Total = (100%) - Undip Repository

(1)

Judul Karya Ilmiah : Alkaloids piperine in dichloromethane fraction of red galangal rizhome (Alpinia purpurata)

Jumlah Penulis : 3 Orang

Status Pengusul : Penulis ke-1

Identitas Prosiding : a. Judul Prosiding : IOP Conference Series: Materials Science and Engineering, 13th Joint Conference on Chemistry (13th JCC)

b. ISBN/ISSN : Online ISSN: 1757-899X, Print ISSN: 1757-8981 c. Thn Terbit, Tempat Pelaks. : 2019, Semarang, Indonesia

d. Penerbit/Organiser : IOP Publishing Ltd

e. Alamat Repository/Web : https://iopscience.iop.org/article/10.1088/1757- 899X/509/1/012076

Alamat Artikel : https://iopscience.iop.org/article/10.1088/1757- 899X/509/1/012076/pdf

f. Terindeks di (jika ada) : Scopus Kategori Publikasi Makalah : √ ProsidingForum Ilmiah Internasional (beripada kategori yang tepat) ProsidingForum Ilmiah Nasional Hasil PenilaianPeer Review:

Komponen Yang Dinilai

Nilai Reviewer

Nilai Rata- Reviewer I Reviewer II rata

a. Kelengkapan unsur isi prosiding (10%) 2,50 2,90 2,70

b. Ruang lingkup dan kedalaman pembahasan (30%) 8,00 8,20 8,10

c. Kecukupan dan kemutahiran data/informasi dan metodologi (30%)

8,50 8,50 8,50

d. Kelengkapan unsur dan kualitas terbitan/prosiding(30%) 8,50 8,70 8,60

Total = (100%) 27,50 28,30 27,90

Nilai Pengusul = (60% x 27,90) = 16,74

Reviewer 2

Prof. Dr. Heri Sutanto, S.Si., M.Si.

NIP. 197502151998021001 Unit : Dep. Fisika, FSM UNDIP

Reviewer 1

Prof. Dr. Hadiyanto, S.T., M.Sc.

NIP. 197510281999031004

Unit Kerja : Teknik Kimia FT UNDIP Semarang, 17 April 2020

(2)

Judul Karya Ilmiah Jumlah Penulis Status Pengusul Identitas Prosiding

Alkaloids piperine in dichloromethane fraction of red galangal rizhome (Alpinia purpurata)

3 Orang Penulis ke-1 a. Judul Prosiding

b.

C. d.

e.

f.

ISBN/ISSN

Thn Terbit, Tempat Pelaks.

Penerbit/Organiser Aiamat Repository/Web Alamat Artikel

Terindeks di (jika ada)

IOP Conference Series: Materials Science and Engineering, 13th Joint Conference on Chemistry (13th JCC)

Online ISSN: 1757-899:X, Print ISSN: 1757-8981 2019, Semarang, Indonesia

IOP Publishing Ltd

https://1opsdence.1op.orgtartlcie1io. i 6ssii 1s1- 899X/509/1/012076

https://iopscience.iop.org/article/10.1088/l 757- 899X/509/I/0 12076/pdf

Scopus Kategofi PutiliKasi Muahili

(beri ✓ pada kategori yang tepat) : [I] Prosidiiig Forum Ilmiali Iiitemasionfil

D

^ProsidingForum Ilmiah Nasional Hasil Penilaian Peer Review

b. Ruang lingkup dan kedalaman pembahasan c. Kecukupan dan kemutahiran data/infonnasi dan30%

metodoio i 30%

d. Kelengkapan unsur dan kualitas

terbit 30%

Total =

Nilai Maksimal Prosiding internasionai Nasionai

0

3,00 9,00

9,00 9,00

Semarang, Reviewer 1

Prof. Dr. Hadiyanto, S. T., M.Sc.

NIP. 197510281999031004

Nilai Akhir Vang Diperoleb

11

Unit Kerja : Tekttilc Kjmit\ FT UNPW

(3)

Judul Karya Ilmiah : Alkaloids piperine in dichloromethane fraction of red galangal rizhome (Alpinia purpurata)

Jumlah Penulis : 3 Orang Status Pengusul : Penulis ke-1

Identitas Prosiding : a. Judul Prosiding : IOP Conference Series: Materials Science and Engineering, 13th Joint Conference on Chemistry (13th JCC)

b. ISBN/ISSN : Online ISSN: 1757-899X, Print ISSN: 1757-8981 c. Thn Terbit, Tempat Pelaks. : 2019, Semarang, Indonesia

d. Penerbit/Organiser : IOP Publishing Ltd

e. Alamat Repository/Web : https://iopscience.iop.org/article/10.1088/1757- 899X/509/1/012076

Alamat Artikel : https://iopscience.iop.org/article/10.1088/1757- 899X/509/1/012076/pdf

f. Terindeks di (jika ada) : Scopus Kategori Publikasi Makalah : √ Prosiding Forum Ilmiah Internasional (beri pada kategori yang tepat) Prosiding Forum Ilmiah Nasional Hasil Penilaian Peer Review :

Nilai Maksimal Prosiding Nilai Akhir Yang Diperoleh Internasional Nasional

a. Kelengkapan unsur isi prosiding (10%) 3,00 2,9

b. Ruang lingkup dan kedalaman pembahasan (30%)

9,00 8,2

c. Kecukupan dan kemutahiran data/informasi dan metodologi (30%)

9,00 8,5

d. Kelengkapan unsur dan kualitas terbitan/prosiding(30%)

9,00 8,7

Catatan Penilaian Paper oleh Reviewer : 1. Kesesuaian dan kelengkapan unsur isi paper:

Artikel telah ditulis secara lengkap dari judul hingga referensi dan sesuai dengan template penulisan IOP Conference Series:

Materials Science and Engineering 2. Ruang lingkup dan kedalaman pembahasan:

Ruang lingkup dan kedalaman pembahasan pada artikel sudah baik. Beberapa hasil penelitian UV Vis, FTIR dan NMR telah diungkapkan dengan jelas

3. Kecukupan dan kemutakhiran data/informasi dan metodologi:

Data penelitian yang diuraikan dalam artikel memadai dan relevan dengan judul artikel dan sesuai dengan metodologi penelitian yang dilakukan. Referensi pendukung artikel masih minim yaitu total 9 buah dan 3 kategori kurang mutakhir.

4. Kelengkapan unsur dan kualitas terbitan:

Kualitas artikel yang diterbitkan IOP Conference Series: Materials Science and Engineering baik dan konsisten serta terindeks Scopus, SJR 0.192 (2018) . Artikel telah direview dengan baik.

Prof. Dr. Heri Sutanto, S.Si., M.Si.

NIP. 197502151998021001 Unit : Dep. Fisika, FSM UNDIP

Total = (100%) 30,00 28,3

Nilai Pengusul = (60% x 28,30)= 16.98

Semarang, Reviewer 2

(4)

Document details

4 of 22

Alkaloids piperine in dichloromethane fraction of red galangal rizhome (Alpinia purpurata)

(Conference Paper) (Open Access)

, ,

Department of Chemistry, Faculty of Science and Mathematics, Diponegoro University, Semarang, 50267, Indonesia

Abstract

Red galangal rizhome (Alpiniapurpurata) was extracted with dichloromethane using maceration methods. The crude extract was fractionated using vacuum column chromatography with a mixture of ethyl acetate:n-hexane (2:3) to give two fractions (F1 and F2). Fraction 2 was fed into the silica gel of column chromatography tailed by recrystallization to produce crystalline (17 mg). The purity was tested by using melting point apparatus and thin-layer chromatography method for any solvent. Their structures were established by spectroscopic methods (UV-Vis, FTIR, H-NMR and C- NMR). Result of analysis gave melting point of crystals around 130°C. The UV-Vis spectrometer obtained maximum wavelength 344 nm. FTIR analysis showed C=O carbonyl, C-O ether, C-N, and C=C aromatic. Analysis by H-NMR spectrometer showed that bioactive compounds have a 19 protons. Analysis by C-NMR spectrometer showed that bioactive compounds have a 17 carbon atoms. The results of identiﬁcation showed that bioactive compounds in dichloromethane fraction of red galangal rhizome was a compound piperine alkaloids types with a chemical formula of C H O N. © 2019 Published under licence by IOP Publishing Ltd.

SciVal Topic Prominence

Topic:

Prominence percentile: 88.289

Author keywords

alkaloids Alpinia purpurata Piperine red galangal rizhome

Indexed keywords

Engineering controlled terms:

Alkaloids Dichloromethane Hexane Magnetic resonance spectrometers Melting point Metabolites Silica Silica gel Spectroscopic analysis Thin layer chromatography

Engineering uncontrolled terms

Alpinia purpurata Bioactive compounds Chemical formulae NMR spectrometer Piperine red galangal rizhome Spectroscopic method UV-vis spectrometer

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IOP Conference Series: Materials Science and Engineering Volume 509, Issue 1, 3 May 2019, Article number 012076

13th Joint Conference on Chemistry, JCC 2018; Semarang; Indonesia; 7 September 2018 through 8 September 2018; Code 147746

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13 ^th Joint Conference on Chemistry

7-8 September 2018

Semarang, Indonesia

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3

Preface

On behalf of the Consortium of Chemistry Department in Central Java, Indonesia and the JCC Committee, I would like to thank you for your participation in the 13th Joint Conference on Chemistry which to be held from 7-8^th September 2018 in Semarang, Indonesia. The Joint Conference on Chemistry is an annual conference organized by the consortium of Chemistry Department of five universities in Central Java: Diponegoro University (UNDIP), State University of Semarang (UNNES), Sebelas Maret University (UNS), Jenderal Soedirman University (UNSOED) and Satya Wacana Christian University (UKSW). The JCC has been held since 2006.

This conference provides an interactive international forum to provide for sharing and exchange information on the latest research on Chemistry and related sciences, to enhance the capacities for creating innovation system, to contribute in the formulation of global strategies in advancing science role as well as developing policy initiatives in community, to stimulate future collaborations among industries, researchers, governments and other stakeholders who apply science and technology for better live. The speakers and participants of the 13^th JCC are up to 250 coming from various countries extending from Indonesia, Malaysia, Philippine, Australia, South Korea, Japan, Iran, Nigeria, UK and India.

We received nearly 200 papers submitted to be included in the proceedings of this conference and after the review and revision process we finally got 158 papers to be published

I would like to thank for the endeavour of committee from Chemistry Department - UNDIP and the consortium member. In addition, the conference committee acknowledges the technical and financial support from Diponegoro University.

Adi Darmawan, Ph.D

The Chair of 13^th Joint Conference of Chemistry

Chemistry Department, Faculty of Science and Mathematics, Diponegoro University

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4

Committee

Chairman : Adi Darmawan, PhD (Diponegoro University, Semarang, Indonesia) Secretary : Yayuk Astuti, M.Si (Diponegoro University, Semarang, Indonesia)

Treasurer : Dr. Choiril Azmiyawati, M.Si (Diponegoro University, Semarang, Indonesia) Program : Dr. Agustina L. N. Aminin, M.Si (Diponegoro University, Semarang, Indonesia)

Nor Basid Adiwibawa Prasetya, Ph.D (Diponegoro University, Semarang, Indonesia) Scientific : M. Alauhdin, PhD (Universitas Negeri Semarang, Indonesia)

Hartiwi Diastuti, S.Si., M.Si (Universitas Jenderal Soedirman, Indonesia) Dr. Soerya Dewi Marliyana, S.Si.,M.Si. (Sebelas Maret University, Indonesia)

November Rianto Aminu, S.Si., M.Sc (Universitas Kristen Satyawa Wacana, Indonesia)

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5

Advisory Board

1. Dr. Lidija Siller (Newcastle University, UK) 2. Dr. Mehrorang Ghaedi (Yasouj University, Iran) 3. Dr. Ratna Balgis (Hiroshima University, Japan)

4. Dr. Simon Kane Smart (The University of Queensland, Australia) 5. Prof. Eiji Osawa (NanoCarbon Research Institute, Japan)

6. Prof. Fadzilah Adibah Abdul Majid (Universiti Malaysia Terengganu, Malaysia)

7. Prof. Insung S. Choi (KAIST - Korea Advanced Institute of Science and Technology, Korea) 8. Prof. Rizwan Hasan Khan (Aligarh Muslim University, Aligarh, India)

9. Dr. Dwi Hudiyanti, M.Sc (Diponegoro University, Semarang, Indonesia) 10. Dr. Ismiyarto (Diponegoro University, Semarang, Indonesia)

11. Dr. Khairul Anam (Diponegoro University, Semarang, Indonesia)

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Documentation

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The 13th Joint Conference on Chemistry 2018

7 September 2018 07:30 - 8 September 2018 17:30, Semarang, Indonesia

Analytical Catalysis Chemical Biology & Medicinal Education Energy Environmental Food General Interest Human Health Industry Inorganic Materials Nanoscience Organic Physical

Introduction

The Joint Conference on Chemistry is an annual conference organized by the consortium of Chemistry Department of five universities in Central Java, Indonesia : Diponegoro University (UNDIP), Universitas Negeri Semarang (UNNES), Sebelas Maret University (UNS), Jenderal Soedirman University (UNSOED) and Satya Wacana Christian University (UKSW). The conference will be a chemistry related disciplinary event considering all the major areas of chemistry, including inorganic, physical, organic, analytical and biochemistry. This conference also presents topics on chemical education, policies, and many other interesting topics. Interfaces with other sciences and other research areas will be actively encouraged.

Deadlines

07

Jun 2018

Further event details

More information about the event

Speakers

Dr. Simon Smart

The University of Queensland, Indonesia https://energy.uq.edu.au/profile/156/simon-smart

Dr. Lidija Siller

Newcastle University, United Kingdom

http://www.ncl.ac.uk/nanolab/staff/profile/lidijasiller.html#background

Prof. Insung S. Choi

KAIST - Korea Advanced Institute of Science and Technology, South Korea http://cisgroup.kaist.ac.kr/people.html

Emiritus Prof. Eiji Osawa

Shinshu University, NanoCarbon Research Institute, Japan https://www.scopus.com/authid/detail.uri?authorId=24374637300

Dr. Mehrorang Ghaedi Yasouj University, Iran, Iran

https://www.scopus.com/authid/detail.uri?authorId=9844537900

Venue

Hotel Santika Premiere Semarang

Borobudur Ballroom , Hotel Santika Premiere Semarang, Jalan Pandanaran No. 116 - 120, Pekunden, Semarang, 50134, Indonesia

Useful links

Venue information

More information about the venue

Committee

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https://www.rsc.org/events/detail/31514/the-13th-joint-conference-on-chemistry-2018 3/5 Yayuk Astuti, Ph.D

Diponegoro University, Indonesia http://jcc.undip.ac.id/23/yayuk-astuti.conf

Nor Basid Adiwibawa Prasetya, Ph.D Diponegoro University, Indonesia

https://jcc.undip.ac.id/22/nor-basid-adiwibawa-prasetya.conf

Dr. Choiril Azmiyawati

Diponegoro University, Indonesia

http://jcc.undip.ac.id/21/choiril-azmiyawati.conf

Dr. Agustina L. N. Aminin Diponegoro University, Indonesia

http://jcc.undip.ac.id/20/agustina-l-n-aminin.conf

Organised by

Chemistry Department of Diponegoro University

Chemistry Department of Universitas Negeri

Semarang

Chemistry Department of Sebelas Maret University

Chemistry Department of Jenderal Soedirman

University

Chemistry Department of Satya Wacana Christian

University

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PAPER • OPEN ACCESS

Alkaloids piperine in dichloromethane fraction of red galangal rizhome ( Alpinia purpurata )

Meiny Suzery , Resti Yuyun Septembe Ria and Bambang Cahyono

Published under licence by IOP Publishing Ltd

IOP Conference Series: Materials Science and Engineering, Volume 509, 13th Joint Conference on Chemistry (13th JCC) 7–8 September 2018, Semarang, Indonesia

Abstract

Red galangal rizhome (Alpiniapurpurata) was extracted with dichloromethane using maceration methods. The crude extract was fractionated using vacuum column

chromatography with a mixture of ethyl acetate:n-hexane (2:3) to give two fractions (F1 and F2). Fraction 2 was fed into the silica gel of column chromatography tailed by

recrystallization to produce crystalline (17 mg). The purity was tested by using melting point apparatus and thin-layer chromatography method for any solvent. Their structures were

more, see our Privacy and Cookies policy. 

1 1 1

[email protected]

Department of Chemistry, Faculty of Science and Mathematics, Diponegoro University, Semarang Indonesia 50267

Meiny Suzery et al 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012076 https://doi.org/10.1088/1757-899X/509/1/012076

Buy this article in print

1

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Corrosion inhibitory properties of La Ca MnO -gold nanoparticles in 1 M HCl

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Department of Chemistry, Covenant University, Ota, Ogun State, Nigeria.

Department of Pure and Applied Chemistry, University of Calabar, Cross River State, Nigeria Applied Magnetism Institute, UCM-ADIF-CSIC, 28230, Las Rozas, Spain.

Abiola-Edobor Osoh et al 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012039 https://doi.org/10.1088/1757-899X/509/1/012039

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Abstract

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[email protected] [email protected]

Nanoscience Research Laboratory, School of Chemical Sciences, Universiti Sains Malaysia, 11800 Penang, Malaysia

Laboratory of Reactions and Process Engineering, Université de Lorraine, UMR CNRS, LRGP, 7274, 1 rue Grandville, 54000 Nancy, France

Laboratoire de Chimie Physique Macromoléculaire, Université de Lorraine, CNRS, LCPM, ENSIC, 1 rue Grandville, BP 20451, F-54 000 Nancy, France

Asmaa Zainal Abidin et al 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012024 https://doi.org/10.1088/1757-899X/509/1/012024

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Enock Olugbenga Dare

Abstract

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[email protected]

Department of Chemistry, Covenant University, Canaan Land, Nigeria

Department of Biological Sciences, Covenant University, Canaan Land, Nigeria

Faculty of Chemistry and Pharmacy, Institute for Organic Chemistry, Regensburg University, Germany

Anuoluwa Abimbola Akinsiku et al 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012018 https://doi.org/10.1088/1757-899X/509/1/012018

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Muhammad Nur , Nelly Bonifaci , Andre Denat and Vlademir M. Atrazhev

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Center for Plasma Research, Faculty of Science and Mathematics, Diponegoro University, Semarang

Physics Department, Faculty of Science and Mathematics, Diponegoro University, Semarang G2E.Laboratory, CNRS and Joseph Fourier University 25 rue des Martyrs, 38042 Grenoble, France

Joint Institute for High Temperatures (JIHT and Russian Academy of Sciences, Izhorskaya St. 13, 2125412, Moscow, Russia

Muhammad Nur et al 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012084 https://doi.org/10.1088/1757-899X/509/1/012084

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Structural characterization of vanadium terpyridine complexes for the study of in-situ ligand cyclization reaction

Wan-Ting Jin and Zhao-Hui Zhou

Abstract

Vanadyl complex [V O(hmfc)(terpy)]3.5H O (1) (hmfc=5-hydroxy-3-methyl-2(5H)- furanone-5-carboxylate; terpy=2,2':6',2-terpyridine) has been isolated, which the hmfc ligand was formed through in-situ cyclization of lactate. X-ray structural analysis shows that hydroxyfuranone carboxylate chelates to vanadium through hydroxy group and carboxy

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[email protected]

State Key Laboratory of Physical Chemistry of Solid Surfaces; College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005 (China) Tel.: +86 592 2184531; Fax: +86 592 2183047

Wan-Ting Jin and Zhao-Hui Zhou 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012158 https://doi.org/10.1088/1757-899X/509/1/012158

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The effects of Sn infiltration on dry reforming of biogas at solid oxide fuel cell operating conditions over Ni-YSZ catalysts

Lina Troskialina and Robert Steinberger-Wilckens

Abstract

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Jurusan Teknik Kimia, Politeknik Negeri Bandung, Bandung, 40012, Jawa Barat, Indonesia Center for Fuel Cell and Hydrogen Research, School of Chemical Engineering, University of Birmingham, Birmingham, B15 2TT, United Kingdom

Lina Troskialina and Robert Steinberger-Wilckens 2019 IOP Conf. Ser.: Mater. Sci. Eng. 509 012064

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Document details

Alkaloids piperine in dichloromethane fraction of red galangal rizhome (Alpinia purpurata)

Source details

IOP Conference Series: Materials Science and Engineering

0.53

0.192

0.531

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0.53

CiteScoreTracker 2019

0.56

CiteScore rank

13 th Joint Conference on Chemistry

7-8 September 2018

Semarang, Indonesia

Preface

Committee

Advisory Board

Documentation

The 13th Joint Conference on Chemistry 2018

7 September 2018 07:30 - 8 September 2018 17:30, Semarang, Indonesia

Introduction

Deadlines

07

07

07

07

14

Useful links

Speakers

Venue

Hotel Santika Premiere Semarang

Useful links

Committee

Organised by

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Table of contents

Preface

Papers

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Volume 509

2019

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13th Joint Conference on Chemistry (13th JCC) 7–8 September 2018, Semarang, Indonesia

Accepted papers received: 08 March 2019 Published online: 03 May 2019

13th Joint Conference on Chemistry (13th JCC)

Peer review statement

Preparation of Cu(II) ion-imprinted based on carboxymethyl chitosan and application as adsorbent of Cu(II) ion

of PP composite

Phytochemicals screening and anti-oxidant activity of hydroethanolic extracts of Ruellia tuberosa L

Momordica charantia stem extract mediated biogenic synthesis of silver nanoparticles:

optical and antimicrobial efficacy

Room temperature phytosynthesis of silver nanoparticles using leaf extract of Momordica charantia: optical and antimicrobial properties

The influence of hydrogen peroxide concentration on catalytic activity of fenton catalyst@bacterial cellulose

The influence of chitosan concentration on morphology and conductivity of lithium aluminium titanate phosphate for solid electrolytes of lithium-ion battery application

Synthesis of surfactant modified activated carbon (SMAC) from rice husks as Ni(II) and Cr(VI) adsorbent

Influence of the synthesis parameters on the properties of natural rubber grafted poly-3- hydroxybutyrate

Analysis of piperine content in cabe jawa extracts (Piper retrofractum Vahl) using UV spectrophotometry and HPLC

The effects goat milk yoghurt casein on malondialdehyde (MDA) level of rats (Rattus norvegicus) exposured by 2,3,7,8 tetrachlorodibenzo-p-dioxin (TCCD)

Degradation of Congo Red in batik wastewater using fenton reagent under visible rays

Synthesis of silica gel from glass waste for adsorption of Mg , Cu , and Ag metal ions

4H-chromenes and their antibacterial and antioxidant activity

Cholesterol implications on coconut liposomes encapsulation of beta-carotene and vitamin C

Effect of kalium hydroxide/fly ash ratio and hydrothermal temperature in Zeolite W formation by X-ray diffraction analysis

Corrosion inhibitory properties of La Ca MnO -gold nanoparticles in 1 M HCl

Synthesis, morphological, optical properties of functionalized La Ca MnO for antibacterial therapy

Catalytic transformation of 1,8-cineole from Cajeput oil to p-cymene with modified zeolite beta catalyst

Synthesis and characterizations of nZVI-AC composites from coconut shells and its

application for the adsorption of Pb(II) and Cr(VI) ions

Synthesis of polymer hybrid latex polystyrene methylmethacrylate-co-butylacrylate with

organo-montmorillonite as filler through miniemulsion polymerization for barrier paper application

Surface modification of montmorillonite by the use of organic cations via conventional ion exchange method

Capability of immobilised glucoamylase on mesostructured cellular foam silica to hydrolyse tapioca starch

Mesostructured cellular foam MCF-(9.2T-3D) silica as support for free α-amylase in liquefaction of tapioca starch

Effect of drying treatments on the contents of lutein and zeaxanthin in orange- and yellow- cultivars of marigold flower and its application for lutein ester encapsulation

Synthesis and characterization of Cu(II) and Co(II) encapsulated metal complexes in zeolite-Y for the oxidation of phenol and benzene

13 ^th Joint Conference on Chemistry