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An update on pre-clinical implications of silk-based TEVGs

Introduction and review of literature

1.2 Review of literature

1.2.5 Silk biomaterials for vascular tissue engineering applications .1 Silk: varieties and molecular structure

1.2.5.3 An update on pre-clinical implications of silk-based TEVGs

which could pre-determine the immune response by means of fabricating ‘immune-informed’

tissue-engineered grafts.

 Highly porous grafts although showed better remodeling but their compromised strength, which potentially reduced their in vivo feasibility.

 Only low molecular weight SF grafts were mechanically stable till six months.

Plaiting and winding of silk fibers

Sprague- Dawley rats

Abdominal aorta

 No observed acute thrombosis for silk grafts.

 Silk graft showed superior patency rates than PTFE grafts over 1 year.

 Silk grafts showed early arrangement of intimal and medial layer. 12-week explants revealed almost confluent endothelium.

 Organization of medial layer was assisted by bone marrow derived cells.

 Presence of vasa vasorum like capillaries were detected.

 No sign of aneurysm formation.

 Macrophage assisted graft degradation over extended time.

[189]

Braiding and winding of natural and recombinant silk fibers

Sprague- Dawley rats

Abdominal aorta

 Excellent patency (85%).

 Signs of neo-tissue formation along the lumen.

 Presence of organized SMC layer and mature endothelium.

 Recombinant grafts (modified to express collagen active sites) showed faster transanastomotic ingrowth of CD31 positive cells compared with control grafts comprised of domestic BM silk fibers.

[190]

Transgenic SF braiding grafts

Sprague- Dawley rats

Abdominal aorta

 Signs of thrombus formation in occluded grafts.

 No sign of intimal hyperplasia.

 Superior endothelialization in central portion of transgenic SF grafts than wild type.

[191]

Double-

raschel knitted silk TEVGs

Sprague- Dawley rats

Abdominal aorta

 Tunable elasticity and thickness of scaffold wall by manipulating knitting pattern.

 Suitable patency and no sign of intimal hyperplasia.

 PGDE crosslinking and aqueous SF coating endow adequate permeability comparable with medical grade PTFE grafts.

 No significant difference in tissue ingrowth after 2 and 8 weeks, signifying slower degradation of scaffold.

[192]

Fibroin sponge coated double-

raschel knitted silk TEVGs

Beagle dogs

Common carotid artery

 No acute thrombosis.

 Sonography observation of 1-year implant suggested signs of intimal plaque formation at the middle and proximal anastomotic portion of the graft.

 Sponge layer was completely replaced with fibrous tissue in 1-year explants.

 Minimal detection of foreign body giant cells, substantiating immune compatibility.

[193]

Fibroin sponge coated double-

raschel knitted silk TEVGs

Sprague- Dawley rats

Abdominal aorta

 Silk grafts coated with lower SF concentration (1-2.5% w/v) sponge facilitate constructive remodeling and prevent intimal hyperplasia/stenosis.

 Significantly improved tissue infiltration in 1-2.5% SF coated grafts.

 Complete degradation of sponge and replacement with host tissue.

[194]

Double-

raschel knitted TEVGs (SF and PE splice grafts)

Beagle dogs

Abdominal aorta

 SF coating assist in rapid endothelialization and prevent medial thickening.

 Thrombus formation in gelatin coated grafts.

 SF coated grafts had thinner luminal layer compared with gelatin coated ones.

 Higher ECs observed in SF coated silk fiber grafts.

[195]

Elastin modified double-

raschel knitted SF grafts

Rats Abdominal aorta

 Elastin coating facilitates ECs’ attachment while prevent platelets adhesion.

 Very good patency.

 No sign of excessive immune response or fibrous capsule formation.

 Rapid endothelialization within 2 weeks of implantation.

[196]

Plaited silk fibers and cocoon filaments coated with SF solution

Beagle dogs

Carotid artery

 Dismal patency possibly due to lost mechanical strength by virtue of degradation.

 Limited remodeling in large animals.

 3-months data revealed superior endothelialization of silk graft compared with PTFE ones.

[197]

Braided SF threads

C57BL/6 mice

Right carotid artery

 ~13% (4/30) patency after 6 months.

 2-week explants showed presence of SMA and CD31 positive cells in neointimal.

 Complete endothelialization at 4 weeks.

 Significant presence of collagen and elastin fibers after 4 weeks.

 Signs of SF degradation at 6 months.

[140]

Silk fabric core layer embedded in a porous

scaffold

Rabbits Common carotid artery

 No sign of stenosis and aneurysmal dilation.

 Complete endothelialization in 3 months.

 Blood flow profile was comparable with native artery.

 Organized medial layer comprising of SMCs substantiating constructive graft remodeling.

[198, 199]

Double-

raschel knitted silk TEVGs

Sprague- Dawley rats

Inferior vena cava

 95% patency for silk grafts, 80% patency for ePTFE grafts over 4 weeks.

 Full lumen coverage by ECs in 4 weeks.

 Podoplanin-positive mesothelial cells were traced on the outer surface of graft.

[200]

Electrospun silk TEVG

Lewis rats

Abdominal aorta

 No sign of thrombus formation.

 Good short-term patency.

 Infiltration of host vascular cells observed in explant.

[201]

 Newly developed elastic lamina along the graft lumen.

 Notable presence of vasa vasorum at the outer scaffold surface.

Electrospun silk TEVGs

Sprague- Dawley rats

Abdominal aorta

 Graft survival at 24 weeks: 95% (20/21) silk grafts, 73% (16/22) ePTFE grafts.

 Rapid endothelialization in 6 weeks.

 Regression of neointimal was also observed.

 Constructive remodeling over time in terms of new ECM deposition, minimal number of inflammatory cells and reduction in granulation tissue.

[202]

Tri-layered SF/PCL composite electrospun TEVGs

Sprague- Dawley rats

Right carotid artery

 Good patency.

 Significant infiltration of host vascular cells.

[203]

Bi-layered SF/PLCL composite electrospun TEVGs

Rabbit Carotid artery

 Good patency.

 Graft remodeling and infiltration of host vascular cells.

 Loss of mechanical strength over time.

[204]

Electrospun silk TEVGs (aqueous and HFP based)

Sprague- Dawley rats

Abdominal aorta

 HFP grafts performed better than aqueous grafts.

 No sign of aneurysm formation.

 Neointimal regression over time.

 HFP grafts facilitated faster contractile phenotype transition of SMCs.

 Increased ECM production in HFP grafts.

[205]

Tri-layered silk TEVG (inner/outer electrospun layer, an intermediate woven layer)

Minipig and Sheep

Carotid artery

 The study identified that sheep would be suitable option for a long-term pre-clinical trial.

 Grafts were easy to handle during surgery and showed adequate suture retention.

 Pre-seeding of cells is not required for SilkGraft.

[154]

Composite electrospun

Rabbit Left carotid artery

 Graft degradation and neo-tissue formation.

[206]

PLCL grafts coated with silk/heparin

 Remarkable patency.

 No sign of intimal thickening.

 Minimal inflammation resulting from biomaterial degradation.

 Discontinuous endothelialization after 2 months.

Composite silk-

polyurethane (Silkothane) graft for haemodialysis

Sheep Arterioven ous shunt

 Implantation between external jugular vein and common carotid artery.

 No graft related complications.

 8/9 sheep: 100% primary patency.

 Signs of initial inflammation and infiltration of ECs.

 Overall 100% patency.

[207]

While prior literature suggests the predominant use of Bombyx mori silk for vascular tissue engineering applications, present thesis work explores the non-mulberry silk varieties. In addition, various innovative approaches are demonstrated to improve the in situ remodeling and clinical feasibility of silk-based TEVGs.

MOTIVATION AND OBJECTIVES