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DIELECTRIC PERFORMANCE OF DIFFERENT TYPES OF POLYMERIC MATERIAL

UNDER STANDARD TEST PROCEDURES

Muhammad Azwadi bin Abdullah

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“ I hereby declare that I have read this fully report entitled “Dielectric Performance of Different Types of Polymeric Material Under Standard Test Procedures” and found that it has comply the partial fulfillment for awarding the Bachelor of Electrical Engineering (Industrial Power)”

Signature :……….

Supervisor’s Name : DR AMINUDIN BIN AMAN

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DIELECTRIC PERFORMANCE OF DIFFERENT TYPES OF POLYMERIC MATERIAL UNDER STANDARD TEST PROCEDURES

MUHAMMAD AZWADI BIN ABDULLAH

A report submitted in partial fulfilment of the requirement for the degree of Bachelor of Electrical Engineering (Industrial Power)

Faculty of Electrical Engineering

UNIVERSITI TEKNIKAL MALAYSIA MELAKA

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I declare that this report entitle “Dielectric Performance of Different Types of Polymeric Material Under Standard Test Procedures” is the result of my own research except as cited in the references. The report has not been accepted for any degree and not concurrently submitted in candidature of any other degree.

Signature :……….

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ACKNOWLEDMENTS

Firstly, my biggest thanks to Allah S.W.T who gave me the opportunity in doing this project and always giving me hope and ways in completing the tasks.

My great appreciation goes to my supervisor, Dr. Aminudin Bin Aman for his guidance, knowledge, skill, and patience in helping his final year students for the two semesters.

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ABSTRACT

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ABSTRAK

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viii

TABLE OF CONTENTS

CHAPTER TITLE PAGE

ACKNOWLEDGEMENT v

ABSTRACT vi

ABSTRAK vii

TABLE OF CONTENTS viii

LIST OF FIGURES ix

LIST OF TABLES xiii

LIST OF ABBREVIATION xv

LIST OF APPENDICES xvi

1 INTRODUCTION 1

1.1 Introduction 1

1.2 Project Motivation 2

1.3 Problem Statement 3

1.4 Objectives 3

1.5 Scope 4

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2 LITERATURE REVIEW 5

2.1 Introduction 5

2.2 Degradation and breakdown 5

2.2.1 Electrical field stress 5 2.2.2 Short- term breakdown 6

2.2.3 Long- term breakdown 6

2.2.4 Accelerated Ageing Test 7 2.3Solid Dielectric Insulating System 9

2.3.1 Organic material 9

2.3.2 Inorganic Material 10

2.3.3 Synthetic Polymer 11

2.4 Selection Material 12

2.4.1 Polyvinyl chloride (PVC) 12

2.4.2 Polypropylene (PP) 12

2.4.3 Polyethylene High Density (HDPE) 13 2.5 Reviews of Electrical Properties Test 14

2.6 Summary 16

3 METHODOLOGY 17

3.1 Introduction 17

3.2 Flowchart of Methodology 18

3.3 Standard Test Procedure 19

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x

3.3.2 Tests perpendicularly to the surface of

Specimen materials 19

3.3.2.1 Boards and sheet materials 19

3.3.2.1.1 Unequal electrodes 19

3.3.2.1.2 Equal diameter electrodes 20

3.2.2.1.3 Tests on thick sample 21 3.3.3 Number of tests 21

3.3.4 conditioning before tests 21

3.3.5Mode of increase of voltage 21

3.3.5.1 Short- Times (Rapid-Rise) Test 22

3.3.6 Voltage Source 22

3.3.7 Criterion of Breakdown 23 3.4 Preparing of test specimen 24 3.4.1 Category & Test parameter of specimen 24 3.4.2 Hydraulic molding test procedure 25 3.4.3 Specimen Preparation Process 26

3.4.4 Operation of Hot Press Machine (Gotech-Gt 7014) 28 3.4.5 Sample of Specimen 29 3.5 Experiment Setup of AC Test 31 3.5.1 Apparatus of High Voltage Test 31 3.5.2 Procedure of Dielectric Strength Test 33

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4 RESULTS & DISCUSSION 37

4.1Introduction 37

4.2 Test Conditions of Dielectric Strength Test 37

4.3 Result of Project 38

4.3.1 Breakdown Voltage of Specimen 39

4.4 Discussion 40

4.4.1 Breakdown Voltage of Polyvinyl Chloride (PVC) 40 4.4.2 Breakdown Voltage of Polypropylene (PP) 41 4.4.3 Breakdown Voltage of High Density Polyethylene

(HDPE) 42

4.5 Dielectric Strength Performance of All Type of Polymer 44 4.6Phenomena of AC Voltage Test 46 4.7 Validation of Result

5 CONCLUSION & RECOMMENDATION 48

5.1 Conclusion 48

5.2 Recommendation 49

REFERENCES 50

APPENDICES 52

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LIST OF FIGURES

FIGURE TITLE PAGE

2.1 A diagnostic test to determine the ageing 8

2.2 Overview of the project 16

3.1 Flowchart of Methodology 18

3.2 (a) Unequal electrodes 20

3.2 (b) Equal diameter electrodes 20

3.3 Dimension of molding plate 26

3.4 Weighting raw material 26

3.5 Molding plate filled with the raw material 27

3.6 Hot press machine (Gotech-GT 7014) 27

3.7 Specimen of PVC 29

3.8 Specimen of PP 30

3.9 Specimen of HDPE 30

3.10 Schematic diagram of AC test setup 31 3.11 Electrode set-up to comply with BS EN 60243-1 32 3.12 High voltage control and measurement equipment 33

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3.14 Actual dielectric strength test setup 34

3.15 Breakdown occurs at test setup 34

3.16 Cage with interlock system 36

4.1 Captured AC wave during breakdown voltage of PVC 40 4.2 Graph waveform breakdown voltage of PVC 41 4.3 Captured AC wave during breakdown voltage of PP 41 4.4 Graph waveform voltage breakdown of PP 42 4.5 Captured AC wave during breakdown voltage of HDPE 42 4.6 Graph waveform voltage breakdown of HDPE 43

4.7 Breakdown voltage of polymer in kV 43

4.8 Breakdown voltage of polymer in kV/mm 44 4.9 Average breakdown voltage of polymer 45

4.10 Corona before breakdown occurs 46

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LIST OF TABLES

TABLE TITLE PAGE

2.1 Organization of solid insulation materials 9 2.2 Important properties and minimum requirement of

Polymeric insulation 15

3.1 Category & test parameter of specimen 24 3.2 The setting time and pressure of specimen 28 4.1 Specimen conditions under dielectric strength test 38

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LIST OF ABBREVIATION

PE – Polyethylene. PVC – Polyvinyl chloride PP – Polypropylene

HPE – High Density Polyethylene

ANSI – American National Standard Institute IEC – International Electrotechnical Commission

CIGRE –The International Council on Large Electric Systems

NEMA – National Electrical Manufacturers Association BS – British Standard

HV – High Voltage

IEEE – Institute of Electrical and Electronics Engineers AC – Alternating Current

OT – Operation Terminal

DMI – Digital Measuring Instruments

KV – Kilovolt

r.m.s –root mean square

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xvi

LIST OF APPENDICES

APPENDICES TITLE PAGE

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CHAPTER 1

INTRODUCTION

1.1 Introduction

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2

1.2 Project Motivation

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3

1.3 Problem Statement

Today a lot of research has been done on the electrical properties of high voltage insulation materials. Normally, there are two types of test can be conducted, standard test used for product test and non-standard test for research work. Where, the breakdown tests are conducted for the analysis of the dielectric strength, performance of polymeric insulation material properties. The high voltage testing used to material in order to get insulation characteristic.Since this experiment generates high voltages, compulsory handling steps and safety precaution need to be taken when handling the equipment. The safety precautions cover the laboratory safety, equipment, safety and user safety. Therefore, the standard test procedure accordingly to international standard is vital to be complied and must follow to get reliable results. And by referring to the British Standard Institution. Selection guide for polymeric materials for outdoor use under HV stress. PD IEC/TR 62039.2007 [6]. The minimum dielectric strength to be fulfilled for outdoor high voltage polymeric insulation shall not be less than 10kV/mm. In order to testing the dielectric strength of the polymer insulation, the international standard BS EN 60243-1:1998 is used. [7].

1.4 Objective

The objectives for this project are stated as follows:

1. To familiarize with high voltage lab testing and procedures.

2. To set up the experiment based on dielectric strength standard. 3. To investigate breakdown characteristics of polymeric material in insulation.

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1.5 Scope of Research

This main scope of this research to studies, investigate and observe the dielectric performance of polymeric material. For this study polymeric material to be studied are Polyvinyl Chloride (PVC), Polypropylene (PP), and high density Polyethylene (HDPE). For dielectric testing procedure the test was conducted by complying with international standard BS EN 60243-1:1998 with the flat sheet test requirement. This test needs to conduct according to specific parameter such as by following the voltage reference in Malaysia at the power frequency level ≈ 50Hz and have safety precaution when doing the testing. Lastly, by setup experiment according to standard, the result of withstanding voltage of the material can be used to analysis the polymeric material and are more reliable to be used as a reference in other studies.

1.6 Outline of Report

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CHAPTER 2

LITERATURE REVIEW

2.1 Introduction

Insulation shows a very important part in determining the performance and lifespan of high voltage equipment. This chapter covers all the related study the characteristic of polymer insulators. It also describes the Development of polymeric insulation, Reviews of Electrical Properties Test, appropriate tests, detection of surface features, standards related to methods

2.2 Degradation and breakdown

2.2.1 Electrical field stress

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material depends on various parameters, such as pressure, temperature, humidity, type of applied voltage, defects in the dielectric materials, material electrodes and electrode surface conditions. The main reason for the presence of insulation failure in the release of either voids in the insulation or on the surface of the insulation [1]

2.2.2 Short- term breakdown

Electric field due to the very high stresses may not occur in the second or faster without damaging the insulation surface before failure.

2.2.3 Long- term breakdown

Breakdown of long-term aging is also known as insulation. The main effects eventually responsible for the aging of insulation, lead to the damage arising from the heat and partial discharge.

i. Ageing and Breakdown due to partial discharge.

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2.2.4 Accelerated Ageing Test

Aging of polymer insulators depending on the chemical and physical properties of materials and stress exposure. In this case, the aging factor can be determined by careful examination whether directly or indirectly. Although, several international organizations and national standards provided for accelerated life tests such as IEEE, IEC, CIGRE, ANSI, BS and NEMA, there are no specific standards that apply to all applications and conditions. This means that the lack of standards means test all materials. As a continuation of material technology, manufacturing often adjust the current test to suit different products [8].

These tests are designed to reveal the performance of the materials and the pressure is divided into four components, test the electrical properties, mechanical properties testing, physical and chemical testing environmental testing. Typically, the surface condition of polymeric materials under test is used as a diagnostic tool to represent the level of performance and aging. Continuity of technology, manufacturing often adjusts the current test to suit different products [8].

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