Bulletin of Chemical Reaction Engineering and Catalysis

(1)

LEMBAR

HASIL PENILAIAN SEJAWAT SEBIDANG ATAU PEER REVIEW KARYA ILMIAH : JURNAL ILMIAH

Judul Karya Ilmiah (Artikel) : Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3

Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

Jumlah Penulis : 5 Orang Penulis ke : 1

Nama Penulis : Yayuk Astuti*, Prisca Putri Elesta, Didik Setyo Widodo, Hendri Widiyandari, Ratna Balgis

Identitas Jurnal Ilmiah

a. Nama Jurnal : Bulletin of chemical reaction engineering & catalysis

b. Nomor ISSN : 1978-2993

c. Volume, No, Bulan, Tahun : 15, 1, Februari, 2020

d. Penerbit : Department of Chemical Engineering, Diponegoro University e. DOI artikel (jika ada) : https://doi.org/10.9767/bcrec.15.1.5483.104-111

f. Alamat web jurnal : https://ejournal2.undip.ac.id/index.php/bcrec/article/view/5483 g. Indexing : Scopus, Schimago JR, Publons, DOAJ

Kategori Publikasi Jurnal Ilmiah : Jurnal Ilmiah Internasional / Internasional Bereputasi (beri pada kategori yang tepat) Jurnal Ilmiah Nasional Terakreditasi

Jurnal Ilmiah Nasional/Nasional Terindeks di DOAJ, CABI Hasil Penilaian Peer Review :

Komponen Yang Dinilai

Nilai Maksimal Jurnal Ilmiah = 40 Nilai

Akhir Yang Diperoleh Internasional

Bereputasi Internasional Nasional Terakreditasi

Nasional Tidak Terakreditasi

Nasional Terindeks DOAJ dll.

a. Kelengkapan unsur isi buku

(10%) 4 4

b. Ruang lingkup dan kedalaman

pembahasan (30%) 12 12

c. Kecukupan dan kemutahiran data/informasi dan metodologi (30%)

12 11

d. Kelengkapan unsur dan kualitas

penerbit (30%) 12 11

Total = (100%) 40 38

Kontribusi Pengusul (Penulis Anggota)

Komentar Peer Review:

a. Kelengkapan dan kesesuaian unsur: Lengkap dan sesuai dengan yang dipersyaratkan jurnal internasional. Artikel yang dimuat, dibahas dan disusun secara lengkap

b. Ruang lingkup dan kedalaman pembahasan: Ruang lingkup penelitian ini tentang sintesis Bi2O3 dan aplikasinya. Data yang disajikan dibahas dengan detil dan lengkap, disertai referensi pendukung

c. Kecukupan dan kemutahiran data/informasi dan metodologi: Kualitas dan kuantitas pustaka baik.

Metodologi disajikan detil sehingga bisa diulang peneliti lain.

d. Kelengkapan unsur dan kualitas penerbit: Kualitas terbitan baik dan masuk dalam Q3, hanya ada beberapa gambar yang kurang jelas.

e. Indikasi Plagiasi: tidak ada

f. Kesesuaian bidang ilmu: sesuai dengan bidang kimia

Semarang, Reviewer 1

Drs. Gunawan, M.Si., Ph.D NIP. 196408251991031001 Unit kerja :

Departemen Kimia FSM Undip Jabatan Fungsional:

Lektor Kepala



60%x38

=22,8

(2)

LEMBAR

Judul Karya Ilmiah (Artikel) : Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

Nama Penulis : Yayuk Astuti, Prisca Putri Elesta, Didik Setyo Widodo, Hendri Widiyandari, Ratna Balgis

d. Penerbit : Department of Chemical Engineering, Diponegoro University e. DOI artikel (jika ada) : https://doi.org/10.9767/bcrec.15.1.5483.104-111

Nilai Maksimal Jurnal Ilmiah = 40

Nilai Akhir Yang Diperoleh Internasional

Bereputasi Internasional Nasional Terakreditasi

Nasional Tidak Terakreditasi

Nasional Terindeks DOAJ dll.

a. Kelengkapan unsur isi buku

(10%) 4 4

b. Ruang lingkup dan kedalaman pembahasan (30%)

12 12

c. Kecukupan dan

kemutahiran data/informasi dan metodologi (30%)

12 11

d. Kelengkapan unsur dan

kualitas penerbit (30%) 12 12

Total = (100%) 40 39

Kontribusi Pengusul

(Penulis Anggota) 60%x40=24 60%x39=23,4

Komentar Peer Review:

a. Kelengkapan dan kesesuaian unsur: Unsur kelengkapan artikel telah terpenuhi, terdiri dari pendahuluan, metode, hasil dan pembahasan, kesimpulan dan referensi

b. Ruang lingkup dan kedalaman pembahasan: : Ruang lingkup adalah sintesis senyawa anorganik, pembahasan cukup mendalam dan telah menggunakan data pembanding.

Bagian pendahuluan cukup detail.

c. Kecukupan dan kemutahiran data/informasi dan metodologi:

Jumlah data memadai dan 17 dari 39 referensi merupakan referensi terkini.

d. Kelengkapan unsur dan kualitas penerbit: Penerbitan Departemen Teknik Kimia Universitas Diponegoro berkualitas baik, dan telah terindeks oleh scopus.

e. Indikasi Plagiasi: Tidak ada

f. Kesesuaian bidang ilmu: Sesuai dengan bidang ilmu kimia

Semarang, Reviewer 2



Lektor Kepala Jabatan Fungsional:

Departemen Kimia FSM Undip Unitkerja :

NIP. 197007021996031004 Dr.M.Cholid Djunaedi,S.Si,M.Si.

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LEMBAR

Nilai Reviewer

Nilai Rata-rata Reviewer I Reviewer II

a. Kelengkapan unsur isi buku (10%)

4 4 4

b. Ruang lingkup dan kedalaman pembahasan

(30%) ¹² ¹²

12 c. Kecukupan dan kemutahiran data/informasi

dan metodologi (30%) ¹¹ ¹¹

11 d. Kelengkapan unsur dan kualitas penerbit

(30%) ¹¹ ¹²

11,5

Total = (100%) 38 39 38,5

Kontribusi Pengusul (Penulis Anggota) 60%x38,5=23,1

Semarang, April 2020 Reviewer 2

Dr. M. Cholid Djunaedi,. S.Si., M.Si.

NIP. 197007021996031004 Unit kerja :

Departemen Kimia FSM Undip

Reviewer 1

Drs. Gunawan, M.Si., Ph.D NIP. 196408251991031001 Unit kerja :



(4)

LEMBAR

Nilai Maksimal Jurnal Ilmiah

Nilai Akhir Yang Diperoleh Internasional /

Internasional Bereputasi **

a. Kelengkapan unsur isi buku (10%) 4 4

b. Ruang lingkup dan kedalaman pembahasan (30%)

12 12

c. Kecukupan dan kemutahiran

data/informasi dan metodologi (30%)

12 11

d. Kelengkapan unsur dan kualitas penerbit (30%)

12 11,5

Total = (100%) 40 38,5

Kontribusi Pengusul (Penulis Anggota) 60%x38,5=23,1

Semarang, April 2020 Reviewer 2

Dr. M. Cholid Djunaedi,. S.Si., M.Si.

NIP. 197007021996031004 Unit kerja :

Reviewer 1

Drs. Gunawan, M.Si., Ph.D

NIP. 196408251991031001 Unit kerja :

Departemen Kimia FSM Undip 40



(5)

CiteScore

1.6

⁼

Calculated on 06 May, 2020

CiteScoreTracker 2020

1.9

⁼

Last updated on 07 September, 2020 • Updated monthly

Source details

Open Access

Bulletin of Chemical Reaction Engineering and Catalysis

Scopus coverage years: from 2009 to Present Publisher: Diponegoro University

ISSN: 1978-2993

Subject area: Chemical Engineering: Chemical Engineering (miscellaneous)

Chemical Engineering: Process Chemistry and Technology Chemical Engineering: Catalysis

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CiteScore 2019

1.6

^

SJR 2019

0.256

^

SNIP 2019

0.808

^

CiteScore CiteScore rank & trend Scopus content coverage

i Improved CiteScore methodology

CiteScore 2019 counts the citations received in 2016-2019 to articles, reviews, conference papers, book chapters and data papers published in 2016-2019, and divides this by the number of publications published in 2016-2019. Learn more▻

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2019 ^

390 Citations 2016 - 2019 241 Documents 2016 - 2019

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448 Citations to date 236 Documents to date

CiteScore rank 2019

Category Rank Percentile

Chemical Engineering

#17/25 34th

Chemical Engineering

#40/58 31st

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Chemical Engineering (miscellaneous)

Process Chemistry and

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Astuti, Yayuk

, Semarang, Indonesia Show all author info

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https://orcid.org/0000-0002-2107-3829 View Mendeley proﬁle

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30 Documents by author

177 Citations by documents

7 ^h-index: ^View^h^-graph

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Documents Citations

Most contributed Topics 2015-2021

Bismuth Oxides; Photocatalytic Activity; Solid Oxide Fuel Cells 10 documents

Iodine Value; Activated Carbon; Palm Kernels 2 documents

Nanoﬁltration Membranes; Pervaporation; Water Flux 2 documents

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Conference Paper • Open Access

, ,

, , ( ), View abstract

Photocatalytic Performance of Bismuth Oxide Prepared by Citric Acid-Fueled Solution Combustion on Decolorisation of Organic Dye Molecules

Astuti, Y. Anggraeni, D. Darmawan, A.

IOP Conference Series: Materials Science and Engineering View at Publisher Related documents

0

Cited by

, , , ,

, , ( ),

Vi b

The influence of high energy milling to the adsorption of Cd(II) and Zn(II) ions on activated zeolite

Pardoyo, P. Astuti, Y. Herinnayah, G. Suhartana, S. Wibawa, P.J.

Journal of Physics: Conference Series

0

Cited by

30 Documents Cited by 151 Documents 64 Co-Authors Topics Brought to you by Universitas Diponegoro

(7)

View abstract View at Publisher Related documents

Conference Paper

, , ,

, , , View abstract

Activation of carbon from rice husk using chemical activating agents and physical treatments as sodium lauryl sulfate adsorbent

Arnelli, Mastuti, L.N. Arini, A.D. Astuti, Y.

AIP Conference Proceedings

View at Publisher Related documents

0

Cited by

Article • Open Access

, , , ,

, , ( ), pp. - View abstract

Hydrazine and urea fueled-solution combustion method for bi2o3 synthesis:

Characterization of physicochemical properties and photocatalytic activity Astuti, Y. Elesta, P.P. Widodo, D.S. Widiyandari, H. Balgis, R.

Bulletin of Chemical Reaction Engineering & Catalysis View at Publisher Related documents

Cited by

1

, , , ,

The Role of H C O and Na CO as Precipitating Agents on the

Physichochemical Properties and Photocatalytic Activity of Bismuth Oxide

2 2 4 2 3

Astuti, Y. Andianingrum, R. Arnelli, A. Haris, A. Darmawan, A.

Open Chemistry

0

Cited by

, , , ... ,

Effect of fuels on the physicochemical properties and photocatalytic activity of bismuth oxide, synthesized using solution combustion method

Astuti, Y. Amri, D. Widodo, D.S. Balgis, R. Ogi, T.

International Journal of Technology

0

Cited by

, , ,

Studying impact of citric acid-bismuth nitrate pentahydrate ratio on photocatalytic activity of bismuth oxide prepared by solution combustion method

Astuti, Y. Fauziyah, A. Widiyandari, H. Widodo, D.S.

Rasayan Journal of Chemistry

Cited by

2

, , ,

Synthesis of surfactant modified activated carbon (SMAC) from rice husks as Ni(II) and Cr(VI) adsorbent

Arnelli, Wahyuningrum, V.N. Fauziah, F. Astuti, Y.

0

Cited by

, , ,

Synthesis of activated carbon/bismuth oxide composite and its characterization for battery electrode

Astuti, Y. Aprialdi, F. Arnelli, Haryanto, I.

0

Cited by

,

Synthesis, characterization and selectivity of molecularly imprinted polymer (MIP) glucose using polyeugenol as a functional polymer

Djunaidi, M.C. Astuti, Y.

Cited by

1

(8)

Document details

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Hydrazine and urea fueled-solution combustion method for bi2o3 synthesis:

Characterization of physicochemical properties and photocatalytic activity (Article) (Open Access)

, , , ,

Chemistry Department, Faculty of Sciences and Mathematics, Diponegoro University, Jl. Prof. Soedarto, Kampus Undip Tembalang, Semarang, 50275, Indonesia

Department of Physics, Faculty of Mathematics and Natural Sciences, University of Sebelas Maret, Jl. Ir Sutami No.

36A, Jebres, Surakarta, 57126, Indonesia

Department of Chemical Engineering, Faculty of Engineering, Hiroshima University, 141 Kagamiyama, Higashi- Hiroshima City Hiroshima, 7398527, Japan

Abstract

Bismuth oxide synthesis using solution combustion method fuelled by hydrazine and urea has been conducted. This study aims to examine the eﬀect of the applied fuels, urea and hydrazine, on product characteristics and photocatalytic activity in degrading rhodamine B dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate

pentahydrate (Bi(NO3)3.5H2O) in a nitric acid solvent. Fuel was added and then stirred. The solution formed was heated at 300°C for 8 hours. The product obtained was then calcined at 700°C for 4 hours. Bismuth oxide synthesized with urea (BO1) and hydrazine (BO2) as fuels both obtained form of yellow powder. The formation of bismuth oxide is indicated by the vibrations of the Bi-O-Bi and Bi-O groups and the crystal structure of α-Bi2O3 in both products.

Pho-tocatalytic activity test showed that BO1 has a photocatalyst activity in degrading rhodamine B higher than that of BO2 with constant values of 3.83×10 s and 3.43×10 s , respectively. The high photo-catalytic activity can be examined through several factors, such as: Band gap values, crystal structure, morphology, and surface area, acquired as a result of the use of diﬀerent fuels in the synthesis process. © 2020 BCREC Group.

SciVal Topic Prominence

Topic:

Prominence percentile: 95.337

Author keywords

Bismuth Oxide Fuels Photocatalysis Rhodamine B Solution Combustion

Indexed keywords

^Export ^Download ^Print ^E-mail  Save to PDF ⋆ Add to List ^More...▻

View at Publisher

Open Access Bulletin of Chemical Reaction Engineering & Catalysis

Volume 15, Issue 1, 1 April 2020, Pages 104-111

Astuti, Y.â  Elesta, P.P.â Widodo, D.S.â Widiyandari, H.^b Balgis, R.^c 

a

b

c

 View references (39)

-5 -1 -5 -1



Bismuth Oxides | Photocatalytic Activity | Solid Oxide Fuel Cells



Chemistry database information 

Substances

⤢

HO

O NH₂

⤢

O

OH O

N

N CH3

CH3

H3C H3C

Cl

⤢

H₂N NH₂

⤢

HO HO

O O OH

OH

O

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(2020) IOP Conference Series:

Materials Science and Engineering

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1.6

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10/20/2020 2020: BCREC Volume 15 Issue 1 Year 2020 (SCOPUS and Web of Science Indexed, April 2020)

https://ejournal2.undip.ac.id/index.php/bcrec/issue/view/522 6/10

(https://ejournal2.undip.ac.id/index.php/bcrec/article/view/5483)

Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

(https://ejournal2.undip.ac.id/index.php/bcrec/article/view/5483) Yayuk Astuti, Prisca Putri Elesta, Didik Setyo Widodo,

Hendri Widiyandari, Ratna Balgis Views: 662 (#) |

| Language: EN (#) | DOI: 10.9767/bcrec.15.1.5483.104-111 (https://doi.org/10.9767/bcrec.15.1.5483.104-111)

Received: 24 Jul 2019; Revised: 18 Oct 2019; Accepted: 19 Oct 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

(https://ejournal2.undip.ac.id/i

Activity Evaluation of CoMo Nanoparticles Supported on Meso-microporous Composites in Dibenzothiophene Hydrodesulphurization

(https://ejournal2.undip.ac.id/index.php/bcrec/article/view/5556) Nastaran Parsafard, Mohammad Hasan Peyrovi, Zahra

Mohammadian, Niloofar Atashi Views: 417 (#) |

Received: 3 Aug 2019; Revised: 21 Oct 2019; Accepted: 24 Oct 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

Characterization and Application of Molten Slag as Catalyst in Pyrolysis of Waste Cooking Oil

(https://ejournal2.undip.ac.id/index.php/bcrec/article/view/3973) Faten Hameed Kamil, Salmiaton Ali, Raja Mohamad Hafriz

Raja Shahruzzaman, Intesar Razaq Hussien, Rozita Omer Views: 436 (#) |

Received: 21 Dec 2018; Revised: 24 Oct 2019; Accepted: 26 Oct 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

Effect of Process Parameters on the Photocatalytic Degradation of Phenol in Oilﬁeld Produced Wastewater using ZnO/Fe2O3 Nanocomposites.

(https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6068) Omer Al Haiqi, Abdurahman Hamid Nour, Rushdi Bargaa,

Bamidele Victor Ayodele Views: 384 (#) |

| Language: ENGLISH (#) | DOI:

10.9767/bcrec.15.1.6068.128-136

(https://doi.org/10.9767/bcrec.15.1.6068.128-136)

Received: 8 Oct 2019; Revised: 5 Nov 2019; Accepted: 5 Nov 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

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10/21/2020 Catalytic Dehydration of Ethanol over W/TiO2 Catalysts Having Different Phases of Titania Support | Kerdnoi | Bulletin of Chemical Rea…

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Catalytic Dehydration of Ethanol over W/TiO2 Catalysts Having Different Phases of Titania Support

Pongsatorn Kerdnoi (https://scholar.google.com/scholar?q=Pongsatorn+Kerdnoi) - Center of Excellence on Catalysis and Catalytic Reaction Engineering, Department of Chemical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand

Chaowat Autthanit (https://scholar.google.com/scholar?q=Chaowat+Autthanit) - Center of Excellence on Catalysis and Catalytic Reaction Engineering, Department of Chemical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand

Nithinart Chitpong (https://scholar.google.com/scholar?q=Nithinart+Chitpong) - Department of Textile Engineering, Faculty of Engineering, Rajamangala University of Technology Thanyaburi, Thailand *Bunjerd Jongsomjit (https://scholar.google.com/scholar?q=Bunjerd+Jongsomjit)

(http://www.scopus.com/authid/detail.uri?authorId=6603065177) - Center of Excellence on Catalysis and Catalytic Reaction Engineering, Department of Chemical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand

(javascript:openRTWindow('https://ejournal2.undip.ac.id/index.php/bcrec/rt/emailAuthor/5606/0');) Received: 15 Aug 2019; Revised: 4 Oct 2019; Accepted: 4 Oct 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

DOI: https://doi.org/10.9767/bcrec.15.1.5606.96-103 (https://doi.org/10.9767/bcrec.15.1.5606.96-103)

License URL: http://creativecommons.org/licenses/by-sa/4.0 (http://creativecommons.org/licenses/by- sa/4.0)

How to cite (IEEE): P. Kerdnoi, C. Autthanit, N. Chitpong, and B. Jongsomjit, "Catalytic Dehydration of Ethanol over W/TiO2 Catalysts Having Different Phases of Titania Support," Bulletin of Chemical Reaction Engineering & Catalysis, vol. 15, no. 1, pp. 96-103, Apr. 2020.

https://doi.org/10.9767/bcrec.15.1.5606.96-103 (https://doi.org/10.9767/bcrec.15.1.5606.96-103) Citation Format: IEEE Download Citation

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Article Info

Section: Original Research Articles Language: EN (#)

In 2020: BCREC Volume 15 Issue 1 Year 2020 (SCOPUS and Web of Science Indexed, April 2020) (https://ejournal2.undip.ac.id/index.php/bcrec/issue/view/522)

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Abstract

This study aims to investigate the catalytic behaviors on W/TiO catalysts having different phases of TiO towards catalytic dehydration of ethanol to higher value products including ethylene, diethyl ether, and acetaldehyde. In fact, TiO support with different crystalline phases can result in

differences of physico-chemical properties of the catalyst. Therefore, the present work reports on the catalytic behaviors that were altered with different phases of TiO in catalytic ethanol dehydration to diethyl ether or ethylene as a major product. To prepare the catalysts, three different phases [anatase (A), rutile (R), and mixed phases (P25)] of TiO supports were impregnated with 10 wt% of tungsten (W). It was found that the W/TiO -P25 catalyst revealed higher activity among other catalysts. At 300

°C, all catalysts can produce the diethyl ether yield of 24.1%, 22.8%, and 10.6% for W/TiO -P25, W/TiO -A, and W/TiO -R catalysts, respectively. However, when the reaction temperature was increased to 400°C, ethylene is the major product. The W/TiO -P25 and W/TiO -A catalysts render the ethylene yield of 60.3% and 46.2%, respectively, whereas only 15.9% is obtained from W/TiO -R catalyst. The most important parameter in uencing their catalytic properties appears to be the proper pore structure, acidity, and distribution of W species. Copyright © 2019 BCREC Group. All rights reserved

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1. Sebayang, A., Masjuki, H., Ong, H.C., Dharma, S., Silitonga, A., Mahlia, T., Aditiya, H. (2016). A perspective on bioethanol production from biomass as alternative fuel for spark ignition engine, RSC Adv., 6, 14964-14992.

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chemistry, catalysts, and engineering, Chem. Rev., 106, 4044-4098.

3. Soh, J.C., Chong, S.L., Hossain, S.S., Cheng, C.K. (2017). Catalytic ethylene production from ethanol dehydration over non-modi ed and phosphoric acid modi ed Zeolite HY (80) catalysts, Fuel Process. Technol., 158, 85-95.

4. Alharbi, W., Brown, E., Kozhevnikova, E.F., Kozhevnikov, I.V. (2014). Dehydration of ethanol over heteropoly acid catalysts in the gas phase, J. Catal., 319, 174-181.

5. Kamsuwan, T., Praserthdam, P., Jongsomjit, B. (2017). Diethyl ether production during catalytic dehydration of ethanol over Ru-and Pt-modi ed H-beta zeolite catalysts, J. Oleo Sci., 66, 199- 207.

6. Lee, J., Szanyi, J., Kwak, J.H. (2017). Ethanol dehydration on g-Al2O3: effects of partial pressure and temperature, Mol. Catal., 434, 39-48.

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Keywords: ethanol dehydration; titania; tungsten; diethyl ether; ethylene Article Metrics:

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10/21/2020 Design, Characterization and Application of The SCMNPs@PC/VB1-Zn as A Green and Recyclable Biocatalyst for Synthesis of Pyrano[…

Hou (https://ejournal2.undip.ac.id/index.php/bcrec/article/view/6179/0)

Design, Characterization and Application of The

SCMNPs@PC/VB1-Zn as A Green and Recyclable Biocatalyst for Synthesis of Pyrano[2,3-c]pyrazole and 4H-benzo-[b]- pyran Derivatives

Fang Hou (https://scholar.google.com/scholar?q=Fang+Hou) - Jiyuan Vocational and Technical College, China

Wei Zheng (https://scholar.google.com/scholar?q=Wei+Zheng) - Jiyuan Vocational and Technical College, China

*Nasser Youse (https://scholar.google.com/scholar?q=Nasser+Youse ) - Islamic Azad University, Iran, Islamic Republic of

(javascript:openRTWindow('https://ejournal2.undip.ac.id/index.php/bcrec/rt/emailAuthor/6179/0');) Received: 26 Oct 2019; Revised: 3 Jan 2020; Accepted: 3 Jan 2020; Published: 1 Apr 2020; Available online: 28 Feb 2020.

DOI: https://doi.org/10.9767/bcrec.15.1.6179.199-212 (https://doi.org/10.9767/bcrec.15.1.6179.199- 212)

How to cite (IEEE): F. Hou, W. Zheng, and N. Youse , "Design, Characterization and Application of The SCMNPs@PC/VB1-Zn as A Green and Recyclable Biocatalyst for Synthesis of Pyrano[2,3- c]pyrazole and 4H-benzo-[b]-pyran Derivatives," Bulletin of Chemical Reaction Engineering &

Catalysis, vol. 15, no. 1, pp. 199-212, Apr. 2020. https://doi.org/10.9767/bcrec.15.1.6179.199-212 (https://doi.org/10.9767/bcrec.15.1.6179.199-212)

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Article Info

Section: Original Research Articles Language: EN (#)

Statistics: 547 (#) 257 (#)

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Abstract

Eco-friendly and reusable solid acid catalysts (SCMNPs@PC/VB -Zn) were identi ed as one of the most effective basic catalysts for the composition of a pot, three-component pyrano[2,3-c]pyrazoles.

Methyl-1-phenyl-1H-pyrazole-5(4H)-one, benzaldehyde and malononitrile in high yield at 80 °C.

SCMNPs@ PC/VB -Zn reports the simple and ef cient catalysis of a three-component pot reaction of dimedone, aldehydes, and malononitrile to 4H-benzo-[b]-pyran derivatives. This magnetic

Keywords: Recyclable biocatalyst; Magnetic nanocatalyst; Synthesis; Pyran derivatives; Eco-friendly Article Metrics:

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1. Utkan, G.G., Sayar, F., Batat, P., Ide, S., Kriechbaum, M., Pişkin, E. (2011). Synthesis and characterization of nanomagnetite particles and their polymer coated forms. Journal of colloid and interface science, 353(2), 372-379.

2. Park, J., An, K., Hwang, Y., Park, J.G., Noh, H.J., Kim, J.Y., Park, J.H., Hwang, N.M., Hyeon, T. (2004).

Ultra-large-scale syntheses of monodisperse nanocrystals. Nature materials, 3(12), 891-895.

3. Mizutani, N., Iwasaki, T., Watano, S., Yanagida, T., Tanaka, H., Kawai, T. (2008). Effect of ferrous/ferric ions molar ratio on reaction mechanism for hydrothermal synthesis of magnetite nanoparticles. Bulletin of Materials Science, 31(5), 713-717.

4. Morel, A.L., Nikitenko, S.I., Gionnet, K., Wattiaux, A., Lai-Kee-Him, J., Labrugere, C., Chevalier, B., Deleris, G., Petibois, C., Brisson, A., Simonoff,

5. M. (2008). Sonochemical approach to the synthesis of Fe3O4@SiO2 core− shell nanoparticles with tunable properties. ACS Nano, 2(5), 847-856.

6. Panella, B., Vargas, A., Baiker, A. (2009). Magnetically separable Pt catalyst for asymmetric hydrogenation. Journal of Catalysis, 261(1), 88-93.

7. Wei, Y., Han, B., Hu, X., Lin, Y., Wang, X., Deng, X. (2012). Synthesis of Fe3O4 nanoparticles and their magnetic properties. Procedia Engineering, 27, 632-637.

8. Shiri, L., Ghorbani-Choghamarani, A., Kazemi, M. (2016). Sul des synthesis: nanocatalysts in C–

S cross-coupling reactions. Australian Journal of Chemistry, 69(6), 585-600.

9. Kim, Y.S., Kim, Y.H. (2003). Application of ferro-cobalt magnetic uid for oil sealing. Journal of Magnetism and Magnetic Materials, 267(1), 105-110.

10. Ghorbani-Choghamarani, A., Norouzi, M. (2014). Synthesis of copper (II)-supported magnetic nanoparticle and study of its catalytic activity for the synthesis of 2,3-dihydroquinazolin-4(1H)- ones. Journal of Molecular Catalysis A: Chemical, 395, 172-179.

11. Hoener, C.F., Allan, K.A., Bard, A.J., Campion, A., Fox, M.A., Mallouk, T.E., Webber, S.E., White, J.M. (1992). Demonstration of a shell-core structure in layered cadmium selenide-zinc selenide small particles by x-ray photoelectron and Auger spectroscopies. The Journal of Physical Chemistry, 96(9), 3812-3817.

12. Yao, G.H., Wang, F., Wang, X.B., Gui, K.T. (2010). Magnetic eld effects on selective catalytic reduction of NO by NH3 over Fe2O3 catalyst in a magnetically uidized bed. Energy, 35(5), 2295-2300.

13. Ishii, M., Nakahira, M., Yamanaka, T. (1972). Infrared absorption spectra and cation distributions in (Mn, Fe)3O4. Solid State Communications, 11(1), 209-212.

14. Tartaj, P., Morales, M.P., Gonzalez-Carreño, T., Veintemillas-Verdaguer, S., Serna, C.J. (2011). The Iron Oxides Strike Back: From Biomedical Applications to Energy Storage Devices and Photoelectrochemical Water Splitting. Advanced Materials, 23, 5243-5249.

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10/23/2020 A Review Paper on Heterogeneous Fenton Catalyst: Types of Preparation, Modification Techniques, Factors Affecting the Synthesi…

Kumar (https://ejournal2.undip.ac.id/index.php/bcrec/article/view/4374/0)

A Review Paper on Heterogeneous Fenton Catalyst: Types of Preparation, Modiﬁcation Techniques, Factors Affecting the Synthesis, Characterization, and Application in the

Wastewater Treatment

Vijyendra Kumar (https://scholar.google.com/scholar?q=Vijyendra+Kumar) - Department of Chemical Engineering, National Institute of Technology Raipur, India

Titikshya Mohapatra (https://scholar.google.com/scholar?q=Titikshya+Mohapatra) - Department of Chemical Engineering, National Institute of Technology Raipur, India

Sandeep Dharmadhikari (https://scholar.google.com/scholar?q=Sandeep+Dharmadhikari) - Department of Chemical Engineering, National Institute of Technology Raipur, India

*Prabir Ghosh (https://scholar.google.com/scholar?q=Prabir+Ghosh) - Department of Chemical Engineering, National Institute of Technology Raipur, India

(javascript:openRTWindow('https://ejournal2.undip.ac.id/index.php/bcrec/rt/emailAuthor/4374/0');)

Received: 18 Feb 2019; Revised: 1 Sep 2019; Accepted: 10 Sep 2019; Published: 1 Apr 2020; Available online: 28 Feb 2020.

DOI: https://doi.org/10.9767/bcrec.15.1.4374.1-34 (https://doi.org/10.9767/bcrec.15.1.4374.1-34)

How to cite (IEEE): V. Kumar, T. Mohapatra, S. Dharmadhikari, and P. Ghosh, "A Review Paper on Heterogeneous Fenton Catalyst: Types of Preparation, Modi cation Techniques, Factors Affecting the Synthesis, Characterization, and Application in the Wastewater Treatment," Bulletin of Chemical Reaction Engineering & Catalysis, vol. 15, no. 1, pp. 1-34, Apr. 2020.

https://doi.org/10.9767/bcrec.15.1.4374.1-34 (https://doi.org/10.9767/bcrec.15.1.4374.1-34) Citation Format: IEEE Download Citation

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10/23/2020 A Review Paper on Heterogeneous Fenton Catalyst: Types of Preparation, Modification Techniques, Factors Affecting the Synthesi…

Article Info

Section: Review Articles Language: EN (#)

Statistics: 2074 (#) 1080 (#)

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Abstract

This comprehensive review focuses on the different factors, modi cation in the synthesis method, characterization and application of heterogeneous catalyst in the wastewater treatment based on the Fenton process. The present review highlights the different catalyst preparation methods like wet impregnation method, hydrothermal method, sol-gel method, precipitation method and their application to treat different recalcitrant organic chemicals. Major heterogeneous catalyst synthesis methods were discussed with their excellent workability. The importance of modi cation through physical and chemical method was also reported. Different catalyst, pollutants and optimum parametric conditions available in the literature along with some relevant studies are summarized.

The effect of factors like pH, calcination and some other modi ers on the synthesis and their ef ciency in the wastewater treatment has been described. The important characterization of

synthesized catalysts explaining their working ef ciency has also been discussed. In the nal section, the application of heterogeneous catalyst synthesized by different methods in the

wastewater/ef uent treatment has been investigated. The main aim of this review is to nd out the