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Lampiran 1
Diagram Alir Penelitian
Telaah Pustaka
Persiapan Bahan dan Alat
Pemilihan Sampel
Pengujian Makroskopik
(Visual, Camera Digital, Mikroskop Stereo)
Pengujian Mikroskopik dan Senyawa Kimia
Mikroskop Optik, EDS OES XRD
SEM
Pengolahan dan Analisis Data
Lampiran 2
Alat-alat yang digunakan dalam penelitian
Gambar 5.1 Jangka Sorong dan Mikrometer Sekrup
Gambar 5.2 Kamera Digital
Gambar 5.4 Mikroskop Optik beserta monitor komputer
(a) (b)
Gambar 5.6 (a) instrumen OES, dan (b) instrumen saat beroperasi.
Lampiran 3
Hasil karakterisasi oleh EDS.
Gambar 5.8 Image EDS Pipa Dalam 1 titik 022
Gambar 5.10 Image EDS Pipa Dalam 1 titik 023
Gambar 5.12 Image EDS Pipa Dalam 1 titik 024
Gambar 5.14 Image EDS Pipa Dalam 1 titik 025
Gambar 5.16 Image EDS Pipa Dalam 1 titik 026
Gambar 5.18 Image EDS Pipa Dalam 1 titik 027
Gambar 5.20 Image EDS Cross Section 2 titik 007
Gambar 5.22 Image EDS Cross Section 2 titik 008
Gambar 5.24 Image EDS Cross Section 2 titik 009
Gambar 5.26 Image EDS Cross Section 2 titik 010
Gambar 5.28 Image EDS Cross Section 2 titik 011
Gambar 5.30 Image EDS Cross Section 2 titik 012
Lampiran 4. Hasil analisis fasa dari grafik XRD
Tabel 9. Analisis fasa untuk grafik pada gambar 4.23
2-Theta d(A) I% Fe (06-0696)
44,907 2,0168 100 2,0268/100-1 65,15 1,4307 14,6 1,4332/20-3
Tabel 10. Analisis fasa untuk grafik pada gambar 4.24
2-Theta d(A) I% FeS (23-1120) FeCO3 (29-0696) Fe2O3 (47-1409) FeOOH (26-0792) 31,618 2,8274 100 2,843/100-1 2,795/100-1 52,356 1,746 100 1,754/50-7 1,7382/30-3 1,747/100-1 60,27 1,5343 71,4 61,042 1,5167 61,9 45,641 1,986 52,4 1,979/100-2 1,965/20-5 1,9200/100-2 2,02/60-9 55,706 1,6487 52,4 1,632/60-3 1,649/80-5 26,565 3,3526 47,6 3,301/100-3 55,079 1,666 47,6 1,6700/100-1 1,674/100-2 62,284 1,4894 47,6 1,400/50-6 1,496-60-10 59,775 1,5458 42,9 1,502/30-10 1,5400/50-5 1,542/60-11 61,623 1,5038 42,9 1,502/30-9 1,5063/14-8
Tabel 11. Analisis fasa untuk grafik pada gambar 4.25
2-Theta d(A) I% FeS (23-1120) FeSO4 (17-873) FeCO3 (29-0696) Fe3O4 (19-0629) FeCl2 (01-1106) 31,566 2,8319 100 2,843/100-1 2,795/100-1 49,137 1,8526 47,5 1,881/40-8 34,61 2,5896 37,3 2,582/60-3 2,532/100-1 2,540/100-1 34,412 2,6039 35,6 2,618/100-1 26,155 3,4043 30,5 3.410/35-3 55,04 1,6671 28,8 1,7315/35-2 49,644 1,8349 27,1 1,825/25-8 1,800/63-2 38,43 2,3405 25,4 2,444/60-4 2,346/20-5 2,32/7 55,304 1,6597 25,4 1,632/60-6 1,6158/40-4 1,633/2 60,534 1,5282 25,4 1,529/3 1,4845/40-2 1,553/4 29,211 3,0547 23,7 2,967/30-3 3,07/30-4 66,957 1,3964 23,7 1,412/20-11 1,431/30-4 1,3969/6 83,113 1,1612 22 1,173/2 1.093/12-6 1,173/2 33,429 2,6783 20,3 41,646 2,1669 18,6 2,113/60-5 2,134/20-6 2,0993/20-5 40,447 2,2283 15,3 2,250/20-10 51,069 1,787 15,3 1,754/50-7 1,797/12 1,7146/10-7 61,81 1,4997 13,6 1,502/30-9 1,506/14 1,467/20-5