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Electrical impedance

tomographic sensor

systems

K. Primrose and

C. Qiu

Electrical methods of sensing material distributions in industrial processes, using tomographic techniques, have been under scientific and technological development over the past decade. Williams and Beck (1995) provided a collected review that is still useful in reviewing the core major technologies. Continuing growth and interest is illustrated in the proceedings of the recent First World Congress in Industrial Process Tomography (Virtual Centre for Industrial Process Tomography ± VCIPT, 1999).

The electrical impedance tomography (EIT) method consists of either injecting currents (or alternatively applying voltages), in the region of interest and measuring voltages (or currents) via a number of electrodes that are mounted non-intrusively, but invasively, on its boundary.

Early EIT instruments were targeted at clinical observations, for example in lung perfusion studies. In contrast, an EIT system for process applications must offer maximum flexibility to suit a range of applications, for example: liquid-liquid and/or liquid-solid mixing processes; cyclonic and dense medium separation; and, hydraulic transportation in pipelines.

A major interest has been to enhance knowledge of the internal behaviour of the process with a view to optimising design. At this early stage in the application of the technology, improvement in process performance varies from case to case. Thus while a standard instrument format can be devised to extract information, a flexible approach must be taken to translate this information into enhanced performance.

A number of well-understood approaches exist for the transfer of technology from research to application. Industrial

Tomography Systems (ITS) has found the optimal solution to centre on a consultancy service which supports organisations interested in applying the new technology. This typically includes the supply of a tailored prototype EIT system. A project will feature a close dialogue with the customer to ensure that applications selected are amenable to process improvement through tomography. While this takes time it provides an

opportunity to build a deeper understanding of the application. Over the last three years the process has developed with an iterative

The authors

K. PrimroseandC. Qiuare with Industrial Tomography Systems Ltd, 47 Newton Street, Manchester M1 1FT, UK. E-mail: [email protected]; WWW: www.itoms.com

Keywords

Imaging, Tomography, Sensors

Abstract

This paper reviews aspects of the current status of process sensing using electrical impedance process tomography. This new sensor technology offers a unique insight into a wide range of industrial processes. Applications include a range of processes that feature complex flows and multiple component interactions. The paper provides an overview of hardware and software technology in terms of an instrument currently targeted at pilot trials through a consultancy service. Finally a case study is used to illustrate a typical application in which a detailed insight into an otherwise intractable process has been obtained.

Electronic access

The research register for this journal is available at

http://www.mcbup.com/research_registers/aa.asp

The current issue and full text archive of this journal is available at

http://www.emerald-library.com

Sensor Review

Volume 20 . Number 3 . 2000 . pp. 189±194

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loop in developing the tomography system itself, designed to explore the following critical aspects:

. access to process plant (including safety); . flow conditions (rate and composition); . time-scale of process measurement; . measurement output (homogeneity, gas

hold-up, relative concentration etc); . process control methodology.

The process control methodology is often refined in the course of the technology transfer process. These refinements relate to the extent to which a single control variable is required or the need for full 3-dimensional visualisation of the process behaviour. Proper design of sensor electrode systems is a most critical part of the process. Once process benefits have been achieved, there is greater confidence in the company for applying tomography elsewhere in its business.

System overview

An accurate and stable data acquisition sub-system (DAS) is a critical part of an EIT instrument. This facilitates the low amplitude measurements required at the region of interest boundary. These typically are of the order of millivolts, and feature dynamic changes of the order of microvolts. It must also support a large number of electrode channel operations. For example a minimum of 104 measurements are needed for 16 electrodes, with high common mode voltages.

The current ITS P2000 prototype base system has a specification designed to maintain flexibility and accuracy over a diverse range of process parameters:

. injected alternating current bandwidth ± 75Hz up to 150kHz;

. injected alternating current amplitude ± 0 to 75mA (peak-to-peak);

. various current injection methods ± adjacent, opposite, multi-reference, and conducting boundary strategies;

. maximum of 64 electrodes either in a single, or over multiple planes.

To suit a wide range of process vessel size and process material electrical conductivity, there is a need to vary the amplitude of injected currents in order to optimise the

measurement signal-to-noise ratio (SNR). Also, for slowly changing processes, such as sedimentation in a viscous medium, more

accurate measurements are facilitated at lower frequencies of injected current, hence the motivation for the ranges given in the first two requirements above.

The requirement to accommodate several different methods of injecting alternating current is readily achievable by utilising more than one current source/sink pair. The adjacent and opposite electrode pairs

methods only require one current source and sink pair, thereby minimising the complexity of the associated circuitry. Conversely, the multi-reference method requires that all but one of the electrodes have an identical fixed amplitude current source attached. The corresponding voltage measurement is taken across a grounded load connected to the free electrode. The conducting boundary strategy is an alternative method in which the current injection is performed between one of the electrodes and the conducting boundary. The resultant boundary voltages being measured from each of other electrodes with respect to the conducting boundary.

The final specification enables up to 64 fixed-amplitude current sources to be attached to the process vessel. These can be arranged across several layers, to meet the requirement of the multi-layered imaging, or across a single layer to enhance the spatial resolution which is generally proportional to the number of unique measurements.

The ITS EIT system is shown in schematic form in Figure 1. It has the following sub-systems, taking the numbered units commencing at the bottom left corner in a clockwise direction. First the voltage generator (1), and the electrode current injection unit (2), which drives each electrode on the process vessel, followed by its control module (3). This is followed by the voltage measurement, demodulation and filtering unit (4). Finally the microcontroller (5) co-ordinates the various sub-systems.

The system is housed in a standard rack suited to pilot plant use, as illustrated in Figure 2 (utilising two out of eight possible planes).

In order to obtain the voltage measurement from the boundary of the domain of interest, an electrical signal, in the form of a voltage or current, is necessary in order to ``probe'' the domain. The design of this system is a critical factor to suit a wide variety of process applications. The four-electrode

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majority of applications to minimise the errors caused by contact impedance at the electrode-process material interface. The transient time arising from the contact impedance is also affected when a voltage injection is adopted. A current injection strategy is therefore selected in the ITS instrument. The device also has a trigger function that is important for data collection, e.g. gating to a mixing, chemical or other process transient.

The data collection speed of an EIT system is mainly limited by the filter in the voltage measurement stage, and its associated couplings, when analogue demodulation is adopted. In the ITS design, modules are available to satisfy differing requirements. The fastest speed of collection for a frame of

104 measurements is 35ms at 38.4kHz, using the digital demodulation option, and 150ms using the analogue demodulation option (see Figure 3).

The repeatability and stability of the DAS are important for a system targeted to industrial use. Repeatability is illustrated through a test of 100 data frames acquired sequentially from a test vessel filled with mains tap-water (0.096mS/cm conductivity at room temperature of 23.1C) using a current of 5 mA (absolute value). Maximum

deviation was less than 0.5 per cent. Stability can also be illustrated using the same experimental conditions through the comparison of two frames of data acquired with an intervening interval. Deviation was found to be less than 0.6 per cent after two hours. Average values of repeatability and stability were less than 0.2 per cent. Key features of the instrument that has formed the base for a wide range of pilot trials are summarised in Table I.

User interface and software

The DAS is coupled to a Pentium (or better) based PC running the Microsoft Windows Figure 1The ITS EIT system in schematic form

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operating system. No special computer hardware is required and the connection utilises a standard serial port.

The P2000 system includes a software package that allows measurement

programmes to be set up and controlled with

data review/analysis feasible both online and offline. Multiple data sets can be compared simply. Data reconstruction and analysis software is supplied in a library format. A range of core and interpretation modules are available:

Figure 3Measurement, demodulation and filtering sub-systems

Table IKey features of P2000 system

P2000 system specification

Microcontroller Intel 80C32

Clock speed 22.1184 MHz

Memory 32 Kbytes ROM, 2MB RAM

Sinewave generator Zero order hold staircase wave

Oscillator 9.8304 MHz

Number of samples 1. 2. 4. 8

Harmonic content ±65 dB @38.4 kHz for 2nd order

Injection frequency 75 Hz-153.6* kHz [in 12 steps]

Injecting current 0-1.5, ±15, ±75mA(ad-ad) [in 256 steps]

Current inj. methods adjacent, conducting boundary

Max. no. electrodes 128

Measurement range ±10 V (pp) to +10 V (pp)

Sensitivity 4.88 uV @gain1000

CMRR > ±70 db @153.6 kHz

Accuracy ‹ 0.5% (@9.6 kHz)**

Repeatability < 0.5% per 100 frames (@9.6 kHz, 21.8C)**

Stability < 0.6% (@9.6 kHz, 2 hours @21.8C)**

ADC resolution 12 bits

Sample window 0.3 us

Conversion speed 3 us

Mode of measurement Sequential

Type of demodulation Phase sensitive demodulation

Phase shift compensation 0.7to 180

Acquisition speed for one frame from DAS < 20 ms (digital demodulation, @9.6 kHz, 16 electrodes)

Max no. frame of group 9000 (16 electrodes)

Serial data interface RS-232c

Baud rate 9600Hz 115200Hz

Size of PCBs Eurocard

Power consumption DC 24 V 45W (power adapter output into DAS)

Power input from mains supply 100-240 V a/c, 50/60 Hz 1.5A

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. instrumentation core module (P2000 system control and data viewing); . viewer core module (for separate off-line

data review);

. process evolution interpretation module (includes pixel history and stacked plane view);

. statistical interpretation module (includes pixel analysis and homogeneity index).

Figure 4 shows the process evolution data analysis module which allows reconstructed images to be sliced, animated and

interrogated at the pixel level.

A further example of data analysis is also given in the case study below.

Case study

To illustrate a typical industrial application, we consider the first stage in a feasibility study of applying EIT to the study of a bubble column. Here the target set was to see what information could be obtained from the simplest possible array of electrodes. Hence only one ring of electrodes was retrofitted into the column section, as shown in Figure 5.

The EIT system was used in conjunction with an independent (calibration) method of injected gas flux in an attempt to estimate:

. gas hold up;

. homogeneity of gas bubble dispersion; . flow state of the column.

Gas was injected at different rates whilst monitoring the response from the 16

Figure 4Windows data viewer showing two tomographic slices in z plane and one image of 25 slices stacked in x and y planes. Colour code relates to conductivity in mS/cm

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electrodes at a frame rate of 1Hz. This represents a low specification and demand on the instrumentation, but was used to assess the capabilities of such a minimal

specification. Figure 6 shows the results. Figure 6(a) provides a time-scrolling animation of the gas distribution, as identified with an iso-contour visualisation, with the instantaneous (current time) image at the top of the stack. The light coloured regions correspond to non-conducting gas phase. The squat appearance of the bubble clouds is due to the low image rate deployed.

Figure 6(b) shows the analysis of the process inputs (i.e. gas valve position) (lower graph) and image-derived data. This consists of an estimate of the instantaneous local gas hold-up from average conductivity (middle), and a statistical assessment of the homogeneity (top graph). The user has control over the time averaging and other features. Different methods can be used

to assess the uniformity of the bubble behaviour.

The methodology has proved effective in characterising the bubble column. By using multiple sensors arranged on such columns, the axial and radial properties of the bubble column can be assessed. Use of time-space data also enables velocity-based information to be derived. Any of these data points can be linked to data loggers through DDE links or output through a 4-20 mA control loop.

Another contrasting study which illustrates the multi-planar use of EIT to assess the detailed 3D behaviour of a range of mixing processes has recently been published by Holden et al.(1999).

Conclusion

The paper has reviewed the general application of EIT instrumentation in feasibility trials in a process-user

environment. Interaction with industry has ensured that measurements and

interpretation of resulting data conform to industrial drivers for enhanced information needs in a process monitoring and control framework. This has resulted in significant modification to process practice for example, making more use of process user-knowledge and a priori information. We anticipate a continued rapid development as the international user-base develops, spreading progressively into new fields and application sectors.

References

Holden, P.J., Wang, M., Mann, R., Dickin, F.J. and Edwards, R.B. (1999), ``On dectecting mixing pathologies inside a stirred vessel using electrical resistance tomography'',Trans I Chem E, Vol. 77, pp. 709-12.

VCIPT (1999),Proceeding of the 1st World Congress in Industrial Process Tomography, VCIPT (see www.vcipt.org).

Williams, R.A. and Beck, M.S. (Ed.), (1995),Process Tomography ± Principles, Techniques and Applications, Butterworth-Heinemann, Oxford.

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