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Synthesis of Cyclic Polymers and Characterization of Their Diffusive Motion in the Melt State at the Single Molecule Level

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Synthesis of Cyclic Polymers and

Characterization of Their Diffusive Motion in the Melt State at the Single Molecule Level

Item Type Article

Authors Habuchi, Satoshi;Yamamoto, Takuya;Tezuka, Yasuyuki Citation Habuchi S, Yamamoto T, Tezuka Y (2016) Synthesis of Cyclic

Polymers and Characterization of Their Diffusive Motion in the Melt State at the Single Molecule Level. Journal of Visualized Experiments. Available: http://dx.doi.org/10.3791/54503.

Eprint version Publisher's Version/PDF

DOI 10.3791/54503

Publisher MyJove Corporation

Journal Journal of Visualized Experiments

Rights Copyright © 2016 Creative Commons Attribution- NonCommercial-NoDerivs 3.0 Unported License Download date 2024-01-02 19:10:57

Link to Item http://hdl.handle.net/10754/621130

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Journal of Visualized Experiments www.jove.com

Copyright © 2016 Creative Commons Attribution-NonCommercial-NoDerivs 3.0 Unported

License Page 1 of 2

Materials List for:

Synthesis of Cyclic Polymers and Characterization of Their Diffusive Motion in the Melt State at the Single Molecule Level

Satoshi Habuchi1, Takuya Yamamoto2,3, Yasuyuki Tezuka3

1Biological and Environmental Sciences and Engineering Division, King Abdullah University of Science and Technology (KAUST) 2Division of Applied Chemistry, Faculty of Engineering, Hokkaido University

3Department of Organic and Polymeric Materials, Tokyo Institute of Technology

Correspondence to: Satoshi Habuchi at [email protected], Yasuyuki Tezuka at [email protected] URL: http://www.jove.com/video/54503

DOI: doi:10.3791/54503

Materials

Name Company Catalog Number Comments

Materials

THF Godo

Wakosil C-300 Wako Pure Chemical Industries

Acetone Godo

Toluene Godo

n-Hexane Godo

CHCl3 Kanto Chemical

Bio-Beads S-X1 Bio-Rad

Methyl triflate Nacalai Tesque

Triflic anhydride Nacalai Tesque

Potassium Hydroxide Wako Pure Chemical Industries

Ethanol Wako Pure Chemical Industries

Poly(tetrahydrofuran) Aldrich

Chloroform Wako Pure Chemical Industries

Immersion oil Cargille Type 37 / Type A

Equipment

2-Neck 100-ml round-bottom flask Flask

Beaker Funnel

Filter paper Whatman

Reflux condenser Syringe

Water bath Magnetic stirrer Rotary evaporator

Microscope cover slips (24 x 24

mm, No. 1) Matsunami Glass CO22241

Staining jar AS ONE Corporation 1-7934-01

Ultrasonic cleaner VWR International 142-0047

Inverted microscope Olympus IX71

Ar-Kr ion laser Coherent Innova 70C

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Journal of Visualized Experiments www.jove.com

Copyright © 2016 Creative Commons Attribution-NonCommercial-NoDerivs 3.0 Unported

License Page 2 of 2

Berek compensator Newport 5540

Excitation filter Semrock LL01-488-12.5

Dichloric mirror Omega optical 500DRLP

Emission filter Semrock BLP01-488R-25

Lens and mirror Thorlabs

EM-CCD camera Andor Technology iXon

Objective lens (100X, N.A. = 1.3) Olympus UPLFLN 100XOP

Objective heater Bioptechs

Preparative GPC Japan Analytical Industry LC-908

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