TOTAL: PHP
36. Conduct Chemical Analysis
Analyze water for the following parameters:
pH calcium lead
acidity iron nickel
total alkalinity magnesium zinc
bicarbonate manganese arsenic
carbonate potassium mercury
total dissolved solids sodium organochlorine pesticides total suspended solids hardness (calculation polycyclic aromatic
hydrocarbons total solids from Ca & Mg total organic carbon
chloride concentration)
nitrate cadmium
phosphate chromium
sulfate copper
Analyze sediment or soil or biological for the following parameters:
moisture copper
calcium lead
iron nickel
magnesium zinc
manganese arsenic with or without moisture potassium mercury with or without moisture
sodium organochlorine pesticides with or without moisture cadmium polycyclic aromatic hydrocarbons with or without
moisture chromium
Analyze prepared solutions for the following parameters:
calcium cadmium
iron chromium
magnesium copper
manganese lead
potassium nickel
sodium zinc
Qualitative analysis of cleaned-up extracts by GC/MS
Office or Division: Research and Analytical Services Laboratory (RASL), Natural Sciences Research Institute (NSRI)
Classification: Highly Technical Type of
Transaction:
Government to Citizen, Government to Government, Government to Business
Who may avail Student, Other Government Office, Business
2883
CHECKLIST OF REQUIREMENTS WHERE TO SECURE Refer to Table of Requirements of
Samples for Analysis
RASL Accomplished Request for Analysis
Form
Proof of payment NSRI Administrative Office or UPD Cash Office CLIENT STEPS AGENCY
ACTION
FEES TO BE PAID
PROCESSING TIME
PERSON RESPONSIBLE Submit sample(s)
and accomplish appropriate Request for Analysis Form
Check
accomplished Request Form and sample(s) 1.1. prepare statement of charges 1.2. endorse sample(s) to designated Laboratory Personnel
None 10 Minutes Laboratory Personnel RASL
Pay appropriate service fee
Receive
payment and issue Official Receipt (OR)
Refer to Table of Fees
3 Minutes
Special Collecting Officer
Administrative Office or
UPD Cash Office 2.1. Perform
requested chemical analysis
None
Refer to Table of Turn-over of
Analysis
Laboratory Personnel RASL
Claim Formal Report for the requested analysis
Release RASL Formal
Report for the requested analysis
None 5 Minutes Laboratory Personnel RASL
Accomplish
Customer Survey Form
Receive
accomplished Customer Survey
None 5 Minutes Laboratory Personnel RASL
TOTAL:
TABLE OF REQUIREMENTS OF SAMPLES FOR WATER ANALYSIS A. Types of Water Analysis Available
A.1. Trace Metals
A.2. Water Quality Parameters
2884 A.3. Organic Contaminants
A.4. Pesticides, PAHs,
List of parameters and corresponding cost of analysis are given as applicable or as specified by the customer. Full payment of charges for the analysis is required upon submission of the samples for analysis.
B. Requirements/Conditions of Samples Submitted for Analysis:
pH should be analyzed immediately (preferably within 15 minutes from sampling).
Prior arrangements should be done for the determination of pH and analysis of Nitrate.
Nitrate analyses are scheduled by the analyst every Wednesday - samples should be submitted on or before Wednesday morning.
For analysis of other parameters, samples can be submitted within 24 hours from sampling without need of preservation, provided samples are kept in ice in a cooler.
The amount of sample required to be submitted depends on the analysis requested.
C. Sample Amount and Preservation Requirements of Water Samples Sample in CLEAN* PLASTIC CONTAINER and REFRIGERATED:
1 Liter pH (analyze immediately) 15 min.
1/2 Liter Acidity, Alkalinity, Bicarbonate and Carbonate 1 day
1/2 Liter Total Dissolved Solids, Total Suspended Solids,
Total Solids 7 days
Sample in CLEAN* PLASTIC CONTAINER and ACIDIFIED:
(Acidify with conc. Nitric Acid, 1.5 mL/L sample)
1 Liter Metals 6 months
Sample in CLEAN* GLASS CONTAINER and REFRIGERATED:
(Line with aluminum foil before covering) 2x100mL to 500mL Total Organic Carbon
(amber bottle, no headspace) 7 days
2x1 Liter Organochlorine Pesticides 7 days
2x1 Liter Polycyclic Aromatic Hydrocarbons 28 days
Sample in CLEAN* GLASS OR PLASTIC CONTAINER and REFRIGERATED:
1 Liter Nitrate, Phosphate 2 days
Chloride, Sulfate 28 days
*Clean plastic and glass containers with soap and water and final rinses should preferably be done with distilled water. Before filling, rinse the containers 5 times with the water being collected.
Label samples properly including date and time of sampling.
2885
TABLE OF REQUIREMENTS OF SAMPLES FOR SEDIMENT OR SOIL OR BIOLOGICAL ANALYSIS
Label samples properly including date and time of sampling.
The required amount for both organic and inorganic analysis is about 500 grams per sample, powdered and in glass container.
TABLE OF REQUIREMENTS OF SAMPLES FOR PREPARED SOLUTIONS ANALYSIS
Label samples properly including date and time of sampling.
The required amount is at least 10 mL per sample in glass container.
TABLE OF REQUIREMENTS OF SAMPLES FOR CLEANED-UP EXTRACTS BY GC/MS ANALYSIS
Label samples properly including date and time of sampling.
The required amount is at least 1 mL per sample in glass container.
TABLE OF FEES FOR WATER ANALYSIS
Fees per Sample (PHP)
Parameter UP
Students
Non-UP Students Government,
Small and Medium Scale
Industries, and Private
Institutions
Multinationals and Big Companies
pH 255.00 330.00 360.00
Chloride, Nitrate, Phosphate, Sulfate
First Analyte: 1,800.00 2,400.00 2,520.00
Succeeding Analytes 540.00 660.00 720.00
Sample Prep. for Drinking Water, Wastewater, Environmental Water
595.00 785.00 860.00
Cadmium 565.00 590.00 770.00
Calcium 565.00 590.00 770.00
Chromium 565.00 590.00 770.00
Copper 565.00 590.00 770.00
Iron 565.00 590.00 770.00
Lead 565.00 590.00 770.00
Magnesium 565.00 590.00 770.00
Manganese 565.00 590.00 770.00
Nickel 565.00 590.00 770.00
Potassium 565.00 590.00 770.00
Sodium 565.00 590.00 770.00
2886
Zinc 565.00 590.00 770.00
Hardness (Calculation from Ca and Mg conc.)
Arsenic 1,410.00 1,775.00 2,000.00
Mercury 975.00 1,125.00 1,370.00
Acidity 435.00 560.00 610.00
Total Alkalinity 860.00 1,125.00 1,245.00
Bicarbonate 440.00 580.00 640.00
Carbonate 430.00 555.00 615.00
Total Dissolved Solids 445.00 585.00 650.00
Total Solids 445.00 585.00 650.00
Total Suspended Solids 495.00 645.00 710.00
Total Organic Carbon 3,000.00 3,000.00 3,000.00
Organochlorine Pesticides /
PAH 5,720.00 8,290.00 9,715.00
Full payment required before analysis is started. Payment in check should be addressed to University of the Philippines Diliman.
TABLE OF FEES FOR SEDIMENT OR SOIL ANALYSIS
Fees per Sample (PHP) Parameter UP Students Non-UP
Students Government,
Small and Medium Scale Industries, and
Private Institutions
Multinationals and Big Companies
Moisture 430.00 560.00 660.00
Sample Preparation (w/ Moisture Analysis)
1,810.00 2,310.00 2,570.00 Sample Preparation (w/o Moisture
Analysis)
1,425.00 1,800.00 1,965.00
Cadmium 850.00 880.00 1,045.00
Calcium 850.00 880.00 1,045.00
Chromium 850.00 880.00 1,045.00
Copper 850.00 880.00 1,045.00
Iron 850.00 880.00 1,045.00
Lead 850.00 880.00 1,045.00
Magnesium 850.00 880.00 1,045.00
Manganese 850.00 880.00 1,045.00
Nickel 850.00 880.00 1,045.00
Potassium 850.00 880.00 1,045.00
Sodium 850.00 880.00 1,045.00
Zinc 850.00 880.00 1,045.00
Arsenic (w Moisture Analysis) 3,870.00 4,915.00 5,500.00 Arsenic (w/o Moisture Analysis) 3,485.00 4,410.00 4,900.00
2887
Mercury (w/ Moisture Analysis) 1,865.00 2,200.00 2,640.00 Mercury (w/o Moisture Analysis) 1,480.00 1,690.00 2,035.00 Organochlorine Pesticides /
Hydrocarbons (w/ Moisture Analysis) 7,850.00 9,450.00 11,935.00 Organochlorine Pesticides /
Hydrocarbons (w/o Moisture Analysis) 7,420.00 8,890.00 11,245.00 Full payment required before analysis is started. Payment in check should be addressed to University of the Philippines Diliman.
TABLE OF FEES FOR BIOLOGICAL ANALYSIS
Fees per Sample (PHP)
Parameter UP
Students
Non-UP Students Government,
Small and Medium Scale
Industries, and Private
Institutions
Multinationals and Big Companies
Moisture 430.00 560.00 660.00
Homogenization 240.00 300.00 300.00
Sample Preparation (w/
Moisture Analysis)
2,715.00 3,465.00 3,855.00 Sample Preparation (w/o
Moisture Analysis)
2,140.00 2,700.00 2,950.00
Cadmium 850.00 880.00 1,045.00
Calcium 850.00 880.00 1,045.00
Chromium 850.00 880.00 1,045.00
Copper 850.00 880.00 1,045.00
Iron 850.00 880.00 1,045.00
Lead 850.00 880.00 1,045.00
Magnesium 850.00 880.00 1,045.00
Manganese 850.00 880.00 1,045.00
Nickel 850.00 880.00 1,045.00
Potassium 850.00 880.00 1,045.00
Sodium 850.00 880.00 1,045.00
Zinc 850.00 880.00 1,045.00
Arsenic (w Moisture Analysis) 3,870.00 4,915.00 5,500.00 Arsenic (w/o Moisture Analysis) 3,485.00 4,410.00 4,900.00 Mercury (w/ Moisture Analysis) 2,985.00 3,460.00 4,230.00 Mercury (w/o Moisture
Analysis)
2,600.00 2,955.00 3,625.00 Organochlorine Pesticides /
Hydrocarbons (w/ Moisture
Analysis) 8,580.00 10,230.00 12,905.00
Organochlorine Pesticides / Hydrocarbons (w/o Moisture
Analysis) 8,090.00 9,600.00 12,125.00
2888
Full payment required before analysis is started. Payment in check should be addressed to University of the Philippines Diliman.
TABLE OF FEES FOR PREPARED SOLUTIONS ANALYSIS
Fees per Sample (PHP)
Parameter UP
Students
Non-UP Students Government,
Small and Medium Scale
Industries, and Private
Institutions
Multinationals and Big Companies
Cadmium 565.00 590.00 770.00
Calcium 565.00 590.00 770.00
Chromium 565.00 590.00 770.00
Copper 565.00 590.00 770.00
Iron 565.00 590.00 770.00
Lead 565.00 590.00 770.00
Magnesium 565.00 590.00 770.00
Manganese 565.00 590.00 770.00
Nickel 565.00 590.00 770.00
Potassium 565.00 590.00 770.00
Sodium 565.00 590.00 770.00
Zinc 565.00 590.00 770.00
Full payment required before analysis is started. Payment in check should be addressed to University of the Philippines Diliman.
TABLE OF FEES FOR CLEANED-UP EXTRACTS BY GC/MS ANALYSIS Fees per Sample (PHP)
Parameter UP
Students
Non-UP Students Government,
Small and Medium Scale
Industries, and Private
Institutions
Multinationals and Big Companies
Instrumentation 2,530.00 3,750.00 4,875.00
Full payment required before analysis is started. Payment in check should be addressed to University of the Philippines Diliman.
Table of Turn-over of Results of Analysis
Analysis No. of samples Regular Turn-over (No. of Working Days
2889
1. Water: FDA & DENR Requirements Analysis
Without Pesticides 1 - 6 samples 10
(Accept only at most 8 samples per
7 - 12 samples 16
two weeks) 13 - 18 samples 22
With Pesticides 1 - 4 samples 12
(Receiving of samples to be limited to
5 - 8 samples 16
1st and 2nd workday of the 3rd week)
13 - 18 samples 24
2. Water Analysis
A. Anions 1 - 3 samples 6
3 - 6 samples 9
6 - 9 samples 12
10 - 12 samples 15
B. pH 3 3
C. Trace Metals (1 - 3 Parameters)
1 - 6 samples 7
7 - 12 samples 10
13 - 18 samples 13
Trace Metals (4 - 5 Parameters)
1 - 6 samples 8
7 - 12 samples 11
13 - 18 samples 14
TDS, TS, TSS 1 - 6 samples 7
7 - 12 samples 10
13 - 18 samples 13
D. Organics
OCPs, PAHs 1 - 4 samples 12
5 - 8 samples 16
(Accept only during 1st and 2nd work
day of the 1st week)
OCPs & PAHs 1 - 4 samples 16
5 - 8 samples 24
(Accept only during 1st and 2nd work
day of the 3rd week)
E. Total Organic Carbon 1 - 12 samples 6
2890 3. Soil / Sludge / Sediment
Samples*
A. Trace Metals (1 - 3 Parameters)
1 - 6 samples 10
7 - 12 samples 15
13 - 18 samples 20
Trace Metals (4 - 5 Parameters)
1 - 6 samples 12
7 - 12 samples 19
13 - 18 samples 26
*Maximum of 3 days for drying B. Organics (1 Parameter)
OCPs 1 - 4 samples 14
PAHs 1 - 4 samples 14
5 - 8 samples 20
Organics (2 Parameters)
OCPs & PAHs 1 - 4 samples 21
5 - 8 samples 26
4. Prepared Solutions
1-5 samples (2-10 solutions) 4
6-10 samples (12-20 solutions) 7
11-15 samples (22-30 solutions) 10
5. Biological Samples
A. Mercury 1 - 5 samples 15
B. Trace Metals except Hg (1 - 5 Parameters)
1 - 3 samples 14
4 - 6 samples 20
7 - 9 samples 32
10 - 12 samples 40
C. Organics (1 Parameter) 1 - 4 samples 16
5 - 8 samples 26
Organics (2 Parameters) 1 - 6 samples 18
5 - 8 samples 28