Thermolyne Furnice High Temperature Planetary Ball Mill
Magnetic field Press
Aquades Peralatan Archimedes
21
22
23
24
LAMPIRAN 2
DATA PENGUKURAN TRUE DENSITY
1.
Pengukuran True Density mill scale
No
m1 (g)
m2 (g)
m3 (g)
m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,07
23,19
0,86
5.619
3
14,09
22,36
15,09
23,21
0,86
5.733
Rata-rata
5.638
2.
Pengukuran True Density FeMo
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm3)
1
14,09
22,36
15
23,19
0,86
9.783
2
14,09
22,36
15
23,19
0,86
9.783
Rata-rata
9.783
3. Pengukuran True Density campuran mill scale + FeMo (99:1)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm
3)
1
14,09
22,36
15,06
23,18
0,86
5.561
2
14,09
22,36
15,08
23,20
0,86
5.676
3
14,09
22,36
15,08
23,20
0,86
5.676
4. Pengukuran True Density campuran mill scale + FeMo (97:3)
No
m1 (g)
m2 (g)
m3 (g)
m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm
3)
1
14,09 22,36 15,08 23,2
0,86
5.676
2
14,09 22,36 15,08 23,2
0,86
5.676
3
14,09 22,36 15,09 23,21
0,86
5.733
Rata-rata
5.695
5. Pengukuran True Density campuran mill scale + FeMo (95:5)
No
m1 (g)
m2 (g)
m3 (g)
m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm
3)
1
14,09 22,36 15,09 23,21
0,86
5.733
2
14,09 22,36 15,08 23,2
0,86
5.676
3
14,09 22,36 15,09 23,21
0,86
5.733
Rata-rata
14,09 22,36 15,087 23,207
0,86
5.714
6. Pengukuran True Density campuran mill scale + FeMo (93:7)
No
m1 (g) m2 (g) m3 (g) m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm
3)
1
14,09 22,36 15,1
23,22
0,86
5.791
2
14,09 22,36 15,09 23,22
0,86
6.143
3
14,09 22,36 15,08
23,2
0,86
5.676
7. Pengukuran True Density campuran mill scale + FeMo (91:9)
No m1 (g) m2 (g) m3 (g) m4 (g)
ρ
Toluen
(g/cm3)
True Density
(g/cm
3)
1
14,09 22,36
15,1 23,23
0,86
6.204
2
14,09 22,36
15,1 23,22
0,86
5.791
3
14,09 22,36
15,1 23,22
0,86
5.791
LAMPIRAN 4
HASIL ANALISIS XRD
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename sampel.rd
File path d:\xrd\mill scale\mill scale (milling)\ Data collected 10/08/2015 16:00:38
Data range 10.000° to 79.980°
Number of points 3500
Step size 0.020
Alpha2 subtracted No
Background subtr. No
Data smoothed Yes
Radiation Cu-Ka
Wavelength 1.541874 Å
Retrieval
No. of matching entries 186
Name Formula Entry No.
(Wustite) Fe0.925 O 96-900-9772
and 186 others...
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-8637
Phase classification
Name
Mineral Name Wustite
Formula FeO
I/Ic 6.03
Sample Name 9008636
Quality C (calculated)
References
Publication
Bibliography Wyckoff R. W. G., "Second edition. Interscience Publishers, New York, New York
rocksalt structure", Crystal Structures 1, 85-237 (1963)
Origin of data
Source of entry
COD (Crystallography Open Database)
Link to orig. entry
9008636
Crystal structure
Crystallographic data
Space group F m -3 m (225)
Crystal system
cubic
Cell parameters
Atom coordinates
Element Oxid.
x
y
z
Bi
Focc
Fe 0.000 0.000 0.000 1.000000 1.000000 O 0.500 0.500 0.500 1.000000 1.000000
Diffraction data
Diffraction lines
d [Å]
Int. h k l Mult.
2.4888 684.5 1 1 1 8 2.1554 1000.0 2 0 0 6 1.5241 515.5 2 0 2 12 1.2998 208.6 3 1 1 24 1.2444 140.7 2 2 2 8 1.0777 59.0 4 0 0 6
Experimental
Physical Properties
Calc. density 5.95600 g/cm³
Remarks
Remarks
Comments - Diffraction pattern calculated by Match!.
Match! Phase Analysis Report
Sample: mill scale
Sample Data
Filename sampel.rd
File path d:\xrd\mill scale\mill scale (milling)\ Data collected 10/08/2015 16:00:38
Data range 10.000° to 79.980°
Number of points 3500
Step size 0.020
Alpha2 subtracted No
Background subtr. No
Data smoothed Yes
Radiation Cu-Ka
Wavelength 1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries 186
Name Formula Entry No.
(Wustite) Fe0.925 O 96-900-9772
and 186 others...
Peak List
No. 2theta [°] d [Å] I/I0 FWHM Matched
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-101-1085
Phase classification
Name Iron diiron(III) oxide
Publication
Bibliography , "The scattering power of oxygen and iron for X-Rays", Proceedings of the
Physical Society, London 38, 482-487 (1926)
Origin of data
Source of
entry COD (Crystallography Open Database)
Link to orig.
entry 1011084
Crystal structure
Crystallographic data
Diffraction data
Diffraction lines
d [Å] Int. h k l Mult.
4.8497 78.3 1 1 1 8
2.9698 282.1 2 0 2 12
2.5327 1000.0 1 3 1 24
2.4249 80.6 2 2 2 8
2.1000 201.2 0 4 0 6
1.9271 7.3 3 1 3 24
1.7146 90.0 2 4 2 24
1.6166 291.1 1 5 1 24
1.4849 388.7 4 0 4 12
1.4199 8.9 5 1 3 48
1.4000 0.0 4 2 4 24
1.3282 31.0 6 0 2 24
1.2810 77.4 3 5 3 24
1.2663 33.2 2 6 2 24
1.2124 24.2 4 4 4 8
1.1762 4.2 1 7 1 24
1.1225 31.7 6 2 4 48
1.0936 119.2 5 3 5 24
1.0500 44.9 0 8 0 6
1.0262 0.3 3 7 3 24
1.0186 0.0 4 6 4 24
Experimental
Physical Properties
Meas. density
5.17900 g/cm³
Calc. density 5.18900 g/cm³
Remarks
Remarks
Comments - Diffraction pattern calculated by Match!.
- I/Icor calculated by Match!.
Entry # 96-231-0324
Phase classification
Name Fe Mo
Publication
Bibliography Wilson C.G., Spooner F.J., "Ordering of atoms in the sigma phase of Fe Mo",
Acta Crystallographica (1,1948-23,1967)16, 230-230 (1963)
Origin of data
Source of entry
COD (Crystallography Open Database)
Link to orig. entry
2310323
Crystal structure
Crystallographic data
Space group P 42/m n m (136)
Diffraction data
Diffraction lines
1.1630 0.1 7 3 1 16
Physical Properties
Calc. density 9.42600 g/cm³
Remarks
Remarks
Comments - Diffraction pattern calculated by Match!.
Match! Phase Analysis Report
Sample: 93%millscale+7%femo tk 900
Sample Data
Filename 93%millscale+7%femo tk 900.ras File path d:\xrd\93%millscale+7%femo-tk 900\ Data collected 12/05/2016 10:14:04
Data range 20.000° to 90.000°
Number of points 7000
Step size 0.010
Alpha2 subtracted No
Background subtr. No
Data smoothed Yes
Radiation Cu-Ka
Wavelength 1.541874 Å
Retrieval
Search String
element=((O OR Fe OR Mo) AND NOT (H OR He OR Li OR Be OR B OR C OR N OR F OR Ne OR Na OR Mg OR Al OR Si OR P OR S OR Cl OR Ar OR K OR Ca OR Sc OR Ti OR V OR Cr OR Mn OR Co OR Ni OR Cu OR Zn OR Ga OR Ge OR As OR Se OR Br OR Kr OR Rb OR Sr OR Y OR Zr OR Nb OR Tc OR Ru OR Rh OR Pd OR Ag OR Cd OR In OR Sn OR Sb OR Te OR I OR Xe OR Cs OR Ba OR La OR Ce OR Pr OR Nd OR Pm OR Sm OR Eu OR Gd OR Tb OR Dy OR Ho OR Er OR Tm OR Yb OR Lu OR Hf OR Ta OR W OR Re OR Os OR Ir OR Pt OR Au OR Hg OR Tl OR Pb OR Bi OR Po OR At OR Rn OR Fr OR Ra OR Ac OR Th OR Pa OR U OR Np OR Pu OR Am OR Cm OR Bk OR Cf OR Es OR Fm OR Mv OR No OR Lr))
Result
No. of matching entries 186
Name Formula Entry No.
Fe2 O3 96-210-1169
and 186 others...
Peak List
No. 2theta [°] d [Å] I/I0 FWHM Matched
Diffraction Pattern Graphics
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Publication
Biblio graph y
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite structure", American Mineralogist 51, 123-129 (1966)
Origin of data
Sourc e of entry
COD (Crystallography Open Database)
Link
Crystal structure
Crystallographic data
Space
group R -3 c (167)
Cryst al syste
m
Diffraction data
Diffraction lines
d [Å] Int. h k l Mult.
Physical Properties
Calc. densi ty
5.25600 g/cm³
Match! Phase Analysis Report
Sample: 93%millscale+7%femo ts 1250
Sample Data
Filename 93%millscale+7%femo ts 1250.ras File path d:\xrd\93%millscale+7%femo-ts 1250\ Data collected 12/05/2016 10:34:52
Data range 20.000° to 90.000°
Number of points 7000
Step size 0.010
Alpha2 subtracted No
Background subtr. No
Data smoothed Yes
Radiation Cu-Ka
Wavelength 1.541874 Å
Retrieval
No. of matching entries 21
Name Formula Entry No.
Fe2 O3 96-210-1169
and 21 others...
Peak List
Match! Copyright © 2003-2011 CRYSTAL IMPACT, Bonn, Germany
Entry # 96-900-0140
Phase classification
Name
Publication
Biblio graph y
Blake R. L., Hessevick R. E., Zoltai T., Finger L. W., "Refinement of the hematite structure", American Mineralogist 51, 123-129 (1966)
Origin of data
Sourc e of entry
COD (Crystallography Open Database)
Link
Crystal structure
Crystallographic data
Space
trigonal (hexagonal axes)
coord
Diffraction data
Diffraction lines
d [Å] Int. h k l Mult.
Physical Properties
Calc. densi ty
5.25600 g/cm³
