C O N T E N T S PART ONE
FUNCTIONAL GROUP ANALYSIS BY CHEMICAL METHODS Page CHAPTER I DIFFERENTIAL KUHN – ROTH C – METHYL
ESTIMATION
Past work 1 – 10 Experimental 11 – 12 Present work and discussion 13 – 27 References 28 – 29 CHAPTER II DETERMINATION OF THE NUMBER AND
NATURE OF ACETYL GROUPS IN ORGANIC COMPOUNDS
Past work 30 – 36
Present work 36 – 39 Experimental 40 – 41 Results and discussion 42 – 50 References 51 – 52
PART TWO
SOME APPLICATIONS OF SP ECTROSCOPIC METHODS OF ANALYSIS
CHAPTER I SCISSORING FREQUENCY OF METHYLENE GROUP FLANKING A CARBONYL
Introduction 53 – 56 Experimental 57 – 72
Page Results and discussion 73 – 80 Appendix 81 – 92 References 93 – 94
CHAPTER II INDETIFICATION OF METHYL- NAPHTHALNES BY NMR
Introduction 95 – 97
Present work 97 – 98 Experimental 99 – 104 References 105 CHAPTER III CHARACTERIZATION OF THE N – METHYL
GROUP IN AN ORGANIC COMPOUND BY NMR
Pregl – Herzig – Meyer method 106 – 107 Application of PMR to N – methyl 108 – 109 estimation
Present work 109 – 111 Experimental 112 – 113 Discussion 113 – 146 References 147 – 148 SYSOPSIS .. .. .. 149 – 151 STATEMENT .. .. .. 159 ACKNOWLEDGEMENT .. .. 153
