Jenis pengujian atau sifat-sifat yang diukur

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Bidang pengujian

yang diuji sifat-sifat yang diukur teknik yang digunakan Keterangan

Kimia Asap rokok utama (mainstream smoke) :

- Jumlah partikel pada asap (TPM/ Total Particulate Matter) ISO 4387:2000 - Tar (Nicotine-free dry particulate matter) ISO 4387:2000

- Nikotin (nicotine) ISO 10315:2000

- Air ISO 10362-1:1999

- Carbon monoksida (CO) ISO 8454:2007

- Jumlah hisapan (puff number) PMI Q0338 (pengukuran jumlah hisapan)

- Eugenol PMI Q0338 (preparasi)

CHE/MTD/002 (GC) Asap rokok utama (mainstream smoke) :

- Air (water) ISO 10362-1:1999

- Eugenol PMI Q0338 (preparasi)

CHE/MTD/002 (GC)

- Menthol PMI Q0338 (preparasi)

CHE/MTD/018 (GC) Rokok kretek (SKT/ sigaret kretek

tangan dan SKM/sigaret kretek mesin)

Rokok kretek (SKM) mengandung menthol

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Kimia Rokok putih (SPM) Asap rokok utama (mainstream smoke) :

- Air ISO 10362-1:1999

- Carbon monoksida (CO) ISO 8454:2007

- Benzo(ά)pyrene Coresta Recommended Method No. 58, 2004

Asap rokok utama (mainstream smoke) :

- Jumlah partikel pada asap (TPM/Total Particulate Matter ) ISO 4387:2000 - Tar (Nicotine-free dry particulate matter) ISO 4387:2000

- Air (water) ISO 10362-1:1999

- Menthol PMI Q0328 (GC)

- Kadar menthol dalam rokok, blend dan filter PMI Q0126(GC) Asap rokok samping, sidestream smoke:

- Jumlah partikel pada asap (TPM/Total Particulate Matter ) Coresta Recommended Method No. 54, 2002 - Tar (Nicotine-free dry particulate matter) Coresta Recommended Method No. 54, 2002

- Nikotin (nicotine) Coresta Recommended Method No. 54, 2002

- Air (water) Coresta Recommended Method No. 54, 2002

- Carbon monoksida (CO) Coresta Recommended Method No. 55, 2002

Penandatangan sertifikat/laporan : Wuryanto; Remy Dinar Prasasti; Rina Apriani; Pangastuti Sri Handayani; Tunggal Saptantyo; Sulistiyani; Asti Ardhyo Febrianti

Rokok putih (SPM) mengandung menthol

Rokok kretek (SKM) dan rokok putih (SPM)

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Kimia Total alkaloid Coresta Recommended Method No. 35, 1994

Klorida (chloride) Coresta Recommended Method No. 38, 1994

Reducing carbohydrates CHE/MTD/005 (Kolorimetri)

Nitrate Coresta Recommended Method No. 36, 1994

Ammonia PMI Q0202 (Kolorimetri)

Eugenol CHE/MTD/009 (GC)

Total alkaloid Coresta Recommended Method No. 35, 1994

Bahan pereduksi (reducing substances) Coresta Recommended Method No. 37, 1994

Klorida (chloride) CHE/MTD/005 (Kolorimetri)

Reducing sugar Coresta Recommended Method No. 37, 1994

Cengkeh Eugenol CHE/MTD/009 (GC)

Menthol CHE/MTD/010 (GC)

Triacetine PMI Q0321

Kimia Tembakau Residu bahan aktif

- Acetamiprid CHE/MTD/060 (LC-MS/MS)

- Alachlor CHE/MTD/060 (LC-MS/MS)

- Azinphos methyl CHE/MTD/060 (LC-MS/MS)

- Benalaxyl CHE/MTD/060 (LC-MS/MS)

- Bendiocarb CHE/MTD/060 (LC-MS/MS)

- Butralin CHE/MTD/060 (LC-MS/MS)

- Carbaryl CHE/MTD/060 (LC-MS/MS)

Penandatangan sertifikat/laporan : Wuryanto; Remy Dinar Prasasti; Rina Apriani; Pangastuti Sri Handayani; Tunggal Saptantyo; Sulistiyani; Asti Ardhyo Febrianti Tembakau dan blend rokok putih

Blend rokok kretek

Alumunium foil pembungkus rokok mengandung menthol

Batang filter, filter rokok kretek (SKM) dan filter rokok putih (SPM)

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Kimia Tembakau (lanjutan) Residu bahan aktif (lanjutan): - Carbendazim CHE/MTD/060 (LC-MS/MS) - Carbofuran CHE/MTD/060 (LC-MS/MS) - Chlorfenvinphos CHE/MTD/060 (LC-MS/MS) - Clomazone CHE/MTD/060 (LC-MS/MS) - Demeton-S-metyl CHE/MTD/060 (LC-MS/MS) - Diazinin CHE/MTD/060 (LC-MS/MS) - Diflubenzuron CHE/MTD/060 (LC-MS/MS) - Dimthoate CHE/MTD/060 (LC-MS/MS) - Dimethomorph CHE/MTD/060 (LC-MS/MS) - Diphenamid CHE/MTD/060 (LC-MS/MS) - Diuron CHE/MTD/060 (LC-MS/MS) - Ethiofencarb CHE/MTD/060 (LC-MS/MS) - Fenamiphos CHE/MTD/060 (LC-MS/MS) - Fenthion CHE/MTD/060 (LC-MS/MS) - Imidacloprid CHE/MTD/060 (LC-MS/MS) - Isopropalin CHE/MTD/060 (LC-MS/MS) - Linuron CHE/MTD/060 (LC-MS/MS) - Malathion CHE/MTD/060 (LC-MS/MS) - Metalaxyl CHE/MTD/060 (LC-MS/MS) - Methidathion CHE/MTD/060 (LC-MS/MS) - Methiocarb CHE/MTD/060 (LC-MS/MS) - Metobromuron CHE/MTD/060 (LC-MS/MS) - Metolachlor CHE/MTD/060 (LC-MS/MS)

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Kimia Tembakau (lanjutan) Residu bahan aktif (lanjutan):

- Metoxuron CHE/MTD/060 (LC-MS/MS) - Monocrotophos CHE/MTD/060 (LC-MS/MS) - Monuron CHE/MTD/060 (LC-MS/MS) - Oxadixyl CHE/MTD/060 (LC-MS/MS) - Pendimethalin CHE/MTD/060 (LC-MS/MS) - Phorate CHE/MTD/060 (LC-MS/MS) - Phoxim CHE/MTD/060 (LC-MS/MS) - Pirimicarb CHE/MTD/060 (LC-MS/MS) - Profenofos CHE/MTD/060 (LC-MS/MS) - Promecarb CHE/MTD/060 (LC-MS/MS) - Propoxur CHE/MTD/060 (LC-MS/MS) - Thiabendazole CHE/MTD/060 (LC-MS/MS) - Vamidothion CHE/MTD/060 (LC-MS/MS)

Residu bahan aktif :

- Acephate CHE/MTD/061 (GC-FPD)

- Azinphos ethyl CHE/MTD/061 (GC-FPD)

- Bromophos-ethyl CHE/MTD/061 (GC-FPD)

- Bromophos-metyl CHE/MTD/061 (GC-FPD)

- Chlorpyrifos CHE/MTD/061 (GC-FPD)

- Chlorpyrifos-methyl ester CHE/MTD/061 (GC-FPD)

- Dichlorvos CHE/MTD/061 (GC-FPD)

- Dimefox CHE/MTD/061 (GC-FPD)

- Dioxabenzofos CHE/MTD/061 (GC-FPD)

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Kimia Tembakau (lanjutan) Residu bahan aktif (lanjutan) :

- Disulfoton CHE/MTD/061 (GC-FPD)

- Ethoprophos CHE/MTD/061 (GC-FPD)

- Ethyl parathion CHE/MTD/061 (GC-FPD)

- Fenamiphos CHE/MTD/061 (GC-FPD)

- Fenamiphos sulfone CHE/MTD/061 (GC-FPD)

- Fenamiphos sulfoxide CHE/MTD/061 (GC-FPD)

- Fenchlorphos CHE/MTD/061 (GC-FPD) - Fenithrothion CHE/MTD/061 (GC-FPD) - Fensulfothion CHE/MTD/061 (GC-FPD) - Fonofos CHE/MTD/061 (GC-FPD) - Formotion CHE/MTD/061 (GC-FPD) - Methamidhopos CHE/MTD/061 (GC-FPD)

- Methyl parathion CHE/MTD/061 (GC-FPD)

- Mevinphos CHE/MTD/061 (GC-FPD)

- Naled CHE/MTD/061 (GC-FPD)

- Phosalone CHE/MTD/061 (GC-FPD)

- Phosphamidon CHE/MTD/061 (GC-FPD)

- Pirimiphos-methyl ester CHE/MTD/061 (GC-FPD)

- Terbufos CHE/MTD/061 (GC-FPD)

- Tetrachlorvinphos CHE/MTD/061 (GC-FPD)

- Thionazin CHE/MTD/061 (GC-FPD)

- Trichlorfon CHE/MTD/061 (GC-FPD)

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Kimia Tembakau (lanjutan) Residu bahan aktif :

- Aldrine CHE/MTD/062 (GC-ECD)

- Chlorothalonil CHE/MTD/062 (GC-ECD)

- Chlorthal dimethyl CHE/MTD/062 (GC-ECD)

- cis-Chlordane CHE/MTD/062 (GC-ECD)

- trans-Chlordane CHE/MTD/062 (GC-ECD)

- lamda-Cyhalothrin CHE/MTD/062 (GC-ECD)

- Cyfluthrin CHE/MTD/062 (GC-ECD)

- Cypermethrin CHE/MTD/062 (GC-ECD)

- 2.4-DDD CHE/MTD/062 (GC-ECD)

- 4.4-DDD CHE/MTD/062 (GC-ECD)

- 2.4-DDE CHE/MTD/062 (GC-ECD)

- 4.4-DDE CHE/MTD/062 (GC-ECD)

- 2.4-DDT CHE/MTD/062 (GC-ECD)

- 4.4-DDT CHE/MTD/062 (GC-ECD)

- alpha-HCH CHE/MTD/062 (GC-ECD)

- betha-HCH CHE/MTD/062 (GC-ECD)

- delta-HCH CHE/MTD/062 (GC-ECD)

- gamma-HCH CHE/MTD/062 (GC-ECD)

- Deltamethrin CHE/MTD/062 (GC-ECD)

- Dicloran CHE/MTD/062 (GC-ECD)

- Dicofol CHE/MTD/062 (GC-ECD)

- Dieldrine CHE/MTD/062 (GC-ECD)

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- alpha-Endosulfan CHE/MTD/062 (GC-ECD)

- beta-Endosulfan CHE/MTD/062 (GC-ECD)

- Endosulfan sulfate CHE/MTD/062 (GC-ECD)

- Endrin CHE/MTD/062 (GC-ECD)

- Fenvalerate CHE/MTD/062 (GC-ECD)

- Flucythrinate CHE/MTD/062 (GC-ECD)

- Heptachlor CHE/MTD/062 (GC-ECD)

- Heptachlor endo epoxide CHE/MTD/062 (GC-ECD)

- Heptachlor exo epoxide CHE/MTD/062 (GC-ECD)

- Hexachlorobenzene CHE/MTD/062 (GC-ECD)

- Isopropalin CHE/MTD/062 (GC-ECD)

- Methoxychlor CHE/MTD/062 (GC-ECD)

- Nitrofen CHE/MTD/062 (GC-ECD)

- Permenthrin CHE/MTD/062 (GC-ECD)

- Quintozene CHE/MTD/062 (GC-ECD)

- Trifluralin CHE/MTD/062 (GC-ECD)

- Chlordimeform CHE/MTD/066 (GC-MS/MS)

- Chlorobenzilate CHE/MTD/066 (GC-MS/MS)

- DBCP CHE/MTD/066 (GC-MS/MS)

- Disulfoton sulfone CHE/MTD/066 (GC-MS/MS)

- Ethofumesate CHE/MTD/066 (GC-MS/MS)

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- Flumetralin CHE/MTD/066 (GC-MS/MS)

- Mirex CHE/MTD/066 (GC-MS/MS)

- Monolinuron CHE/MTD/066 (GC-MS/MS)

- Napropamide CHE/MTD/066 (GC-MS/MS)

- Pebulate CHE/MTD/066 (GC-MS/MS)

- Piperonyl butoxide CHE/MTD/066 (GC-MS/MS)

- Pentachloroanisole CHE/MTD/066 (GC-MS/MS)

- Aldicarb CHE/MTD/067 (HPLC-FLD)

- Aldicarb Sulfone CHE/MTD/067 (HPLC-FLD)

- Aldicarb Sulfoxide CHE/MTD/067 (HPLC-FLD)

- Aminocarb CHE/MTD/067 (HPLC-FLD)

- Methomyl CHE/MTD/067 (HPLC-FLD)

- Oxamyl CHE/MTD/067 (HPLC-FLD)

- Thiodicarb CHE/MTD/067 (HPLC-FLD)

Dithiocarbamates (EBDC) PMI Method QR2660.M100

Tobacco-specific Nitrosamine (TSNA) :

- NAB (N-Nitrosoanabasine) PMI Method QR2660.M220 (LC-MS/MS)

- NAT (N-Nitrosoanatabine) PMI Method QR2660.M220 (LC-MS/MS)

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Kimia Tembakau (lanjutan) Tobacco-specific Nitrosamine (TSNA) (lanjutan):

- NNK (4-(methyl-nitrosamino)-1-(3-pyridyl)-1-butanone) PMI Method QR2660.M220 (LC-MS/MS)

- NNN (N-Nitrosonornicotine) PMI Method QR2660.M220 (LC-MS/MS)

- Benzo(ά)pyrene Coresta Recommended Method No. 58, 2004

Nicotine & Minor Alkaloids :

- Anabasine PMI Method QR2660.M300 (GC-NPD)

- Anatabine PMI Method QR2660.M300 (GC-NPD)

- Nicotine PMI Method QR2660.M300 (GC-NPD)

- Nornicotine PMI Method QR2660.M300 (GC-NPD)

- Myosmine PMI Method QR2660.M300 (GC-NPD)

Rokok putih dan rokok kretek Hydroquinone Health Canada Method No.T-114, 1999

Resorcinol Health Canada Method No.T-114, 1999

Catechol Health Canada Method No.T-114, 1999

Phenol Health Canada Method No.T-114, 1999

m+p Cresol Health Canada Method No.T-114, 1999

o-Cresol Health Canada Method No.T-114, 1999

NAB (N-Nitrosoanabasine) PMI Method QR2540.M026 (LC-MS/MS)

NAT (N-Nitrosoanatabine) PMI Method QR2540.M026 (LC-MS/MS)

NNK (4-(methyl-nitrosamino)-1-(3-pyridyl)-1-butanone) PMI Method QR2540.M026 (LC-MS/MS)

NNN (N-Nitrosonornicotine) PMI Method QR2540.M026 (LC-MS/MS)

Ammonia Health Canada Method No.T-116, 1999

1,3-Butadiene Health Canada Method No.T-116, 1999

Isoprene Health Canada Method No.T-116, 1999

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Kimia Acrylonitrile Health Canada Method No.T-116, 1999

Benzene Health Canada Method No.T-116, 1999

Toluene Health Canada Method No.T-116, 1999

Acetaldehyde Health Canada Method No.T-104, 1999

Acetone Health Canada Method No.T-104, 1999

Acrolein Health Canada Method No.T-104, 1999

Butyraldehyde Health Canada Method No.T-104, 1999

Crotonaldehyde Health Canada Method No.T-104, 1999

Formaldehyde Health Canada Method No.T-104, 1999

Methyl ethyl ketone Health Canada Method No.T-104, 1999

Propionaldehyde Health Canada Method No.T-104, 1999

1-Aminoaphtalene Health Canada Method No.T-102, 1999

2-Aminonaphtalene Health Canada Method No.T-102, 1999

3-Aminobiphenyl Health Canada Method No.T-102, 1999

4-Aminobiphenyl Health Canada Method No.T-102, 1999

Benzo(ά)pyrene Coresta Recommended Method No. 58, 2004

Pyridine Health Canada Method No.T-112, 1999

Quinoline Health Canada Method No.T-112, 1999

Styrene Health Canada Method No.T-112, 1999

Penandatangan sertifikat/laporan : Sonyarita Yulia Susianti; Rahma Hidayat; Wisnu Mahendra Rokok putih dan rokok kretek

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Fisika Berat individu (individual weight) PMI Q0370 (Gravimetri)

Keliling (circumference) PMI Q0370 (Pemindaian laser)

Resistance to Draw (RTD) PMI Q0370 (Pengukuran tekanan udara)

Ventilasi (Ventilation) PMI Q0370 (Pengukuran kecepatan aliran udara)

Kekerasan (Firmness) PMI Q0312 (Pengukuran dimensi)

Batang filter Keliling (circumference) PMI Q0371 (Pemindaian laser)

Resistance to Draw (RTD) PMI Q0371 (Pengukuran tekanan udara)

Rokok putih (SPM), tembakau Oven volatile PMI Q0210 (Gravimetri)

Ketebalan (thickness) ISO 534:2005

Gramatur (Grammage) ISO 536:1995

Permeabilitas kertas ISO 2965:1997

Brightness ISO 2470:1999

Opacity ISO 2471:2008

Plugwrap Permeabilitas kertas ISO 2965:1997

Tanggal : 30 Desember 2009

Disahkan oleh Ketua Komite Akreditasi Nasional: Kertas, karton, alumunium foil Kertas rokok, tipping

Penandatangan sertifikat/laporan : Wuryanto; Remy Dinar Prasasti; Rina Apriani; Pangastuti Sri Handayani; Tunggal Saptantyo; Ani Tri Kumalawati; Husna Wardani Rokok (SKM & SPM)