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Quantification of Ag in Ag doped glass based metamaterials using XPS analysis.

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63<sup>rd</sup> ANNUAL CONFERENCE OF THE SA INSTITUTE OF PHYSICS

Contribution ID:180 Type:Oral Presentation

Quantification of Ag in Ag doped glass based metamaterials using XPS analysis.

Wednesday, 27 June 2018 10:40 (20 minutes)

Quantification in XPS is not easy, more especially if the concentrations of the substituents in the sample are not homogeneous on the sample surface or with depth. In this study the Quases-Tougaard Software analyses approach was used to quantify Ag nano clusters in a Ag doped glass host. The specimens were synthesized by a simple molten bath ion exchange method and then annealed at different temperatures. A XPS-spectrum of the Ag 3d peaks were isolated from a survey spectrum of the specimen and compared to a spectrum generated from a pure Ag reference. The morphology was changed until there was a good match between the two spectra.

The results shows that the QUASES Software can be a vital tool in determining the morphology of elements in a sample.These results are then compared with results from TEM data.

Please confirm that you<br>have carefully read the<br>abstract submission in- structions<br>under the menu item<br>”Call for Abstracts”<br><b>(Yes / No)</b>

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Consideration for<br>student awards<br><b>Choose one option<br>from those below.</b><br>N/A<br>Hons<br>MSc<br>PhD

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institution and email address.

Prof. WD. Roos, University of the Free State, [email protected]

Primary authors: Prof. SWART, Hendrik (University of the Free State); Dr KUMAR, Promod (University of the Free State); Ms MAKOLE, Rethabile (University of the Free State); Prof. ROOS, Wiets (University of the Free State)

Presenter: Ms MAKOLE, Rethabile (University of the Free State)

Session Classification: Physics of Condensed Matter and Materials

Track Classification: Track A - Physics of Condensed Matter and Materials

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