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PENGARUH PERBEDAAN PERENDAMAN DAN KONSENTRASI LIQUEUR CENGKEH (Syzygium aromaticum L.) TERHADAP KANDUNGAN ANTIOKSIDAN PADA SORBET

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38

7.

LAMPIRAN

Lampiran 1. Proses Perendaman Cengkeh

(a)

(b)

(c)

Gambar 11. Perendaman Cengkeh Menggunakan Air Panas Sekitar 80

o

C (a), Campuran

Alkohol dan Air (b),

Basic Spirit

Alkohol 95% (c)

(2)

Lampiran 2. Scoresheet Uji Sensori Sorbet Liqueur Cengkeh

Nama

:

Tanggal :

Produk

: Sorbet

Liqueur

Cengkeh (A) / (B)

Atribut

: Rasa, aroma, tekstur,

overall

Instruksi

:

Berkumur-kumurlah dulu sebelum menguji sampel

Di hadapan anda terdapat 4 sampel

sorbet

. Tulislah terlebih dahulu kode sampel secara

berurutan dari kiri ke kanan. Cicipi sampel secara berurutan dari kiri ke kanan. Setelah

mencicipi semua sampel, Anda boleh mengulang sesering yang Anda perlukan. Urutkan

skor sampel dari rasa, aroma, tekstur dan

overall

(1= sangat tidak suka, 2= sedikit suka, 3=

suka, 4= sangat suka). Jawaban boleh dobel

Terima Kasih

(3)

Lampiran 3. Hasil Analisa Pengolahan SPSS

a.

Analisa Sensori Kruskal Wallis

b.

Analisa Sensori Mann Whitney

Cara A 5% - A 10%

Cara A 5% - A 15%

Cara A 5% - B 5%

(4)

Cara A 5% - B 15%

Cara A 10% - A 15%

Cara A 10% - B 5%

Cara A 10% - B 10%

(5)

Cara A 15% - B 5%

Cara A 15% - B 10%

Cara A 15% - B 15%

Cara B 5% - B 10%

(6)

Descriptive Statistics

Dependent Vari able: hardness

2380.653 34.367851 6 1532.683 49.943945 6 907.74667 16.503545 6 1607.028 622.038659 18 699.25500 8.342248 6 502.53833 5.004096 6 310.83333 17.464788 6 504.20889 163.534050 18 3812.950 189.311867 6 3812.950 189.311867 6 1539.954 878.405310 12 1017.611 539.038990 12 609.29000 312.148495 12 3812.950 189.311867 6 1449.523 1181.752301 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Tests of Between-Subjects Effects

Dependent Variable: hardnes s

57057145.8a 6 9509524.306 1656.442 .000 116922427 1 116922426.8 20366.441 .000 10945885.5 1 10945885.52 1906.638 .000 5222817.008 2 2611408.504 454.875 .000 1787928.296 2 893964.148 155.717 .000 200932.749 35 5740.936 145504972 42 57258078.6 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .996 (Adjus ted R Squared = .996) a.

Cara B 10% - B 15%

c.

Hasil Analisa Hardness

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(7)

hardness Duncana,b ,c 18 504.20889 18 1607.028 6 3812.950 1.000 1.000 1.000 formula

sorbet form ula B sorbet form ula A sorbet kontrol Sig.

N 1 2 3

Subset

Means for groups in hom ogeneous subsets are displayed. Based on Type III Sum of Squares

The error term is Mean Square(Error) = 5740.936. Us es Harm onic Mean Sample Size = 10.800. a.

The group s izes are unequal. The harm onic mean of the group s izes is used. Type I error levels are not guaranteed. b. Alpha = .05. c. ha rdn ess Duncana,b ,c 12 609.29000 12 1017.611 12 1539.954 6 3812.950 1.000 1.000 1.000 1.000 persentase 15% 10% 5% kontrol Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = 5740.936. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b.

Alpha = .05.

c. Tests of Between-Subjects Effects

Dependent Variable: viskositas

3728.004a 6 621.334 2753.309 .000 19285.508 1 19285.508 85459.613 .000 850.500 1 850.500 3768.809 .000 344.786 2 172.393 763.924 .000 .775 2 .388 1.718 .194 7.898 35 .226 20591.549 42 3735.903 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .998 (Adjus ted R Squared = .998) a.

Descriptive Statistics

Dependent Vari able: vis kosi tas

26.07500 .620862 6 20.75667 .301971 6 18.34000 .315468 6 21.72389 3.350077 18 16.03167 .194568 6 10.97000 .880500 6 9.00667 .424531 6 12.00278 3.092860 18 39.05167 .100681 6 39.05167 .100681 6 21.05333 5.263271 12 15.86333 5.149306 12 13.67333 4.887201 12 39.05167 .100681 6 20.03310 9.545658 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

d.

Hasil Analisa Viskositas

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(8)

viskositas Duncana,b ,c 18 12.00278 18 21.72389 6 39.05167 1.000 1.000 1.000 formula

sorbet form ula B sorbet form ula A sorbet kontrol Sig.

N 1 2 3

Subset

Means for groups in hom ogeneous subsets are displayed. Based on Type III Sum of Squares

The error term is Mean Square(Error) = .226. Us es Harm onic Mean Sample Size = 10.800. a.

The group s izes are unequal. The harm onic mean of the group s izes is used. Type I error levels are not guaranteed. b. Alpha = .05. c. viskositas Duncana,b ,c 12 13.67333 12 15.86333 12 21.05333 6 39.05167 1.000 1.000 1.000 1.000 persentase 15% 10% 5% kontrol Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = . 226. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b.

Alpha = .05.

c. Tests of Between-Subjects Effects

Dependent Variable: timetomelt

897.216a 6 149.536 906.155 .000 124008.516 1 124008.516 751464.8 .000 157.461 1 157.461 954.178 .000 76.241 2 38.120 231.001 .000 3.105 2 1.552 9.407 .001 5.776 35 .165 130803.503 42 902.991 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .994 (Adjus ted R Squared = .993) a.

Descriptive Statistics

Dependent Vari able: tim etom elt

57.75833 .298959 6 55.63000 .374967 6 54.87000 .420904 6 56.08611 1.304639 18 54.03667 .466205 6 51.81500 .391242 6 49.85833 .357962 6 51.90333 1.797685 18 65.32667 .499466 6 65.32667 .499466 6 55.89750 1.979119 12 53.72250 2.025542 12 52.36417 2.643635 12 65.32667 .499466 6 55.61357 4.692993 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

e.

Hasil Analisa Time to Melt

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(9)

timetomelt Duncana,b ,c 18 51.90333 18 56.08611 6 65.32667 1.000 1.000 1.000 formula

sorbet form ula B sorbet form ula A sorbet kontrol Sig.

N 1 2 3

Subset

Means for groups in hom ogeneous subsets are displayed. Based on Type III Sum of Squares

The error term is Mean Square(Error) = .165. Us es Harm onic Mean Sample Size = 10.800. a.

The group s izes are unequal. The harm onic mean of the group s izes is used. Type I error levels are not guaranteed. b.

Alpha = .05. c.

tim eto mel t

Duncana,b ,c 12 52.36417 12 53.72250 12 55.89750 6 65.32667 1.000 1.000 1.000 1.000 persentase 15% 10% 5% kontrol Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = . 165. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b.

Alpha = .05. c.

Descriptive Statistics

Dependent Vari able: pH

5.45333 .022509 6 5.51000 .014142 6 5.57667 .021602 6 5.51333 .055094 18 6.82500 .015166 6 6.90667 .010328 6 6.96500 .015166 6 6.89889 .060477 18 6.50500 .023452 6 6.50500 .023452 6 6.13917 .716563 12 6.20833 .729481 12 6.27083 .725252 12 6.50500 .023452 6 6.24881 .659894 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Tests of Between-Subjects Effects

Dependent Variable: pH 17.842a 6 2.974 9090.010 .000 1514.837 1 1514.837 4630505 .000 17.278 1 17.278 52814.474 .000 .104 2 .052 159.113 .000 .001 2 .000 1.486 .240 .011 35 .000 1657.854 42 17.854 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .999 (Adjus ted R Squared = .999) a.

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

f.

Hasil Analisa pH

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(10)

Descriptive Statistics

Dependent Vari able: brix

18.66667 .816497 6 20.68333 .453505 6 22.13333 .647045 6 20.49444 1.587255 18 19.41667 .491596 6 20.45000 .441588 6 22.25000 .437035 6 20.70556 1.279003 18 17.75000 .524404 6 17.75000 .524404 6 19.04167 .752521 12 20.56667 .443813 12 22.19167 .529937 12 17.75000 .524404 6 20.19286 1.668853 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Tests of Between-Subjects Effects

Dependent Variable: brix

103.220a 6 17.203 54.896 .000 15187.686 1 15187.686 48463.973 .000 .401 1 .401 1.280 .266 59.555 2 29.778 95.020 .000 1.491 2 .745 2.378 .108 10.968 35 .313 17239.750 42 114.188 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .904 (Adjus ted R Squared = .887) a. pH Duncana,b ,c 12 6.13917 12 6.20833 12 6.27083 6 6.50500 1.000 1.000 1.000 1.000 persentase 5% 10% 15% kontrol Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = . 000. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b. Alpha = .05. c. pH Duncana,b ,c 18 5.51333 6 6.50500 18 6.89889 1.000 1.000 1.000 formula

sorbet form ula A sorbet kontrol sorbet form ula B Sig.

N 1 2 3

Subset

Means for groups in hom ogeneous subsets are displayed. Based on Type III Sum of Squares

The error term is Mean Square(Error) = .000. Us es Harm onic Mean Sample Size = 10.800. a.

The group s izes are unequal. The harm onic mean of the group s izes is used. Type I error levels are not guaranteed. b.

Alpha = .05. c.

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

g.

Hasil Analisa Kadar Gula

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(11)

br ix

Duncan

a,b ,c

6

17.75000

18

20.49444

18

20.70556

1.000

.387

formula

sorbet kontrol

sorbet form ula A

sorbet form ula B

Si g.

N

1

2

Subset

Means for groups in homogeneous subs ets are displayed.

Based on Type III S um of S quares

The error term is M ean Square(Error) = .313.

Us es Harm onic Mean S am ple S ize = 10.800.

a.

The group sizes are unequal. The harmonic mean

of the group siz es i s us ed. Type I error l evel s are

not guaranteed.

b.

Al pha = .05.

c.

brix Duncana,b ,c 6 17.75000 12 19.04167 12 20.56667 12 22.19167 1.000 1.000 1.000 1.000 persentase kontrol 5% 10% 15% Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = . 313. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b.

Alpha = .05.

c. Tests of Between-Subjects Effects

Dependent Variable: antioksidan

383.378a 6 63.896 1211.227 .000 151943.253 1 151943.253 2880259 .000 171.304 1 171.304 3247.273 .000 71.912 2 35.956 681.590 .000 1.677 2 .838 15.893 .000 1.846 35 .053 169523.893 42 385.224 41 Source Corrected Model Intercept formula persentase formula * persentas e Error Total Corrected Total

Type III Sum

of Squares df Mean Square F Sig.

R Squared = .995 (Adjus ted R Squared = .994) a.

Descriptive Statistics

Dependent Vari able: antioks idan

60.04833 .159301 6 62.08500 .225455 6 63.92500 .260058 6 62.01944 1.642156 18 65.01667 .194594 6 66.07833 .168572 6 68.05167 .203019 6 66.38222 1.306146 18 59.01167 .343419 6 59.01167 .343419 6 62.53250 2.600161 12 64.08167 2.094069 12 65.98833 2.166530 12 59.01167 .343419 6 63.45952 3.065242 42 persentase 5% 10% 15% Total 5% 10% 15% Total kontrol Total 5% 10% 15% kontrol Total formula

sorbet form ula A

sorbet form ula B

sorbet kontrol

Total

Mean Std. Deviati on N

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

h.

Aktivitas Antioksidan

Uji

Two Ways

(Signifikansi - Beda Nyata / Tidak )

(12)

Correl ations 1.000 .985** .952** -.980** . .000 .000 .000 42 42 42 42 .985** 1.000 .954** -.977** .000 . .000 .000 42 42 42 42 .952** .954** 1.000 -.950** .000 .000 . .000 42 42 42 42 -.980** -.977** -.950** 1.000 .000 .000 .000 . 42 42 42 42 Correlation Coefficient Sig. (2-tailed) N Correlation Coefficient Sig. (2-tailed) N Correlation Coefficient Sig. (2-tailed) N Correlation Coefficient Sig. (2-tailed) N vis kositas hardness

tim etom elt

ak t.ant ioks idan Spearm an's rho

vis kositas hardness tim etom elt

ak t. antioks idan

Correlation is s ignificant at t he 0.01 level (2-t ailed). **.

antioksidan

Duncan

a,b ,c

6

59.01167

18

62.01944

18

66.38222

1.000

1.000

1.000

formula

sorbet kontrol

sorbet form ula A

sorbet form ula B

Sig.

N

1

2

3

Subset

Means for groups in hom ogeneous subsets are displayed.

Based on Type III Sum of Squares

The error term is Mean Square(Error) = .053.

Us es Harm onic Mean Sample Size = 10.800.

a.

The group s izes are unequal. The harm onic mean of the

group s izes is used. Type I error levels are not guaranteed.

b.

Alpha = .05.

c.

an tioksida n Duncana,b ,c 6 59.01167 12 62.53250 12 64.08167 12 65.98833 1.000 1.000 1.000 1.000 persentase kontrol 5% 10% 15% Sig. N 1 2 3 4 Subset

Means for groups in hom ogeneous s ubs ets are displayed. Based on Type III S um of S quares

The error term is M ean Square(E rror) = . 053. Us es Harm onic Mean S ample S ize = 9.600. a.

The group sizes are unequal. The harmonic m ean of t he group siz es is used. Ty pe I error levels are not guaranteed.

b.

Alpha = .05. c.

Post Hoc – Duncan (Berdasarkan Cara Pembuatan

Liqueur

)

Post Hoc – Duncan (Berdasarkan Konsentrasi Penambahan

Liqueur

)

(13)

Lampiran 4. Hasil Analisa Kadar Alkohol di Universitas Gadjah Mada,

Yogyakarta (Laboratorium Penelitian dan Pengujian Terpadu)

(14)

Gambar

Gambar  11.    Perendaman  Cengkeh  Menggunakan  Air  Panas  Sekitar  80 o C  (a),  Campuran   Alkohol  dan Air (b), Basic Spirit Alkohol 95% (c)

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