NMR Data of Doped D2O

(1)

-2 -1

0 1

2 3

4 5

6 7

8 9

10 11

12 13

14

-20 0 20 40 60 80 100 120 140 160 180 200

(2)

6.85 6.95

7.05 7.15

7.25 7.35

7.45 7.55

7.65 7.75

7.85 7.95

f1 (ppm)

-5 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75

In te n si ty

Sample : Doped D2O

Selective band center: 6.16 (ppm); width: 37.0 (Hz) Selective band center: 8.87 (ppm); width: 26.9 (Hz) Selective band center: 7.86 (ppm); width: 18.1 (Hz) Selective band center: 7.65 (ppm); width: 28.1 (Hz) Selective band center: 1.29 (ppm); width: 6.1 (Hz) Selective band center: 3.89 (ppm); width: 14.6 (Hz)

1.06

1.95

0.97

1.04

0.29

1.99

1.06

1.03

2.96

0.96

1.00 6.856.866.88

6.936.946.976.98

7.107.117.127.12

7.26 Chloroform-d

7.377.397.417.437.447.46

7.54

7.587.597.61

7.777.807.827.837.847.84

(3)

6.1 6.2 6.3 6.4 6.5 6.6 6.7 6.8 6.9 7.0 7.1 7.2 7.3 7.4 7.5 7.6 7.7 7.8 7.9 8.0 8.1 8.2 8.3 8.4 8.5 8.6

-5 0 5 10 15 20 25 30 35 40 45 50 55 60

6.866.876.896.946.966.986.99

7.117.127.137.13

7.23

7.27

7.397.417.427.447.467.477.557.597.607.62

7.787.817.847.85

(4)

3.5 3.6

3.7 3.8

3.9 4.0

4.1 4.2

4.3 4.4

4.5 4.6

4.7 4.8

4.9 f1 (ppm)

-20 0 20 40 60 80 100 120 140 160 180 200 220 240 260

Sample : Doped D2O

0.88

21.99

1.01

16.95

0.86

16.74

0.79 3.86

4.124.134.14

4.444.464.47

(5)

1.1 1.2

1.3 1.4

1.5 1.6

1.7 1.8

1.9 2.0

2.1 2.2

2.3 2.4

2.5 2.6

2.7 2.8

-20 0 20 40 60 80 100 120 140 160 180 200

1.00

3.87

37.94 1.66

2.01

2.04

(6)

-10 0

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 230

f1 (ppm)

-8 -7 -6 -5 -4 -3 -2 -1 0 1 2 3 4 5 6 7 8 9 10 11 Sample : Doped D2O 12

(7)

110 115

120 125

130 135

140 145

f1 (ppm)

-9 -8 -7 -6 -5 -4 -3 -2 -1 0 1 2 3 4 5 6 7 8 9 10

117.58117.58119.14

119.41 119.41

119.77

121.00121.00

135.65135.67

144.72144.75

(8)

25 30

35 40

45 50

55 60

65 70

f1 (ppm)

-8 -7 -6 -5 -4 -3 -2 -1 0 1 2 3 4 5 6 7 8 9 10 11 Sample : Doped D2O 12

25.4125.4425.9025.90

55.4155.44

64.9864.98

67.4267.42