Page 34 of 105 Course
Name Safety in laboratories Course
Code KCHE 101 Prerequisite
Training semester 1 2 3 4 5
Credit hours 2
Collaborative training Contact hours
(Hour/ week)
Lecture 2
Practical 0
Training 0
Course Description
The course aims to provide the trainee with basic knowledge of general safety precautions in chemical laboratories, and to know how to deal with glass bottles and chemicals of various kinds and how to store and store them, in addition to identifying the types of fires and means of extinguishing them and knowing first aid.
The general objective of the course:
This course aims to provide the trainee with the basic knowledge and skills to equip chemical laboratories and properly deal with them and with the equipment, chemicals, and glass tools they contain.
The detailed objectives of the course:
By the end of this course, the trainee will be able to:
Ensures availability of safety elements and tools in the chemical laboratory
It follows the instructions, procedures and examination of health, safety and environmental standards in the chemical laboratory
Follow safety instructions for collecting samples Follow safety instructions in the preparation process
It follows the necessary safety instructions for analyzing samples
Determines the harms and risks of the waste chemicals used based on their nature Follow and report on emergency procedures.
Page 35 of 105
Units (theoretical and practical) Training hours Theoretical practical o General precautions for safety in chemical laboratories 4
o Knowing the risks and injuries in chemical laboratories 2 o Knowing the safety precautions for experiments that
need to be heated 2
o Knowing the safety precautions when dealing with
glassware 2
o Knowing safety precautions when dealing with
compressed gas cylinders 4
o Chemical Safety Data Sheet 2
o Knowing the safety precautions after completing the
work in the laboratory 2
o Knowing safety precautions when storing and storing
chemicals. 4
o Knowledge of the types of fires and means of
extinguishing them 4
o Knowledge of first aid 4
o Safety inspection in chemical laboratories 2
Total 32
32
Procedures of Safety Requirements:
1. Identify and assess the risks that may pose a risk of injury or illness.
2. Reducing direct risks to the soul and to the health and safety of the victim / victims.
3. Evaluate the victim / victims and determine injuries, illnesses and health conditions before using first aid.
4. Quietly providing information to reassure the injured.
5. Monitor and respond to the condition of the injured according to effective first aid principles and procedures.
6. Use effective resources and equipment to make the injured as comfortable as possible.
7. Responding to the injured with appropriate cultural and emotional differences; And seek approval from the injured person / injured or the right person and provide first aid.
8. Operating first aid equipment properly when necessary to administer first aid, and requesting assistance in providing first aid from others in a timely and appropriate manner.
9. Seek help from the ambulance and / or appropriate medical assistance.
10. Accurate news of the ambulance services about the injured case assessment and management activities.
11. Prepare reports as appropriate in a timely manner, and provide all relevant facts in accordance with procedures or other emergency services or according to relief workers
Page 36 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
4
General precautions for safety in chemical laboratories
o Basic specifications of chemical laboratories o Essential safety equipment to be provided in the
laboratory
Oral exams Written exams The detailed approach (theoretical and practical)
hours Content Assessment tools
o Personal protection tools
o Precautions to be taken for the safety of chemicals in circulation
o General safety directions and guidelines o Guidelines to be observed in laboratories
2
Material Safety Data Sheets (MSDS) o Explanation of the safety data sheet o Card template
o Chemical Safety Sticker Explanation o Poster template
Oral exams Written exams
4
Hazards and injuries in chemical laboratories:
o Types of hazards in chemical laboratories o Risk factors in chemical laboratories.
o Types of injuries.
o Symptoms of exposure to chemicals.
o Methods of entry of chemicals into the body.
o Work accidents and injuries and their aftermath o Various damages to chemicals.
Oral exams Written exams
2
Safety precautions for experiments that need to be heated:
o General safety guidelines for experiments that need heating
o Heat the non-combustible liquids.
o Boiling point.
o Methods of heating organic liquids.
Oral exams Written exams
2
Safety precautions when handling glassware
o Dealing with glass bottles keeping solid chemicals and liquids.
o Test tube shaking methods.
o Safety precautions when cutting glass tubes.
Oral exams Written exams
Page 37 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
o Safety precautions when inserting glass tubes into seal holes.
o Safety precautions for removing glass tubes from clogs
4
Safety precautions when handling gas cylinders o an introduction
o Uses of gas cylinders.
o The main risks arising from the use of compressed gas cylinders.
o The main causes of accidents when dealing with compressed gas cylinders.
o Ways to reduce risks.
o Dealing with leakage cylinders o Knowing the gases involved.
o Toxic gas properties
Oral exams Written exams
The detailed approach (theoretical and practical)
hours Content Assessment tools
2
Safety precautions after completing work in the laboratory:
o an introduction
o Safety precautions when removing excess chemical residue.
o Safety precautions after completion of laboratory work
Oral exams Written exams
4
Safety precautions when storing and preserving chemicals:
o an introduction
o Storage of flammable chemicals.
o Toxic storage.
o Storage of explosive chemicals
Oral exams Written exams
Page 38 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
2
o Storing oxidizing agents.
o Storage of bulk materials.
o Storage of compressed gases.
o Store sensitive materials.
o Discordant matter.
Oral exams Written exams
4
Types of fires and means of extinguishing them o an introduction
o Chemical properties o Fire classification.
o Types of extinguishers
Oral exams Written exams
4 first aid
o First aid methods for burn cases
o First aid methods in cases of poisoning.
o Recommendations when gas leaks o First aid kit
Oral exams Written exams
2 Safety inspection in chemical laboratories o Safety regulation
o Safety inspection o Carry out the inspection o Safety checklist
o Safety inspection form
Oral exams Written exams
References - Safety in laboratories and chemical factories d. Ibrahim Al-Mutaz and Dr.
Mohammed Al-Hassan. Al-Khuriji Library 1408
Page 39 of 105 Course
Name Chemical Calculations Course
Code KCHE 105 Prerequisite
Training semester 1 2 3 4 5
Credit hours 2
Collaborative training Contact hours
(Hour/ week)
Lecture 2
Practical 0
Training 0
Course Description
The course aims to provide the trainee with basic knowledge in performing calculations in each of the international system of units, calculations on the atomic structure, methods of expression of concentration, calculations of states of matter, calculations of oxidation and reduction, calculations of acids and bases, calculations of chemical equilibrium, calculations in thermodynamics
The general objective of the course:
This course aims to provide the trainee with the basic knowledge and skills to perform various chemical calculations.
The detailed objectives of the course:
By the end of this course, the trainee will be able to:
1. Learn about the international system of measurements.
2. Learn to perform atomic composition calculations 3. Master the calculations by expressing focus.
4. He can perform calculations on material states 5. Distinguish accounts for oxidation and reduction.
6. Proficient in making the necessary calculations for acids and bases.
7. Identifies special calculations in chemical equilibrium.
8. Distinguish between the laws of thermodynamics.
Page 40 of 105
Units (theoretical and practical) Training hours Theoretical practical
o International System of Units 2
o Calculations on the atomic structure 6
o Expressions of focus 6
o Chemical case calculations 4
o Calculations of oxidation and reduction 4
o Calculations of acids and bases 4
o Chemical equilibrium calculations 4
o Thermodynamic calculations 2
Total 32
32
Procedures of Safety Requirements:
1. Identify and assess the risks that may pose a risk of injury or illness.
2. Reducing direct risks to the soul and to the health and safety of the victim / victims.
3. Evaluate the victim / victims and determine injuries, illnesses and health conditions before using first aid.
4. Quietly providing information to reassure the injured.
5. Monitor and respond to the condition of the injured according to effective first aid principles and procedures.
6. Use effective resources and equipment to make the injured as comfortable as possible.
7. Responding to the injured with appropriate cultural and emotional differences; And seek approval from the injured person / injured or the right person and provide first aid.
8. Operating first aid equipment properly when necessary to administer first aid, and requesting assistance in providing first aid from others in a timely and appropriate manner.
9. Seek help from the ambulance and / or appropriate medical assistance.
10. Accurate news of the ambulance services about the injured case assessment and management activities.
11. Prepare reports as appropriate in a timely manner, and provide all relevant facts in accordance with procedures or other emergency services or according to relief workers
Page 41 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
2
International System of Units
o The basic units of the international system o Units derived from the international system o Common units outside the international system o Transfers between the international system and
other systems (temperature, pressure, time)
Oral exams Written exams
6
Calculations on the atomic structure
o Calculations on atomic structure, electromagnetic radiation, relationship between absorption and permeability.
o Calculations in the primary and molecular formulas
o Calculations in quantum numbers
Oral exams Written exams
6
Expressions of focus
o Weighted, volumetric percentage, volumetric weight
o Molar fracture o Molarity o Molarity o Standard o Gram / liter o Mg / L PPm
o Micrograms / liter - PPb
Oral exams Written exams
4
Chemical cases calculations
o Mass, density and volume calculations.
o Invasive condition o (Boyle's Law) o Charles's Law o Jay Lusak's Law
Oral exams Written exams
Page 42 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
o The General Law of Gases o Dalton's Law
o Liquid state
o A Brazilian Viscosity law o Viscosity Breeding Law o Surface tension
4
Calculations of oxidation and reduction o Oxidation and reduction equations o Prepare oxidation and reduction o Pole voltage
o Cell voltage
o Calculations on Farday Law I and II in electrolysis
Oral exams Written exams
4
Calculations of acids and bases o Strong acids and bases o Weak acids and bases o Acid and basic salts o Calibration
Oral exams Written exams
4
Chemical equilibrium calculations o Measuring reaction velocity o Static equilibrium
o The relationship between Kc and Kp
o The most recent material accounts for the reaction and theoretical and centenary returns
o Solubility and dissolving quotient
Oral exams Written exams
4 Calculations in thermodynamics o The laws of thermodynamics
Oral exams Written exams The detailed approach (theoretical and practical)
hours Content Assessment tools
o Heat capacity and specific heat o Measuring reaction temperature o Hess Law
o Gypsum energy
References
- The simplified explanation in general chemistry, Dr. Muhammad Shafiq Al- Kanani and Dr. Sulaiman Hammad Al-Khwaiter. Dar Al-Khuraiji for Publishing and Distribution 1427
Page 43 of 105 Course
Name Principles in Organic Chemistry Course
Code KCHE 111 Prerequisite
Training semester 1 2 3 4 5
Credit hours 4
Collaborative training Contact hours
(Hour/ week)
Lecture 2
Practical 4
Training 0
Course Description
The course aims to provide the trainee with basic knowledge of organic chemistry and its interactions.
In this course, the compounds (aliphatic and aromatic hydrocarbons, halides, alcohols and phenols, ethers, aldehydes and ketones, carboxylic acids and their derivatives, amines and their derivatives, carbohydrates) will be identified and in practice the training will be conducted on the detection of compounds and functional groups and their preparation in practice in the laboratory
The general objective of the course:
This course aims to provide the trainee the basic knowledge and skills of organic chemistry and effective groups and their interactions.
The detailed objectives of the course:
By the end of this course, the trainee will be able to:
1. It applies the methods adopted in the preparations 2. Dilute the original materials as required
3. Analyzes the samples 4. Chemical preparation
5. Chemical analysis is performed
6. It gets results for the methods of analysis 7. Ensure that the analysis used is correct 8. Prepares chemical calculations
9. Designs a table of results and analyzes 10. Take notes on the results
11. Submit final reports
Page 44 of 105
Units (theoretical and practical) Training hours Theoretical practical
The foundations of general organic chemistry 4
Study of aliphatic hydrocarbons 4
Aromatic compounds 4
Organic halides 4
Mules (alcohols) and ether 4
Aldehydes and ketones 4
Carboxylic acids and derivatives 2
Amines 2
Carbohydrates 4
Qualitative analysis of organic compounds 8
Disclosure of organic groups 12
Prepare some organic compounds 12
Total 32 32
64
Procedures of Safety Requirements:
1. Identify and assess the risks that may pose a risk of injury or illness.
2. Reducing direct risks to the soul and to the health and safety of the victim / victims.
3. Evaluate the victim / victims and determine injuries, illnesses and health conditions before using first aid.
4. Quietly providing information to reassure the injured.
5. Monitor and respond to the condition of the injured according to effective first aid principles and procedures.
6. Use effective resources and equipment to make the injured as comfortable as possible.
7. Responding to the injured with appropriate cultural and emotional differences; And seek approval from the injured person / injured or the right person and provide first aid.
8. Operating first aid equipment properly when necessary to administer first aid, and requesting assistance in providing first aid from others in a timely and appropriate manner.
9. Seek help from the ambulance and / or appropriate medical assistance.
10. Accurate news of the ambulance services about the injured case assessment and management activities.
11. Prepare reports as appropriate in a timely manner, and provide all relevant facts in accordance with procedures or other emergency services or according to relief workers
Page 45 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
4
General principles:
o an introduction
o Definition of organic chemistry o Effective groups.
o Interactions of organic compounds o Study of hydrocarbons
Oral exams Written exams
Practical performance
4
Alkanes:
o an introduction o The label
o Physical properties
o The industrial source of alkanes o How to prepare
o Reduction or hydrogenation of alkanes o Greenard reaction
o Its interactions are halogenation of alkanes.
o Alkanes oxidation o Alkenes and Alkynes:
o an introduction o The label
o Physical properties
Oral exams Written exams
The detailed approach (theoretical and practical)
hours Content Assessment tools
o How to prepare o Thermal cracking
o Reduction or hydrogenation - its interactions o Halogenation
o Oxidation
o The effect of water on calcium carbide o add the water
o Add sulfuric acid
4
Aromatic compounds:
o Introduction - benzene synthesis - aromatic properties o Physical properties - Designation of benzene derivatives o Source of aromatic compounds
o Aromatic compounds interactions
o Aromatic electrophoresis of the aromatic ring o Halogenation
o Sulfonation o nitrification o Alkylation o Acylation
o Industrial applications of aromatic compounds
Oral exams Written exams
4
Organic halides:
o an introduction o Physical properties o Preparation methods
o Organic halides (alkylated halides and aromatic halides).
Oral exams Written exams
4
Alcohol and ether:
o an introduction o The label
Oral exams Written exams
Page 46 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
o Physical properties o Ways to prepare for it 4 Aldehydes and ketones:
o an introduction o The label
o Physical properties o Ways to prepare for it
o Identify aldehydes and ketones 2 Carboxylic acids and derivatives:
o an introduction o The label
o Physical properties o Ways to prepare for it o Their interactions o Acidity constant
2 Amines:
o an introduction o The label
o Physical properties o Ways to prepare for it 4 Carbohydrates:
o an introduction
o Carbohydrate classification and example for each class.
8 Descriptive analysis of organic compounds:
o Solubility test.
o Saturation and combustion test.
o Element detection test in solid and liquid materials.
Page 47 of 105
The detailed approach (theoretical and practical)
hours Content Assessment tools
12 Disclosure of membership groups:
o Identify the carbonyl group of aldehydes and ketones.
o Detection of sugars.
o Identify the acidic carboxyl group and phenolic hydroxyl.
o Familiarize yourself with the Al-Amin group and its nitro-amide group.
o Identify unknown organic compounds by following the previous detection steps with measurements on infrared and ultraviolet devices 12 Preparing some organic compounds:
o Preparation of acetylsalicylic acid (aspirin).
o Prepare paranitrous and benzoic acid from paranetrotoluene.
o Prepare the stanlide from the insulin.
o Prepare the stapled barabromo from the stanelide.
o Prepare paranitroeniline from paranetrostanilide.
o Study of infrared spectra of some previously damaged organic compounds
References - The foundations of organic chemistry, d. Salem Althiab
- Organic chemistry, d. Mohammed Al-Hassan d. Mohsen al-Hazmi
Page 48 of 105 Course
Name Principles in analytical Chemistry Course
Code KCHE 112 Prerequisite
Training semester 1 2 3 4 5
Credit hours 4
Collaborative training Contact hours
(Hour/ week)
Lecture 2
Practical 4
Training 0
Course Description
The course aims to provide the trainee with basic knowledge in analytical chemistry, and training will be in the analysis of samples using traditional methods of analysis through theoretical information in analytical chemistry, and training will also be conducted on how to properly use the tools of traditional analysis (volumetric analysis, weight analysis and qualitative analysis of inorganic compounds).
The general objective of the course:
This course aims to provide the trainee with basic knowledge and skills in preparing reagents and evidence and analyzing samples using traditional methods
The detailed objectives of the course:
By the end of this course, the trainee will be able to:
1. Prepare standard materials for required concentrations
2. Perform the necessary measurements to comply with the recommended results 3. Determines appropriate tools for collecting samples according to scientific methods 4. It applies the methods adopted in the preparation process to obtain the required chemicals 5. Dilute the original materials to prepare a standard dilute solution with a suitable concentration 6. The prepared reagents are standardized using concentration information reagents to accurately
determine the concentration of these reagents
7. The reagents are checked periodically with titrated standard known solutions to confirm the concentration value
8. Determines the method of analysis compatible with the nature of the sample to ensure the correctness of the method of analysis
9. Bring the required chemicals with the appropriate scientific methods to obtain the chemicals with the appropriate concentrations
10. Analyzes the samples by known analytical methods to determine what they are 11. Verify the accuracy of the analysis by matching the result with the standard materials 12. Chemical calculations are prepared according to the correct equations for calculating the
concentrations of minerals and compounds 13. Design the table of results for the analysis
14. Without notes on the results clearly to show his views on it
15. The report shall be submitted in an appropriate and integrated manner
Page 49 of 105
Units (theoretical and practical) Training hours Theoretical practical o Description of chemical analysis processes 6
o Volumetric analysis (acid and base titrations - sediment titrations - oxidation and reduction titrations - complexity titrations)
12 16
o Weighted analysis 8 16
o Theoretical basis for the qualitative analysis of inorganic
compounds 6
Total 32 32
64
Procedures of Safety Requirements:
1. Identify and assess the risks that may pose a risk of injury or illness.
2. Reducing direct risks to the soul and to the health and safety of the victim / victims.
3. Evaluate the victim / victims and determine injuries, illnesses and health conditions before using first aid.
4. Quietly providing information to reassure the injured.
5. Monitor and respond to the condition of the injured according to effective first aid principles and procedures.
6. Use effective resources and equipment to make the injured as comfortable as possible.
7. Responding to the injured with appropriate cultural and emotional differences; And seek approval from the injured person / injured or the right person and provide first aid.
8. Operating first aid equipment properly when necessary to administer first aid, and requesting assistance in providing first aid from others in a timely and appropriate manner.
9. Seek help from the ambulance and / or appropriate medical assistance.
10. Accurate news of the ambulance services about the injured case assessment and management activities.
11. Prepare reports as appropriate in a timely manner, and provide all relevant facts in accordance with procedures or other emergency services or according to relief workers