ATOM INDONESIA
Author's Responses
Article : #473
Name of All Authors : Meri Suhartini1*, J. Ginting2, Sudirman,2, Atika Dania P.3
Article Title : STUDY OF CELLULOSE- N,N'-METHYLENE BISACRYLAMIDE - ACRYLATE ACID AS Pb2+ ADSORBENT
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Line # Referee’s Comments Author's Responses
3
The word of “Simultaneous method”in the title, seems has no meaning either in the introduction or in the discussion, and considering the journal scope it is better to be changed such as “using gamma irradiation method”
Revised
24
&
65
The citation must be put before point such as “[1]
.[1]”
Revised
52 The citation jumped from [2] to [11] and the conta maching with the statement. Please rearrange and r
Revised
53-55 There are no reference no 33-41. The total referen 27.
Revised
58 There is no scheme 2. Please add it 65
Revised
65 There is no reference no
Revised 66-72,
182, 429
The sentences are ambiguous.
Revised
70-80 The reference (No [4]) is no maching (wrong).
Revised
104 The reference (No [4]) is no maching (wrong). It d straw
Revised
104 The insulation of cellulose must state clearly espe hemicelluloce from the rice straw. Otherwise, the l many functional groups will be observed from FTI
Revised
109,11 9, and so on
Experimental method must be discribed using pas tense.
Revised
117 An effort has been done to remove residual mono but no effort has been taken to remove the homopo author
Revised
125 &
152
Please add the equation number. Revised 191 There is no legend for copolymer B in Figure 1. Revised
197
Which one is righ, with increasing the radiation doses, the grafting of copolymer A dan B
increased linearly or logarithmic? increased logarithmic
211- 214
What the evident (data or references) for the statement of:
“Increased percentage of grafting copolymer A and B obtained is different because amount of radicals formed, radical position, availability and diffusion of monomer and gel formation.”
References added
246
Give deferent mark/color in the figure 2 for
cellulose and coplymer B. Original data from DSC cannot be changed
266
It the peak at 550˚C for copolymer A
endothermic? It is contradiciton with the figure
and previous explanation. revised
270 It must be thermal properties instead of properties
thermal. Thermal stability
299
It is said that “FTIR spectra cellulose-MBA-AA indicates the occurrence of crosslinking
N,N'-methylenebisacrylamide (MBA) and grafting from acrylic acid because it appears that there are no peaks in the FTIR spectra pure cellulose.”
How did the crosslinking and grafting reactions happen? As consequnecy of the reaction, some functional groups may disappear and make a new chemical bond (new functional
group).
How about the existance of polyacrilic acid homopolymer which have not been removed.
polyacrilic acid homopolymer completely removed
422 Fig 6. The Y axis was double value??? revised
478
It is said that “The fig.8 indicates that the optimum adsorption of Pb is 90.28% at neutral (pH ± 7). ..”
However, tt is contradiction with Fig. 6 where the adsorption of Pb could reach more than
98%. How it can be explaned.
90, 28% on 3 ppm 99,87% on 10 ppm Miss explanation
483 Where does the sulfur atom come from? (NH4)2SO4 buffer 629 What is the “unsur” in Table 2? Element...revised
666
Please recheck all references. Some references were not used, some others were not listed and some others also were cited incorrectly. It is fatal error!!!
Use only the recent (up to date) references
revised
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