34
Lampiran 1. Jadwal Pengambilan Sampel
Bulan Febuari 2007
Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28
Pengambilan dan
pengeringan sampel
Powder sampel dan kadar air
Destruksi sampel
Bulan Maret 2007
Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31
Pengambilan dan
pengeringan sampel
Powder sampel dan kadar air
Destruksi sampel
Bulan Apr-07
Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31
Pengambilan dan
pengeringan sampel
Powder sampel dan kadar air
Destruksi sampel
Bulan Mei-07
Tanggal 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31
Pengambilan dan
pengeringan sampel
Powder sampel dan kadar air
Destruksi sampel
Keterangan : Kodok Purwodadi
: Kodok Demak
: Kodok Semarang
36
Lampiran 2. Peta Lokasi Pengambilan Sampel
Lampiran 3. Hasil Pengukuran kadar air dan AAS
Pengukuran Kadar air Kodok (Pakai Tulang) Semarang
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel
kering Berat awal
Berat akhir
Kadar air
Paha 1 40,236 21,159 61,395 5,431 45,667 21,159 5,431 74,3324
Paha 2 40,253 35,63 75,883 6,703 46,956 35,63 6,703 81,1872
Paha 3 39,014 30,102 69,116 5,6 44,614 30,102 5,6 81,3966
Paha 4 46,769 31,375 78,144 6,134 52,903 31,375 6,134 80,4494
Paha 5 31,012 27,745 58,757 5,438 36,45 27,745 5,438 80,4001
Sisa 1 39,625 25,595 65,22 4,878 44,503 25,595 4,878 80,9416
Sisa 2 44,992 32,33 77,322 6,148 51,14 32,33 6,148 80,9836
Sisa 3 44,67 30,109 74,779 5,497 50,167 30,109 5,497 81,743
Sisa 4 43,74 33,741 77,481 6,778 50,518 33,741 6,778 79,9117
Sisa 5 33,521 28,777 62,298 5,32 38,841 28,777 5,32 81,513
Jeroan 1 47,772 2,364 50,136 0,474 48,246 2,364 0,474 79,9492
Jeroan 2 32,284 2,536 34,82 0,404 32,688 2,536 0,404 84,0694
Jeroan 3 42,297 2,712 45,009 0,508 42,805 2,712 0,508 81,2684
Jeroan 4 47,184 2,706 49,89 0,51 47,694 2,706 0,51 81,153
Jeroan 5 19,902 2,26 22,162 0,472 20,374 2,26 0,472 79,115
Avarage 20,6094 60,1608 43,57106667 20,6094 80,5609
38
Pengukuran Kadar air Kodok (Tanpa Tulang) Semarang
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel
kering Berat awal
Berat akhir
Kadar air
Paha 1 31,169 17,876 49,045 2,926 34,095 17,876 2,926 83,6317
Paha 2 33,548 15,515 49,063 2,493 36,041 15,515 2,493 83,9317
Paha 3 21,973 17,479 39,452 2,885 24,858 17,479 2,885 83,4945
Sisa 1 27,54 5,382 32,922 0,739 28,279 5,382 0,739 86,269
Sisa 2 32,695 5,231 37,926 0,718 33,413 5,231 0,718 86,2741
Sisa 3 19,315 5,142 24,457 0,683 19,998 5,142 0,683 86,7172
Jeroan 1 26,354 2,255 28,609 0,452 26,806 2,255 0,452 79,9557
Jeroan 2 28,366 2,976 31,342 0,522 28,888 2,976 0,522 82,4597
Jeroan 3 29,855 2,902 32,757 0,539 30,394 2,902 0,539 81,4266
Pengukuran Logam
Kodok (Pakai Tulang) Semarang
Kode
Berat
distruksi Volume dilution
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel
basah Dilution Zn (AAS)
Kadar Zn
Zn sampel
basah Dilution
Paha 1 1,682 5 1 74,332 0,08 0,059 0,0153 1,143 3,398 0,872 0,9 0,892 0,229
Paha 2 1,722 5 10 81,187 0,02 0,058 0,0109 0,741 2,152 0,405 2,1 4,355 0,819
Paha 3 1,688 5 81,397 0,08 0,237 0,0441 1,219 3,611 0,672 0,7 10,37 1,929 5
Paha 4 1,669 5 80,449 0,16 0,479 0,0937 2,95 8,838 1,728 1,1 16,48 3,221 5
Paha 5 1,724 5 80,4 0,21 0,435 0,0853 2,59 7,512 1,472 1,4 2,32 0,455
Sisa 1 1,713 5 80,942 0,39 0,788 0,1502 12,05 32,22 6,141 1,8 26,27 5,007 5
Sisa 2 1,776 5 80,984 0,37 0,732 0,1392 9,34 263 50 10 1,9 26,75 5,086 5
Sisa 3 1,706 5 81,743 0,44 1,114 0,2033 13,43 33,37 6,092 1,8 26,38 4,816 5
Sisa 4 1,7 5 79,912 0,69 1,765 0,3545 10,06 295,9 59,44 10 2,2 32,35 6,499 5
Sisa 5 1,76 5 81,513 1,3 3,125 0,5777 10,72 304,5 56,3 10 2,3 32,67 6,04 5
Jeroan 1 0,31 5 79,949 2,92 44,68 8,9582 3,309 53,37 10,7 0,7 56,45 11,32 5
Jeroan 2 0,345 5 84,069 3,2 22,46 3,5786 3,119 8,014 1,277 0,7 50,72 8,081 5
Jeroan 3 0,302 5 81,268 3,26 11,42 2,1399 2,547 9,321 1,746 1 82,78 15,51 5
Jeroan 4 0,314 5 81,153 3,31 51,59 9,7236 3,663 46,1 8,688 1,1 87,58 16,51 5
Jeroan 5 0,358 5 79,115 2,24 30,45 6,3588 2,462 34,39 7,181 0,8 55,87 11,67 5
Blanko 0,06 0,6
Sum 169,4 32,433 1106 212,7 512,2 97,18
Avarage 11,29 2,1622 73,71 14,18 34,15 6,479
40
Kodok (Tanpa Tulang) Semarang
Kode
Berat
distruksi Volume
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel basah
Zn (AAS)
Kadar Zn
Zn sampel
basah Dilution
Paha 1 1,158 5 83,632 0,12 0,259 0,0424 1,011 3,064 0,5 1,5 3,886 0,501
Paha 2 1,132 5 83,932 0,11 0,221 0,0355 2,14 4,163 0,67 0,6 13,251 0,669 5
Paha 3 1,184 5 83,494 1,34 5,659 0,934 2,044 146 24,1 0,6 12,669 24,1 5
Sisa 1 0,525 5 86,269 0,09 0,857 0,1177 2,957 246,4 33,8 1,1 4,7619 33,84
Sisa 2 0,531 5 86,274 0,2 1,883 0,2585 7,677 72,29 9,92 0,6 28,249 9,922 5
Sisa 3 0,521 5 86,717 0,15 0,864 0,1147 6,308 60,54 8,04 0,5 23,992 8,041 5
Jeroan 1 0,319 5 79,956 1,65 24,92 4,9954 2,566 40,22 8,06 0,6 47,022 8,062 5
Jeroan 2 0,31 5 82,46 2,57 40,48 7,101 1,984 32 5,61 0,5 40,323 5,613 5
Jeroan 3 0,315 5 81,427 0,07 0,159 0,0295 0,768 12,19 2,26 0,9 4,7619 2,264
Blanko 0,06 0 0,6
Sum 75,31 13,629 616,9 93 178,92 93,01
Avarage 8,367 1,5143 68,54 19,879 10,33
Pengukuran Kadar Air Kodok (Pakai Tulang) Demak
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel kering
Kadar air
Paha 1 42,29 42,686 84,976 7,403 49,693 82,6571
Paha 2 60,502 42,27 102,772 7,471 67,973 82,3255
Paha 3 44,681 42,456 87,137 7,455 52,136 82,4406
Paha 4 45,548 44,721 90,269 7,625 53,173 82,9498
Paha 5 50,077 45,472 95,549 8,62 58,697 81,0433
Sisa 1 39,63 32,418 72,048 5,985 45,615 81,538
Sisa 2 32,663 33,812 66,475 6,117 38,78 81,9088
Sisa 3 44,672 30,278 74,95 5,565 50,237 81,6203
Sisa 4 43,745 30,304 74,049 5,544 49,289 81,7054
Sisa 5 33,404 19,855 53,259 3,35 36,754 83,1277
Jeroan 1 47,779 2,174 49,953 0,384 48,163 82,3367
Jeroan 2 32,288 1,504 33,792 0,248 32,536 83,5106
Jeroan 3 42,304 1,117 43,421 0,18 42,484 83,8854
Jeroan 4 47,194 1,277 48,471 0,243 47,437 80,971
Jeroan 5 19,904 1,796 21,7 0,289 20,193 83,9087
Avarage 24,8093
42
Pengukuran Kadar Air Kodok (Tanpa Tulang) Demak
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel
kering Kadar air
Paha 1 31,083 11,151 42,234 1,72 32,803 84,5754
Paha 2 33,449 12,227 45,676 2,015 35,464 83,5201
Paha 3 21,9 11,905 33,805 1,901 23,801 84,0319
Sisa 1 27,509 4,564 32,073 0,522 28,031 88,5627
Sisa 2 44,998 4,429 49,427 0,696 45,694 84,2854
Sisa 3 19,304 4,772 24,076 0,651 19,955 86,3579
Jeroan 1 26,359 1,297 27,656 0,233 26,592 82,0355
Jeroan 2 28,368 1,487 29,855 0,267 28,635 82,0444
Jeroan 3 29,857 2,544 32,401 0,586 30,443 76,9654
Pengukuran Logam
Kodok (Pakai Tulang) Demak
Kode
Berat
distruksi Volume
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel basah
Zn (AAS)
Kadar Zn
Zn sampel
basah Dilution
Paha 1 1,681 5 82,6571 0,16 0,2974 0,0516 0,58 1,7252 0,2992 1,1 16,3593 2,8372 5
Paha 2 1,737 5 82,3255 0,17 0,4893 0,0865 1,01 2,9073 0,5139 1,1 15,8319 2,7982 5
Paha 3 1,721 5 82,4406 0,09 0,2615 0,0459 0,42 1,2202 0,2143 0,8 11,6212 2,0406 5
Paha 4 1,684 5 82,9498 0,1 0,1188 0,0202 0,67 1,9893 0,3392 1,3 7,71971 1,3162 2
Paha 5 1,655 5 81,0433 0,17 0,5136 0,0974 0,76 2,2961 0,4353 1,4 21,148 4,009 5
Sisa 1 1,646 5 81,538 0,09 0,2734 0,0505 1,07 3,2503 0,6001 1,1 6,68287 1,2338 2
Sisa 2 1,713 5 81,9088 0,09 0,0876 0,0158 2,6 6,1588 1,1142 0,9 13,1349 2,3763 5
Sisa 3 1,654 5 81,6203 0,2 0,6046 0,1111 0,94 0,9976 0,1834 1,9 28,7183 5,2783 5
Sisa 4 1,59 5 81,7054 0,13 0,4088 0,0748 0,58 0,0943 0,0173 0,9 14,1509 2,5889 5
Sisa 5 1,58 5 83,1277 0,14 0,2532 0,0427 0,55 0,538 0,0908 1,2 18,9873 3,2036 5
Jeroan 1 0,393 5 82,3367 1,99 24,555 4,3372 4,21 16,158 2,854 1,1 69,9746 12,36 5
Jeroan 2 0,253 5 83,5106 2,59 50 8,2447 3,85 76,087 12,546 1,1 108,696 17,923 5
Jeroan 3 0,183 5 83,8854 2,09 57,104 9,202 3,52 51,366 8,2774 0,6 81,9672 13,209 5
Jeroan 4 0,248 5 80,971 2,97 58,669 11,164 3,47 69,96 13,313 0,9 90,7258 17,264 5
Jeroan 5 0,258 5 83,9087 2,66 51,55 8,2951 3,15 61,047 9,8232 0,8 77,5194 12,474 5
Blanko 0,06 0,6
Sum 245,19 41,84 295,79 50,621 583,237 100,91
Avarage 16,346 2,7893 19,72 3,3747 38,8825 6,7275
44
Kodok (tanpa Tulang) Demak
Kode
Berat
distruksi Volume
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel basah
Zn (AAS)
Kadar Zn
Zn sampel
basah Dilution
Paha 1 1,482 5 84,5754 0,34 0,9447 0,1457 2,61 8,8057 1,3582 0,7 11,8084 1,8214 5
Paha 2 1,461 5 83,5201 0,47 1,4031 0,2312 2,48 8,4873 1,3987 0,8 13,6893 2,256 5
Paha 3 1,541 5 84,0319 0,53 1,7197 0,2746 0,49 1,5899 0,2539 0,8 12,9786 2,0724 5
Sisa 1 0,521 5 88,5627 0,16 1,5355 0,1756 0,61 5,8541 0,6696 1,2 57,5816 6,5858 5
Sisa 2 0,55 5 84,2854 0,21 1,9091 0,3 0,55 5 0,7857 1 45,4545 7,143 5
Sisa 3 0,51 5 86,3579 0,1 0,9804 0,1337 0,38 3,7255 0,5082 1 49,0196 6,6873 5
Jeroan 1 0,231 5 82,0355 3,45 74,675 13,415 2,94 63,636 11,432 0,8 86,5801 15,554 5
Jeroan 2 0,278 5 82,0444 1,45 26,079 4,6827 5,1 91,727 16,47 1,1 98,9209 17,762 5
Jeroan 3 0,25 5 76,9654 1,76 35,2 8,1082 1,64 32,8 7,5553 1 100 23,035 5
Blanko 0,06 0 0,6
Sum 752,379 8,47 144,45 27,467 221,63 40,432 476,033 82,916 45
avarage 16,05 3,0519 24,625 4,4924 0 52,8925 9,2129 5
Pengukuran Kadar Air Kodok (Pakai Tulang) Purwodadi
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel kering
Kadar air
Paha 1 40,226 40,566 80,792 10,263 50,489 74,7005
Paha 2 40,244 47,786 88,03 10,374 50,618 78,2907
Paha 3 44,653 44,462 89,115 10,341 54,994 76,7419
Paha 4 46,759 48,157 94,916 11,68 58,439 75,746
Paha 5 30,812 43,078 73,89 9,371 40,183 78,2464
Sisa 1 39,617 43,609 83,226 9,395 49,012 78,4563
Sisa 2 44,983 42,706 87,689 8,37 53,353 80,4009
Sisa 3 38,966 44,302 83,268 8,528 47,494 80,7503
Sisa 4 43,73 44,016 87,746 9,006 52,736 79,5393
Sisa 5 33,38 45,687 79,067 9,415 42,795 79,3924
Jeroan 1 47,765 3,322 51,087 0,605 48,37 81,7881
Jeroan 2 32,28 2,754 35,034 0,517 32,797 81,2273
Jeroan 3 42,29 2,856 45,146 0,512 42,802 82,0728
Jeroan 4 47,176 2,589 49,765 0,479 47,655 81,4986
Jeroan 5 19,891 2,045 21,936 0,389 20,28 80,978
46
Pengukuran Kadar Air Kkodok (Tanpa Tulang) Purwodadi
Kode
Berat cawan
Sampel basah
Berat cawan dan sampel basah
Sampel kering
Berat cawan dan sampel kering
Kadar air
Paha 1 31,054 11,613 42,667 2,112 33,166 81,8135
Paha 2 33,368 11,857 45,225 2,246 35,614 81,0576
Paha 3 21,881 12,512 34,393 2,538 24,419 79,7155
Sisa 1 27,491 3,655 31,146 0,5 27,991 86,3201
Sisa 2 32,646 3,048 35,694 0,431 33,077 85,8596
Sisa 3 19,29 2,706 21,996 0,375 19,665 86,1419
Jeroan 1 26,345 1,611 27,956 0,27 26,615 83,2402
Jeroan 2 28,352 1,245 29,597 0,179 28,531 85,6225
Jeroan 3 29,845 1,791 31,636 0,305 30,15 82,9704
Pengukuran Logam
Kodok (Pakai Tulang) Purwodadi
Kode
Berat
distruksi Volume
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel basah
Zn
(AAS) Kadar Zn
Zn sampel
basah Dilution
Paha 1 1,725 5 74,7005 0,17 0,319 0,0807 0,51 1,4783 0,374 0,6 8,695652 2,2 5
Paha 2 1,725 5 78,2907 0,17 0,493 0,107 0,46 1,3333 0,2895 0,7 10,14493 2,2024 5
Paha 3 1,661 5 76,7419 0,22 0,662 0,154 0,86 2,5888 0,6021 1,2 18,06141 4,2007 5
Paha 4 1,741 5 75,746 0,1 0,115 0,0279 0,5 1,436 0,3483 0,6 8,615738 2,0897 5
Paha 5 1,729 5 78,2464 0,26 0,752 0,1636 1,02 2,9497 0,6417 1,4 20,24291 4,4036 5
Sisa 1 1,7 5 78,4563 0,32 0,941 0,2028 2,77 6,9706 1,5017 1 14,70588 3,1682 5
Sisa 2 1,649 5 80,4009 0,44 1,152 0,2258 8,41 23,893 4,6829 0,8 24,25713 4,7542 10
Sisa 3 1,735 5 80,7503 0,43 1,239 0,2385 8,5 22,882 4,4047 0,6 17,29107 3,3285 10
Sisa 4 1,652 5 79,5393 0,24 0,726 0,1486 6,5 16,858 3,4493 1 15,13317 3,0964 5
Sisa 5 1,69 5 79,3924 0,45 1,154 0,2378 0,41 1,213 0,25 1 29,5858 6,0969 10
Jeroan 1 0,309 5 81,7881 1,27 19,58 3,5658 5,84 34,628 6,3064 0,9 72,81553 13,261 5
Jeroan 2 0,356 5 81,2273 3,89 53,79 10,098 9,32 89,045 16,716 1,2 84,26966 15,82 5
Jeroan 3 0,315 5 82,0728 2 31,75 5,6912 6,87 59,683 10,699 0,8 63,49206 11,382 5
Jeroan 4 0,335 5 81,4986 1,76 25,37 4,6944 7,53 112,39 20,793 0,9 67,16418 12,426 5
Jeroan 5 0,314 5 80,978 1,25 19,9 3,7862 5,49 87,42 16,629 0,8 63,69427 12,116 5
Blanko 0,06 0 0,6
Sum 157,9 29,422 464,77 87,688 518,1694 100,55
Avarage 10,53 1,9615 30,984 5,8459 34,54463 6,7031
48
Kodok (Tanpa Tulang) Purwodadi
Kode
Berat
distruksi Volume
Kadar air
Cu (AAS)
Kadar Cu
Cu sampel basah
Fe (AAS)
Kadar Fe
Fe sampel basah
Zn
(AAS) Kadar Zn Zn sampel
basah Dilution
Paha 1 1,13 5 81,8135 0,14 0,354 0,0644 1,63 7,2124 1,3117 1,9 5,752212 1,0461
Paha 2 1,185 5 81,0576 0,09 0,38 0,0719 0,4 1,6878 0,3197 1,6 6,751055 1,2788
Paha 3 1,124 5 79,7155 0,18 0,801 0,1624 0,53 2,3577 0,4782 0,9 4,003559 0,8121 5
Sisa 1 0,512 5 86,3201 0,18 1,758 0,2405 0,56 5,4688 0,7481 0,7 6,835938 0,9351
Sisa 2 0,514 5 85,8596 0,17 1,654 0,2338 0,93 9,0467 1,2792 0,6 5,836576 0,8253 5
Sisa 3 0,499 5 86,1419 0,1 1,002 0,1389 0,64 6,4128 0,8887 0,5 5,01002 0,6943 5
Jeroan 1 0,219 5 83,2402 1,57 35,84 6,0075 3,7 84,475 14,158 0,8 18,26484 3,0611
Jeroan 2 0,219 5 85,6225 1,7 38,81 5,5803 2,98 68,037 9,782 0,9 20,54795 2,9543
Jeroan 3 0,205 5 82,9704 3,78 92,2 15,7 3,11 75,854 12,918 0,8 19,5122 3,3228
Blanko 0,06 0 0,6
Sum 172,8 28,2 14,48 260,55 41,883 92,51434 14,93
Avarage 19,2 3,1334 28,95 4,6537 10,27937 1,6589
49
Lampiran 4. Hasil Perhitungan MCL
MCL berdasarkan Perhitungan Cu
ULSR pria = 12 mg/hari ULSR wanita =10mg/hari
= 12mg x 7 = 10mg x 7
= 84 mg/minggu = 70mg/minggu
MCL Cu untuk pria:
Semarang =
g
g
ggu
mg
/
162
,
2
min
/
84
µ
= 0,04g/minggu
Demak =
g
g
ggu
mg
/
789
,
2
min
/
84
µ
= 0,03g/minggu
Purwodadi =
g
g
ggu
mg
/
961
,
1
min
/
84
µ
= 0,04g/minggu
MCL Cu untuk wanita:
Semarang =
g
g
ngu
mg
/
162
,
2
min
/
70
µ
= 0,03g/minggu
Demak =
50
MCL berdasarkan perhitungan Zn
ULSR pria = 45mg/hari ULSR wanita = 35mg/hari
= 45mg x7 = 35mg x7
= 315mg/minggu = 245mg/minggu
MCL Zn pria:
Semarang =
g
g
ggu
mg
/
478
,
6
min
/
315
µ
= 0,04g/minggu
Demak =
g
g
ggu
mg
/
727
,
6
min
/
315
µ
= 0,05g/minggu
Purwodadi =
g
g
ggu
mg
/
703
,
6
min
/
315
µ
= 0,05g/minggu
MCL Zn wanita:
Semarang =
g
g
ggu
mg
/
478
,
6
min
/
245
µ
= 0,03g/minggu
Demak =
