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Universitas Sumatera Utara

Lampiran 1.Spesifikasi GC-MS RTX-5MS

C:\GCMSsolution\Data\Project1\Rtx 5 MS 2019\Jeremi 1.qgd

Lab Kimia Flow Control Mode :Pressure

Pressure :13.0 kPa

Total Flow :79.3 mL/min

Column Flow :0.55 mL/min Linear Velocity :26.8 cm/sec

Purge Flow :3.0 mL/min

Split Ratio :139.0

High Pressure Injection :OFF Carrier Gas Saver :OFF

Splitter Hold :OFF

Oven Temp. Program

Rate Temperature(°C) Hold Time(min)

- 50.0 5.00

5.00 240.0 7.00

< Ready Check Heat Unit >

Column Oven : Yes

SPL1 : Yes

MS : Yes

5. Ready Check Detector(FTD) >

6. Ready Check Baseline Drift >

7. Ready Check Injection Flow >

SPL1 Carrier : Yes

SPL1 Purge : Yes

< Ready Check APC Flow >

< Ready Check Detector APC Flow >

External Wait :No Solvent Cut Time :3.00 min Detector Gain Mode :Absolute

Lampiran. 2 Hasil Identifikasi Spesies dari daun Eucalyptus Citriodora

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Lampiran 3. Alat Stahl Destilation

3.1 Lampiran Penyulingan destilasi Air

3.2 Lampiran Penyulingan Pada Suhu 80-900C

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Lampiran 4. Gas Chromatography – Mass Spectrofotometry

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Lampiran 5. Data hasil Analisa GC-MS Minyak Atsiri dari daun Eucalyptus Citriodora

C:\GCMSsolution\Data\Project1\Rtx 5 MS 2019\Jeremia Sitohang 1.qgd

Lab.Kimia Organik FMIPA - UGM

Sample Information Analyzed by : Admin

Sample Name : Jeremia Sitohang 1

Sample ID :

Data File : C:\GCMSsolution\Data\Project1\Rtx 5 MS 2019\Jeremi 1.qgd Method File : C:\GCMSsolution\Data\Project1\Rtx 5 MS 2019\Atsiri.qgm Tuning File : C:\GCMSsolution\System\Tune1\nopember 18 2017.qgt

Chromatogram Jeremi 1 C:\GCMSsolution\Data\Project1\Rtx 5 MS 2019\Jeremi 1.qgd

1,424,435 3

9325810 100.00 2674108

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65

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Universitas Sumatera Utara

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