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Lampiran 1. Posisi geografis titik-titik sampling lokasi penelitian Titik

Sampling Zona Perairan

Posisi Geografis Long Lat 1 Sungai 770784.165 9424951.027 2 Sungai 769172.929 9425565.751 3 Sungai 767296.802 9425236.403 4 Estuaria 767195.501 9425254.306 5 Estuaria 766632.539 9425404.274 6 Estuaria 766203.570 9425545.122 7 Estuaria 765668.564 9425592.634 8 Estuaria 765103.319 9425464.775 9 Estuaria 764559.174 9425456.996 10 Estuaria 763883.447 9425524.694 11 Pantai 763539.611 9423807.763 12 Pantai 763126.906 9425568.102 13 Pantai 764153.359 9427658.941 14 Pantai 763929.687 9429804.873 15 Pantai 762904.523 9428470.326 16 Pantai 762347.424 9425654.920 17 Pantai 762523.309 9423507.342

Lampiran 2. Data hasil pengukuran parameter fisika kimia sedimen A. Musim Barat (3 s/d 5 Januari 2015)

Titik Sampling

Karbon Organik Eh (mV)

Persentase Tekstur Kelas Tekstur (SkalaWenworth)

(%) Sand Silt Clay

1 2.24 23.43 65 29 6 Lempung liat berpasir

2 2.29 17.37 69 12 19 Lempung liat berpasir

3 2.25 17.1 70 22 8 Lempung liat berpasir

4 2.64 10.52 63 5 32 Lempung liat berpasir

5 2.15 9.15 60 5 35 Lempung liat berpasir

6 2.45 8.73 79 10 11 Lempung berpasir

7 2.74 8.43 77 8 15 Lempung berpasir

8 2.25 8.18 75 7 18 Lempung berpasir

9 2.38 7.95 77 7 16 Lempung berpasir

10 2.89 8.52 63 2 35 Lempung liat berpasir

11 2.14 2.20 63 3 34 Lempung liat berpasir

12 2.67 2.35 70 6 24 Lempung liat berpasir

13 2.90 2.33 78 2 20 Lempung liat berpasir

14 3.04 -11.17 39 45 16 Lempung

15 2.87 -13.53 36 4 60 Liat

16 2.75 -13.75 35 5 60 Liat

17 2.62 -14.13 39 2 59 Liat

B. Musim Timur (1 s/d 3 Agustus 2015) Titik

Sampling

Karbon Organik Eh (mV)

Persentase Tekstur Kelas Tekstur (SkalaWenworth)

(%) Sand Silt Clay

1 2.07 -71.37 53 19 28 Lempung berpasir

2 2.05 -73.50 56 17 27 Lempung berpasir

3 2.03 -87.71 79 3 18 Lempung berpasir

4 2.31 -31.56 55 25 20 Lempung liat berpasir

5 1.21 -33.3 59 26 15 Lempung liat berpasir

6 1.14 -27.45 79 2 19 Lempung berpasir 7 1.10 -59.80 78 4 18 Lempung berpasir 8 1.01 -49.31 88 2 10 Pasir berlempung 9 1.13 -33.6 85 5 10 Pasir berlempung 10 1.05 -59.70 82 7 11 Pasir berlempung 11 1.18 -71.60 63 24 13 Lempung berpasir 12 1.10 -72.95 68 20 12 Lempung berpasir 13 2.74 -96.73 9 68 23 Lempung berdebu

14 3.46 -98.90 3 68 29 Lempung liat berdebu

15 2.64 -80.85 13 11 76 Liat

16 2.33 -92.21 10 13 77 Liat

Lampiran 3. Data hasil pengukuran parameter fisika kimia perairan A. Musim Barat (3 s/d 5 Januari 2015)

Titik Sampling

PARAMETER

SUHU (°C) pH SALINITAS (‰) DO (mg/l) TSS (mg/l) DOC (mg/l)

PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT

1 27.00 5.50 0.2 3.50 264 3.83 2 27.00 5.55 0.2 3.50 249 5.24 3 27.00 5.55 0.2 3.50 251 3.19 4 27.50 29.50 5.90 5.32 0.5 0.5 3.50 3.35 170 200 2.81 4.93 5 28.25 29.70 5.57 5.27 0.5 0.5 3.45 3.37 178 194 1.23 4.61 6 28.50 29.00 5.65 5.55 1.0 0.5 3.35 3.63 166 172 1.71 4.77 7 28.00 29.50 5.75 5.69 2.0 0.5 4.22 3.58 128 138 1.39 5.43 8 28.00 29.00 6.10 6.02 2.5 1.5 4.25 3.55 154 156 1.76 4.14 9 28.00 28.00 6.13 6.10 6.0 4.0 4.51 4.01 154 152 2.49 4.29 10 26.50 28.00 6.20 6.09 8.0 4.0 6.05 3.52 116 148 1.79 3.66 11 27.00 28.50 7.10 7.04 15.0 13.0 5.54 4.55 104 135 3.29 6.38 12 26.50 28.50 7.05 7.05 14.0 12.5 5.75 5.04 126 150 3.60 15.45 13 27.00 29.00 7.10 7.05 15.0 13.0 6.57 5.23 130 145 15.64 14.69 14 26.50 29.00 7.20 7.12 21.0 20.0 6.23 5.04 60 65 27.05 27.68 15 25.00 28.00 7.25 7.17 21.0 20.0 6.77 5.26 32 35 25.82 25.94 16 25.00 28.50 7.25 7.20 21.0 20.0 6.36 5.21 30 35 12.67 24.55 17 25.00 28.50 7.25 7.20 21.0 20.5 6.58 5.39 30 35 11.41 20.95

B. Musim Timur (1 s/d 3 Agustus 2015)

Titik Sampling

PARAMETER

SUHU (°C) pH SALINITAS (‰) DO (mg/l) TSS (mg/l) DOC (mg/l)

PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT PASANG SURUT

1 31.00 6.70 0.3 3.60 16 6.48 2 31.00 6.70 0.3 3.50 14 6.64 3 31.00 6.80 0.3 3.24 11 6.60 4 28.00 31.00 7.20 7.03 7.0 3.5 4.20 3.50 14 14 18.64 20.21 5 28.50 30.50 7.25 7.04 9.0 4.0 5.00 3.18 12 14 18.47 25.33 6 29.00 31.00 7.25 7.05 12.0 5.0 4.70 3.21 12 14 23.38 25.12 7 30.00 31.00 7.27 7.21 16.0 9.0 4.05 3.17 12 12 26.69 26.97 8 29.50 30.00 7.26 7.21 18.0 10.0 4.13 3.35 14 19 29.23 30.25 9 29.70 31.00 7.26 7.23 20.5 10.5 4.18 3.72 14 18 30.04 30.12 10 30.00 30.50 7.28 7.30 22.0 15.5 5.00 3.51 16 25 30.18 30.86 11 29.00 30.50 7.29 7.25 29.0 27.0 5.24 4.46 16 30 28.60 28.87 12 28.50 31.00 7.29 7.29 27.0 25.0 5.47 5.14 16 31 26.93 25.40 13 29.00 32.00 7.20 7.10 28.5 26.0 5.35 5.05 14 26 28.12 24.02 14 27.50 31.00 7.15 7.05 30.0 28.5 5.15 4.50 12 12 31.62 31.91 15 28.00 30.00 7.30 7.30 30.0 29.0 5.65 5.20 12 12 28.10 28.10 16 27.50 30.00 7.50 7.30 30.0 29.0 6.10 5.13 12 12 22.91 24.02 17 27.50 30.00 7.40 7.30 30.0 28.5 6.26 5.21 10 10 26.58 25.25

Lampiran 4. Data hasil analisis konsentrasi logam berat Pb dan Zn

A. Musim Barat (3 s/d 5 Januari 2015)

Titik Sampling

Konsentrasi Logam Berat

Pb Zn

Terlarut (mg/l) Partikulat (mg.kg-1)

Dalam

Air Pori Sedimen (mg.kg-1)

Terlarut (mg/l) Partikulat (mg.kg-1)

Dalam

Air Pori Sedimen (mg.kg-1) Pasang Surut Pasang Surut (mg/l) Pasang Surut Pasang Surut (mg/l)

1 <0.002 2.569 <0.002 4.308 <0.002 90.946 0.051 113.190 2 <0.002 2.521 <0.002 4.215 <0.002 90.942 0.055 103.294 3 <0.002 2.513 <0.002 4.330 <0.002 88.175 0.080 115.792 4 0.020 0.015 0.639 0.560 0.033 0.237 0.004 0.003 34.235 28.536 0.102 57.843 5 0.025 0.022 1.006 0.752 0.025 0.370 <0.002 <0.002 38.287 30.913 0.105 68.492 6 0.025 0.015 1.283 0.971 0.038 0.525 0.003 <0.002 38.660 30.436 0.110 62.275 7 0.018 0.018 1.020 0.615 0.045 0.364 0.003 <0.002 50.941 53.992 0.136 71.347 8 0.018 0.017 1.003 0.964 0.050 1.086 <0.002 <0.002 40.441 33.632 0.113 70.984 9 0.030 0.025 0.883 0.801 0.038 1.364 0.006 0.005 50.771 40.947 0.108 64.835 10 0.036 0.022 1.139 0.971 0.047 1.526 0.009 0.005 70.308 55.810 0.127 70.665 11 0.019 0.019 0.945 1.022 0.025 2.508 0.004 <0.002 58.613 57.684 0.104 71.511 12 0.015 0.017 1.070 1.089 0.030 2.296 0.008 0.006 64.472 64.313 0.141 65.659 13 0.075 0.052 1.095 1.031 0.065 3.091 0.018 0.010 65.228 70.118 0.225 78.556 14 0.075 0.056 1.288 1.176 0.094 4.232 0.020 0.015 75.634 75.732 0.278 101.781 15 0.023 0.021 1.267 1.154 0.042 4.004 0.015 0.008 75.443 72.579 0.210 88.898 16 0.020 0.019 1.154 1.133 0.036 3.865 0.007 0.004 72.831 72.556 0.109 80.053 17 0.016 0.016 1.136 1.395 0.020 3.523 0.005 <0.002 64.564 64.861 0.225 75.979

B. Musim Timur (1 s/d 3 Agustus 2015)

Titik Sampling

Konsentrasi Logam Berat

Pb Zn

Terlarut (mg/l) Partikulat (mg.kg-1)

Dalam

Air Pori Sedimen (mg.kg-1) Terlarut (mg/l) Partikulat (mg.kg-1) Dalam Air Pori Sedimen (mg.kg-1) Pasang Surut Pasang Surut (mg/l) Pasang Surut Pasang Surut (mg/l)

1 <0.002 2.046 <0.002 2.013 <0.002 29.151 0.220 45.359 2 <0.002 1.807 <0.002 2.217 <0.002 26.876 0.455 42.910 3 <0.002 1.835 <0.002 2.329 <0.002 24.171 0.606 46.060 4 0.067 0.065 0.521 0.520 0.168 0.660 0.011 0.005 17.005 16.992 2.216 38.730 5 0.076 0.059 0.548 0.534 0.175 0.775 0.008 0.003 19.007 18.990 2.342 38.982 6 0.083 0.060 1.273 1.270 0.182 1.465 <0.002 <0.002 20.027 20.016 2.530 39.018 7 0.077 0.063 0.924 0.911 0.170 1.581 0.008 0.006 19.441 19.436 2.415 39.005 8 0.039 0.024 0.837 0.904 0.176 1.714 <0.002 <0.002 20.414 20.410 2.782 39.110 9 0.059 0.055 1.072 1.039 0.174 1.611 0.015 0.010 22.249 22.250 2.559 39.207 10 0.166 0.122 1.271 1.270 0.179 1.665 0.015 0.013 26.643 26.636 2.706 39.520 11 0.107 0.085 0.470 0.459 0.255 0.957 <0.002 <0.002 19.467 19.410 2.685 39.215 12 0.080 0.063 0.667 0.652 0.401 1.706 0.003 0.003 21.462 21.407 2.753 39.330 13 0.221 0.142 0.525 0.555 0.423 1.541 0.061 0.035 21.453 21.631 3.330 41.313 14 0.221 0.175 0.965 0.966 0.446 2.027 0.092 0.074 22.877 22.775 3.526 42.870 15 0.195 0.125 0.712 0.730 0.412 1.453 0.045 0.027 22.142 22.166 3.251 41.679 16 0.171 0.065 0.557 0.573 0.405 1.004 0.012 0.007 22.075 22.086 3.068 39.214 17 0.063 0.058 0.582 0.562 0.305 0.980 <0.002 <0.002 20.455 20.490 3.142 38.840

Lampiran 5. Data hasil analisis fraksinasi geokimia logam berat Pb dan Zn

A. Musim Barat (3 s/d 5 Januari 2015)

Titik Sampling

Fraksinasi Geokimia Logam Berat (%)

Pb Zn

Residual Organik Oksida Mn-Fe Karbonat Exchangeable Residual Organik Oksida Mn-Fe Karbonat Exchangeable

1 78.99 16.22 1.49 3.30 0.00 68.77 25.00 6.23 0.00 0.00 2 83.22 11.53 1.89 3.36 0.00 73.97 16.88 9.14 0.00 0.00 3 84.86 9.62 2.29 3.23 0.00 74.07 16.45 9.48 0.00 0.00 4 79.66 15.01 1.29 4.04 0.00 73.36 25.55 1.09 0.00 0.00 5 80.08 14.57 1.36 3.99 0.00 75.49 22.88 1.63 0.00 0.00 6 80.20 13.93 1.47 4.40 0.00 76.91 21.16 1.94 0.00 0.00 7 80.96 12.96 1.55 4.53 0.00 78.00 19.96 2.04 0.00 0.00 8 82.13 12.11 1.78 3.98 0.00 76.50 20.60 2.90 0.00 0.00 9 84.54 9.03 1.97 4.47 0.00 75.99 20.64 3.37 0.00 0.00 10 84.93 8.33 2.25 4.50 0.00 75.42 20.21 4.38 0.00 0.00 11 82.71 11.26 3.39 2.64 0.00 77.30 22.45 0.26 0.00 0.00 12 81.52 11.70 3.03 3.75 0.00 74.35 22.47 3.19 0.00 0.00 13 75.92 17.61 2.74 3.72 0.00 75.55 23.56 0.89 0.00 0.00 14 74.47 18.87 2.75 3.91 0.00 74.99 23.95 1.06 0.00 0.00 15 75.13 18.06 2.57 4.25 0.00 75.39 23.81 0.80 0.00 0.00 16 79.23 13.96 2.57 4.23 0.00 73.60 23.17 3.23 0.00 0.00 17 78.39 14.39 2.92 4.30 0.00 74.79 24.93 0.28 0.00 0.00

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