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CHAPTER .3 MODEL DESCRIPTlON

Boiling point elevation

A series of attempts has been made over the years to correlate the boiling point elevation of sucrose solutions with sucrose concentration. All of these studies were, however, based on a severely limited number of data points provided by the individual authors. Moreover, only a few were based on sound thennodynamic principles, utilising the concept of the activity coefficient. None of these correlations was thus considered to be ideally suited for use in the climbing film evaporator model Thus, in order to improve the reliability of boiling point elevation prediction, Starzak and Peacock (1997) collected boiling point temperature, vapour pressure, equilibrium relative humidity and other closely related data for aqueous sucrose solutions from 56 studies published over more than a century. These data were processed to derive a thermodynamically rigorous and statistically sound equation for the water activity coefficient. which can be used to predict the boiling point elevation (in °C) of sucrose solutions over the full :range of sucrose concentrations and at different system pressures:

CHAPTER 3 MODEL DESCRIPTlON

This boiling point elevation prediction correlation was compared with twenty other well known prediction methods available in the literature and shown to be the most accurate and reliable of all the methods tested, with a mean deviation of about 2% (Starzak and Peacock, 1998) .

Density of condensate

The density of condensate (in kg/dm') was calculated using the correlation of Aggarwal (1989) for the specific volume of saturated water:

9

+

"A

L... n tnc - 4 0=5

where Vc is the specific volume of condensate. tc is the condensate temperature in degrees Kelvin and the coefficients AI through ~ are given by

For I, s 373,2 K

A, =0.31060619e+01; A, = -0.90267563e+01; A, = 0.51 853027e+02;

A"

= -0.39588600e+02;

A, = 0.39760528e+01;

A"

= -0.5 I 528862e+02;

A, = 0.12148573e+03; As = -0.14039282e+03;

A"

= 0.65221863e+02;

For 373.2 K < I, S 600 K

A, = 0.31060000e+01;

A, = -0,56161909e+01; A, = 0.13398 111e+02;

A, = 0.58633842e+01;

CHAPTER 3

A, ~ -0.18599625e+02;

A.

~ 0.64106083e+01;

A, ~ -0.87578869e+01; As ~ 0.88766804e+01; A, ~ -0.37156558e+01;

For 1< > 600K

A, ~ 0.31060000e+01;

A, ~ -0.54649353e+01;

A, ~ -0.72486047e+03;

A, ~ 0.12055044e+04;

A, ~ -0.57213086e+03;

A, ~ 0.72626416e+03; A, ~ -0.65027012e+04; As ~ 0.41431125e+05;

A, ~-0.11816734e+06;

Density of sugar cane juice

MODEL DESCRIPTION

The density of sugar cane juice (in kg/m') was calculated using the correlation of Kadlec el. al. (1983):

PL ~ a+bTL+cT~+dT{

where the coefficients a, b, c and d are given by:

a ::::;

ao + al Bx + a2 Bx2 + a3 Bx3

, ,

b = bo + bl Bx + b, Bx + b, Bx

d = do + dl Bx + d, Bx' + d, Bx'

CHAFTEA3 MODEL DESCRIPTION

where Bx is the dry solids content (sucrose and impurities) of the sugar cane juice on a mass percent basis. and the coefficients are given in Table 1.

Table 1. Coefficients for the Kadlec et, ai_ density correlation_

Concentration range i- 1 2 3 4

a 1000,45 3,94325 0,0146409 2,69936 x 1 O-~

b -6,01137 x 10-3 -6,85707 x 10-) -2,63869 x 10-<5 -1,54649 x 104 Bx :s 69%

c -5,44367 x 10'3 7,64646 x 1O,s -6,50649 x 10-7 8,44748 x 10-9 d 1,31672 x lO-s -3,55879 X 10-' 6,36639 x 10-9 -7,25049 x 10-1\

a 1316,33 -Q,61119 0,130327 -3,91182 x 10-' b -1,7077 0,0299153 -1,46234 x 10'" -4,69390 X 10-7 Bx>69%

C 6,51225 x 10-3 -1,65477 x 1~ 2,15744 x 10'7 8,36737 x 10'"

d 0 0 0 0

Density of vapour and steam

The density of vapour was calculated using the ideal gas equation.

Enthalpy of saturated liquid water

The specific enthalpy of saturated liquid water (in kJ/kg) was calculated using the correlation of Aggarwal (1989):

9

+

"A

L.... n tDw - 4

0 ; 5

where

hw

is the specific enthalpy, t,.,.. is the temperature in degrees Kelvin and the coefficients AI through A, are given by

For '. $ 287.2 K

AI ~ 0.2364914ge-02;

A, ~ 0.10918589e+04;

A, ~ -0.92032929e+04;

CHAPTER 3

A.

= 0.22190031e+05;

As = -O.78623057e+04;

A"

= -0.32543672e+05;

A, = 0.40901742e+05;

A, = -0.36393298e+03;

A"

= -0. 19495543e+05;

For t. > 287,2 K

A, = 0.20860000e+04;

A, = -0.10864822e+04;

A, = 0.30911332e+05;

A.

= -0.44055891e+05;

As = 0.11541795e+05;

A"

= 0.48651314e+02;

A, = -0. 18603667e+04;

A, = 0.24305122e+04;

A"

= -0. 13371470e+04;

Enthalpy of saturated water vapour

MOOEL. OESCR1PT10N

The specific enthalpy of satuIated water vapour (in kJlkg) was calculated using the correlation of Aggarwal (1989):

9

+ ' " A tn- 4

L... a v

a.S

where

h.

is the specific enthalpy,

t.

is the temperature in degrees Kelvin and the coefficients AI through ~ are given by

For t. 5591,2 K

A, = 0.20860000e+04;

CHAP'Tl!R 3

A, ~ O.13530557e+04;

A, ~ -O.33616219e+05;

A., ~ O.53989891e+05;

A, ~ -O.22623269e+05;

A., ~ O.14442905e+04;

A, ~ -O.34480552e+04;

A, ~ 0.47304248e+04;

A, ~ -0. 172409J3e+04;

For t. < 591,2 K

A, ~ O.20860000e+04;

A, ~ O.86537622e+03; A, ~ 0.46032137e+06;

A., ~ -O.7264J812e+06;

A, ~ O.31508275e+06;

A., ~ -0.39173969e+06;

A, ~ O.37372265e+07;

A, ~ -O.25566604e+08;

A, ~ O.77743632e+08;

Enthalpy of sugar cane juice

MODEL DESCRIPTION

The specific enthalpy of sugar cane juice (in kJ/kg) was calculated using the correlation by Lyle (1950)

{(BX) ( 100 +

BX )

hL

=

2,326

10

900 _ 8 Bx

where Bx is the dry solids content (sucrose and impurities) of the sugar cane juice on a mass percent basis and T L is the juice temperature in cc.

CHAP'TER3 MODEL DESCR1PTION

Saturation pressure of water

The absolute vapour pressure of saturated boiling water (in bar) at a given boiling point temperature, Ts in degrees Kelvin, was calculated using the Wagner equation (Wagner,1973):

where

and the coefficients are given by

For 273,2 ,; T,'; 323,2 K

A, = -8,10988775;

A, = 2,17464254;

A, = -3,51897089;

A., = -0,50283681; A, = 647,126;

A =22055"

"<> "

For 323,2 < T, ,; 423,2 K A, = -7,81340301; A, = 1,55097861; A, = -2,84616200;

A., = -1,26127042; A, = 647,126;

A"

= 220,55;

+

A

2 '1,1,5 +

A

3 '1" +

A

4

'1'6]

1 - '1'

' 1 ' = 1 - - T,

A s

CHAPTEA3

For 423,2 < T, $ 523,2 K

A, - -7,74037537;

A, - 1,38109682;

A, - -2,60773347;

A. - -1,57952429;

A, - 647,126;

• -22055

"6 "

For T, > 523,2 K

A, - -7,82843137;

A, - 1,69248424;

A, - -4,27203456;

A. -

49,12068163;

A, - 647,126;

• - 22055'

"6 "

Saturation temperature of water

MOOEL DESCAIP'TIOH

The boiling point temperature of pure water (in degrees Kelvin) at a given absolute pressure was calculated using the correlation of Aggarwal (1989):

T

=

A + A 2

s I logP

.

+ A

,

where Ps is the absolute pressure in Mpa and the coefficients are given as:

For P, $ 0,085 MPa

A, - 0.39612064e+02;

A, - -O.39839608e+04;

A, - -0.96562826e+01;

CHAPTER 3

For 0,085 < P, $ 2,625 MPa

AI ~ 0.45864958e+02; A, ~ ·0.38175562e+04;

A, ~ ..Q.93753290e+Ol;

For 2,625 < P, $ 11,25 MPa

AI ~ ..Q.43211877e+01; A, ~ ·0.46978731e+04;

A, ~ ..Q.I0285592e+02;

For p. > 11,25 MPa

AI ~ ..Q.31177350e+03;

A, ~ ..Q.I0757354e+05;

A, ~ ..Q.14310894e+02;

Specific heal capacity of condensale

MOO~L DESCRIFT10N

The specific heat capacity of pure water (in kJ/kg. QC) was calculated using an empirical correlation:

where T c is the temperature of the condensate in

0 c.

Specific heat capacity of sugar cane juice

The specific heat capacity of sugar cane juice (in kJ/kg.°C) was calculated using the correlation developed by Watson (1989):

CPL

=

4,1253 - 0,024804Bx + 6,7 x 10-' Bx . TL

+ 1 ,8691

X

10-

3

TL - 9,271

X

10-6

T~

CI-lAP'ITR 3 MODEL DESCRIPTION

where T L is the juice temperature and Bx is the dry solids content (sucrose and impurities) of the sugar cane juice on a mass percent basis.

Specific heat capacity of water vapour

The specific heat capacity of water vapour (in kJikg. 'C) was calculated using an empirical correlation:

Cpv

=

0,2323418 (8,10 - 0,72 x 10-

3

tv + 3,63x 10"'; t~ - 1,16x 10-' t; )

where !v is the vapour temperature in degrees Kelvin.

Swface tension

The swface tension at the liquid / vapour interface in sugar cane juice (in N/m) was calculated using the correlation of Watson (1989):

where T L is the temperature of the juice in °C andBx is the dry solids content (sucrose and impurities) of the sugar cane juice on a mass percent basis.

Thermal conductivity of condensate

The thermal conductivity of pure water (in W/m.'C) was calculated using an empirical correlation:

k

w 6,308 x 10-6 T2 c

where T

c

is the temperature of the condensate in

c c.

Thermal conductivity of sugar cane juice

The thermal conductivity of sugar cane juice (in W/m.oC) was calculated using the correlation ofRiedel (1949):

kL =

1,162222 x 10-

3

(486 + 1,55T

L -

0,005T~)(I- 0,0054Bx)

CI-tAPT!:R 3 MODEL. DescRlPTloN

where T L is the temperature of the juice in °C and Bx is the dry solids content (sucrose and impurities) of the sugar cane juice on a mass percent basis.

Thermal conductivity of water vapour

The thermal conductivity of water vapour (in W Im.oC) was calculated using an empirical correlation:

+ 4 , 3 X 10-4 t2 v -21,73xlO-8 t~) where lv is the vapour temperature in degrees Kelvin.

Viscosity of condensate

The viscosity of pure water (in kg/m.s) was calculated using an empirical correlation:

f'w = 2,73xlO-3 + 2,88xlO--{i Tc - 5,95x10-4logTc

where Tc: is the temperature of the condensate in QC.

Viscos ity of sugar cane juice

The viscosity of sugar cane juice (in cP, where I cP = 1000 kg/m.s) was calculated using the correlation ofGenotelle (1978):

[

ll + 431N 1

.2 5 )