 25000, Pakistan.
Corresponding Address: Abd Hamid, S (corresponding author)
Int Islamic Univ Malaysia, Kulliyyah Sci, Kuantan 25200, Pahang, Malaysia.
Addresses:
[ 1 ] Hadhramout Univ, Fac Sci, Chem Dept, Mukalla 50511, Hadhramout, Yemen [ 2 ] Sarhad Univ Sci & Informat Technol, Dept Chem, Peshawar 25000, Pakistan
[ 3 ] Int Islamic Univ Malaysia, Kulliyyah Sci, Kuantan 25200, Pahang, Malaysia E-mail Addresses:[email protected]; [email protected]
Funding
Funding Agency Grant Number
Malaysian government
International Islamic University Malaysia (IIUM) Fund ERGS12-017-0017 View funding text
Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER, 233 SPRING ST, NEW YORK, NY 10013-1578 USA
Journal Information
Impact Factor: Journal Citation Reports
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Research Areas: ChemistryWeb of Science Categories: Chemistry, Organic See more data fields
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4/1/2021 Web of Science [v.5.35] - Web of Science Core Collection Full Record
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