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LAMPIRAN

Lampiran 1. Kromatogram GC MEAL Minyak Biji karet

Lampiran 2. Penentuan Kadar Asam Lemak Bebas

Kadar FFA (%) = x 100%

A. Kadar Asam Lemak Bebas Sebelum Pemurnian

1. Kadar FFA (%) = x 100 %

= 5, 8026 %

2. Kadar FFA (%) =

x 100%

= 5, 8996 %

3. Kadar FFA (%) =

X 100%

= 5, 6763 %

Rata – rata kadar asam lemak sebesar 5, 7 % B. Kadar FFA Setelah Deguming dan Bleaching

1. Kadar FFA (%) = x 100 %

= 5, 8705 %

2. Kadar FFA (%) =

x 100%

= 5, 4679 %

3. Kadar FFA (%) =

X 100%

= 5, 7 %

Rata – rata kadar asam lemak sebesar 5,67 % B. Kadar Asam Lemak Setelah Pemurnian

1. Kadar FFA (%) =

X 100%

= 0, 2699 %

2. Kadar FFA (%) =

X 100%

= 0, 1990 %

3. Kadar FFA (%) =

X 100%

= 0, 1997 %

Rata – rata kadar asam lemak sebesar 0, 2184 %

Lampiran 3. Penentuan Volume NaOH 10 % untuk netralisasi Berat Asam Lemak Bebas = Berat Minyak x % FFA

= 120 g x 5,7 %

= 6,84 g

Mol ALB =

=

= 0, 025 mol mol ALB = mol NaOH

mol NaOH = 0, 025

Berat NaOH yang dibutuhkan = mol NaOH x BM NaOH

= 0, 025 x 40

= 1 g

Volume NaOH 10 % yang dibutuhkan sebanyak 10 ml.

Lampiran 4. Penentuan Bilangan Iodin

Bilangan Iodin =

3, 328

A. Bilangan Iodin Sebelum Pemurnian 1. Bilangan Iodin =

= 110,79 2. Bilangan Iodin =

=

113,4

Rata – rata bilangan iodin sebesar 112, 095 B. Bilangan Iodin Setelah Pemurnian 1. Bilangan Iodin =

=

107, 2433

2. Bilangan Iodin =

=

110, 67

Rata – rata bilangan iodin sebesar 108, 9566 C. Bilangan Iodin Epoksida

1. Bilangan Iodin =

=

11,007

2. Bilangan Iodin =

=

10,39

Rata – rata bilangan iodin sebesar 10,6985

Lampiran 5. Minyak Biji Karet Hasil Ekstraksi dan Minyak Biji Karet Hasil Pemurnian

1. Minyak Biji Karet Hasil Ekstraksi

2. Minyak Biji Karet Hasil Pemurnian

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