Hasil Uji Distribusi Ukuran Partikel Formula A Batch I

(1)

cxxvii

Lampiran 1

Hasil Uji Distribusi Ukuran Partikel Formula A Batch I

Replikasi Mesh d (μm)

ℓn _d

(μm)

(2)

cxxviii

Lampiran 2

Hasil Uji Distribusi Ukuran Partikel Formula A Batch _II

ℓn_d

(μm)

(3)

cxxix

Lampiran 3

Hasil Uji Distribusi Ukuran Partikel Formula A Batch _III

ℓn_d

(μm)

(4)

cxxx

Lampiran 4

Hasil Uji Distribusi Ukuran Partikel Formula B Batch _I

ℓn_d

(μm)

(5)

cxxxi

Lampiran 5

Hasil Uji Distribusi Ukuran Partikel Formula B Batch II

ℓn_d

(μm)

(6)

cxxxii

Lampiran 6

Hasil Uji Distribusi Ukuran Partikel Formula B Batch _III

ℓn_d

(μm)

(7)

cxxxiii

Lampiran 7

Hasil Uji Distribusi Ukuran Partikel Formula C Batch _I

ℓn_d

(μm)

(8)

cxxxiv

Lampiran 8

Hasil Uji Distribusi Ukuran Partikel Formula C Batch _II

ℓn_d

(μm)

(9)

cxxxv

Lampiran 9

Hasil Uji Distribusi Ukuran Partikel Formula C Batch III

ℓn_d

(μm)

(10)

cxxxvi

Lampiran 10

Hasil Uji Distribusi Ukuran Partikel Formula D Batch _I

ℓn_d

(μm)

(11)

cxxxvii

Lampiran 11

Hasil Uji Distribusi Ukuran Partikel Formula D Batch _II

ℓn_d

(μm)

(12)

cxxxviii

Lampiran 12

Hasil Uji Distribusi Ukuran Partikel Formula D Batch _III

ℓn_d

(μm)

(13)

cxxxix

Lampiran 13

PERHITUNGAN ANAVA KEKERASAN TABLET

PERLAKUAN ULANGAN

A B C D JUMLAH

1 5,36 7,23 7,84 3,38

2 5,38 7,2 7,85 3,36

3 5,34 7,24 7,85 3,36

n 3 3 3 3 12

RATA-RATA 5,360 7,223 7,847 3,367

-Ji 16,08 21,67 23,54 10,1 71,39

Ji2 258,57 469,59 554,13 102,01 1384,30

Perhitungan JK:

k = 4 n = 3 N = 12

JK.Ey = TOTAL - Py = 0,0020

(

∑

Y_i2

)

=461,4343

7213 , 36

= −

=

∑

N J n

J Py

JK.

2 2

i

7233 , 36

= −

=

∑

N J Y

TOTAL JK

2 2

(14)

cxl

TABEL ANAVA

SV db JK RJK F hit. F (0,05) F (0,01 )

Py 3 36,7213 12,2404 48961,722 4,07 7,59

Ey 8 0,0020 0,0003

TOTAL 11 36,7233 - - - -

db (TOTAL) = kn - 1 RJK = JK / db

db (Py) = (k - 1) F hitung = RJK (Py) / RJK (Ey) db (Ey) = db (TOTAL - Py)

Kriteria Pengujian:

2. Bila F hitung > F(0,05) maka berbeda signifikan PENGUJIAN HIPOTESA :

a. H : Pi = 0

Yang berarti tidak ada perbedaan kekerasan yang signifikan sebagai akibat perbedaan perlakuan.

b. KESIMPULAN:

(15)

cxli

UJI HSD / TUCKEY

PERLAKUAN MEAN A

5,360

B 7,223

C 7,847

D 3,367

A 5,360 0 1,863 * 2,487 * 1,993 *

B 7,223 0 0,623 * 3,857 *

C 7,847 0 4,480 *

D 3,367 0

RJK = 0,000 = 4,53

n = 3

db = 8 = 0,041

Keterangan

* : Perbedaannya signifikan, karena selisihnya > HSD(5%) TS : Perbedaannya tidak signifikan, karena selisihnya < HSD (5%)

5,360

7,223 7,847

3,367

0 5 10

A B C D

Formula

Keker

asan

db) p; (5%/2; q

n RJK q (5%)

(16)

cxlii

Lampiran 14

PERHITUNGAN ANAVA Kerapuhan Tablet

PERLAKUAN ULANGAN

A B C D JUMLAH

1 0,363 0,257 0,16 0,903

2 0,353 0,237 0,15 0,96

3 0,327 0,25 0,167 0,957

n 3 3 3 3 12

RATA-RATA 0,348 0,248 0,159 0,940

-Ji 1,043 0,744 0,477 2,82 5,084

Ji2 1,09 0,55 0,23 7,95 9,82

Perhitungan JK:

k = 4 n = 3 N = 12

(

Y2

)

3,276872

i =

∑

J = SJi = 5,084

JK TOTAL =

N J

-Y2 2

iJ

∑ _{= 1,1230}

N J n

J Py

JK.

2 2

i ₋

=

∑

= 1,1199

(17)

cxliii

TABEL ANAVA

Py 3 1,1199 0,3733 963,105 4,07 7,59

Ey 8 0,0031 0,0004

TOTAL 11 1,1230 - - -

-db (TOTAL) = kn - 1 RJK = JK / db

Kriteria Pengujian:

- Bila F hitung > F(0,05) maka berbeda signifikan

PENGUJIAN HIPOTESA : a. H : Pi = 0

Yang berarti tidak ada perbedaan kerapuhan yang signifikan sebagai akibat

perbedaan perlakuan.

b. KESIMPULAN:

(18)

cxliv

UJI HSD/TUCKEY

PERLAKUAN MEAN A

0,348

B 0,248

C 0,159

D 0,940

A 0,348 0 0,100 * 0,189 * 0,592 *

B 0,248 0 0,089 * 0,692 *

C 0,159 0 0,781 *

D 0,940 0

RJK = 0,000 = 4,53

n = 3 db = 8

Keterangan

0,348

0,248 _0,159

0,940

0 0,5 1

A B C D

Formula

Kera

puhan

db) p; (5%/2;

q

0,051 n

RJK q

(5%)

(19)

cxlv

Lampiran 15

PERHITUNGAN ANAVA Waktu Hancur Tablet

PERLAKUAN ULANGAN

A B C D JUMLAH

1 8,67 10,33 12 1

2 8,67 10 12,67 1

3 8,17 10,33 12 1

n 3 3 3 3 12

RATA-RATA 8,503 10,220 12,223 1,000

-Ji 25,51 30,66 36,67 3 95,84

Ji2 650,76 940,04 1344,69 9,00 2944,48

Perhitungan JK:

k = 4 n = 3 N = 12

(

∑

Y_i2

)

=982,0334

J = SJi = 95,84

JK TOTAL =

N J

-Y_iJ2 2

∑ _{= 216,5913}

N J n

J Py

JK.

2 2

i ₋

=

∑

= 216,0527

(20)

cxlvi

TABEL ANAVA

Py 3 216,0527 72,0176 1069,833 4,07 7,59

Ey 8 0,5385 0,0673

TOTAL 11 216,5913 - - -

Kriteria Pengujian:

3. Bila F hitung > F(0.05) maka berbeda signifikan

Yang berarti tidak ada perbedaan waktu hancur tablet yang signifikan sebagai akibat perbedaan perlakuan.

b. KESIMPULAN:

(21)

cxlvii

UJI HSD/TUCKEY

PERLAKUAN MEAN A 8,503

B 10,220

C 12,223

D 1,000

A 8,503 0 1,717 * 3,720 * 7,503 *

B 10,220 0 2,003 * 9,220 *

C 12,223 0 11,223 *

D 1,000 0

RJK = 0,067

n = 3 db = 8

Keterangan

* : Perbedaannya signifikan, karena selisihnya > HSD(5%)

TS : Perbedaannya tidak signifikan, karena selisihnya < HSD (5%)

8,503 10,220 12,223

1,000 0

5 10 15

A B C D

Formula

Waktu Hancur

4,53

=

db) p; (5%/2; q

0,679 n

RJK q

(5%)

(22)

cxlviii

Lampiran 16

PERHITUNGAN ANAVA Disolusi obat

PERLAKUAN ULANGAN

A B C D JUMLAH

1 80,64 76,42 74,37 83,43

2 80,96 74,47 72,76 82,78

3 80,96 77,72 74,37 83,11

n 3 3 3 3 12

RATA-RATA 80,853 76,203 73,833 83,107

-Ji 242,56 228,61 221,5 249,32 941,99

Ji2 58835,35 52262,53 49062,25 62160,46 222320,60

Perhitungan JK:

k = 4 n = 3 N = 12

(

Y2

)

74114,2253

i =

∑

J = SJi = 941,99

JK TOTAL =

N J

-Y2 2

iJ

∑ _{= 168,7953}

N J n

J Py

JK.

2 2

i ₋

=

∑

= 161,4360

(23)

cxlix

TABEL ANAVA

Py 3 161,4360 53,8120 58,497 4,07 7,59

Ey 8 7,3593 0,9199

TOTAL 11 168,7953 - - -

Kriteria Pengujian:

4. Bila F hitung > F(0,05) maka berbeda signifikan

Yang berarti tidak ada perbedaan disolusi (harga Q) yang signifikan sebagai akibat perbedaan perlakuan.

b. KESIMPULAN:

(24)

cl

UJI HSD/TUCKEY

PERLAKUAN MEAN A 80,853

B 76,203

C 73,833

D 83,107

A 80,853 0 4,650 * 7,020 * 2,253 ts

B 76,203 0 2,370 ts 6,903 *

C 73,833 0 9,273 *

D 83,107 0

RJK = 0,920 q_(5%/2;_p;_db)=4,53

n = 3 2,508

n RJK q

(5%)

HSD = =

db = 8

Keterangan

80,853

76,203

73,833

83,107

65 70 75 80 85

A B C D

Formula

Pelepasa

(25)

cli

Lampiran 17

'.'.Slo rlter;

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(26)

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Lampiran 18

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(27)

cliii

Lampiran 19

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(29)

clv

Lampiran 20

-

Sertifikat Analisa Aerosil

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(30)

clvi

Lampiran 21

Sertifikat Analisis

Tara Gum

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(31)

clvii

Lampiran 22

j

YUNG ZIP CHEMICAL IND. CO., LTD.

59, Yu Shih Road Youth Industrial District

Tachia, Taiwan, 437

R.O. C.

TE L: 886·4·26818780, 2681134 4 FAX: 886-4-26612911

ott:~ _ ·

CERTIFICATE OF ANALYSIS

Lot No.: SSGA02121 Mfg. Date: Nov. 29,2007

I':XI', I)lIle: Nov. 2M, 20 10

Aunlysl!l Fulluwlng lJSI' JO· N F 25

ITEMS

Dcsc:ripliol1

/J .. ,,,;n,,,,,;on

Microbl allimits

pH

Loss on drying

Iron

Heavy metals

Sodium chloride

Sod ium glycolate

Assay

SP~;CIFICATIONS

A white, tasteless, odorless, relati vely free-flowing powder,

usp lOJN I= 25

Salmonella E. Coli

Between 5.5 and 7.5

Not more than

.

,

Not more than

Sodium (Na) (2.8% to 4.2%)

10.0

0.002

7.0

2.0

,,:,

,".~i:';l ~ , ~l

%

RESULTS

"'f'rly ,

Confim}t'd I

;: \i ~, :

Confirmed

Negative""':'

Negative

6.1 "

Passed

4.0%

1.8 %

3.2 %

"' f*'

Conclusion : Passed

Date . ~

1212812007/40053

(32)

clviii

Lampiran 23

Nomor Sifat Perihal

Nama

N IM

Faku ltas

Divisi Sub divi si Kelas Bangsa Suku Marga Jen is

mestinya.

DlNAS KESEHAT AN PROPINSI JA WA TIMUR DALAI MATERIA MEDICA

Jalan LahorNo.87 Telp. (0 341 ) 5933 96 Batu (653 13) KOTA BATU

074 178 1 I I 1.14 1 IV 12007

Biasa

Determinasi Tauaman Kayu Rapet

Memenuhi pennohonan saudara Fitria Yun ita

: 2443003 I 48

: Faku ltas Farmas i Universitas Widya Mandala

Perihal detenninasi tanaman Ka~ Rapet

: Spennatophyta : Angiospennae : Dicoty ledonae : Apocynalcs : Apocynaceae : Parameria

: Parameria laevigata (J uss.) Moldenke

Demikian detenni nasi ini kaml buat untuk dipergunakan sebagaimana

Batu , 24 April 2007

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Lampiran 24

Tabel 1.

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.7'510 .7611 . 1642 . 7G13 .770: . 7734 .716 4 ,719 • . 1823 .1152

,' " ' . 7'JlO . 1939 . 11'7 .l9n •• Oll .1051 .1<17' •• ,06 .lIll

., '59 .• tOG .1212 .8238 . '21 ~ .IZlt .'215 .'l40 .n 'S ,n89

"413 .8431 .14Gl ... 5 .85eil .I!ill .15'H .• 511 .• ~ n .162'

.""3 .1145 .HaG .1101 ,I n ' .'74' .1110 ,1.1,0 .1810 . lIn ."4" ... .. HI .8901 ,IUS ,1946 .1"'2 .• "0 .• 19' .to15 . ~3: .tlo .... ",06 .9002 .!tOr.. ." 15 .'131 ."47

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.11 77

.1192 .120~ .1212 .1236 .1251 .'2G$ .'27 • . un .'306 .lll1

.lll2 .9345 .'35' ,9no .1302 .91'. ,'40G .'418 .I430 ., u l

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. MU .. . . " .'1571 ."12 •• Sll ." , . .HOI .11'& .H:z5 .• n l

1 . . .'$41 .MQ .1156 .~ .. . 9671 .1 . " .16" .Ktl ."00 .1706

, . • ..713 .'71, .112G

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2 , • .t121 .'12' .Ino .11)4 .'al( .'14." "1"4 ."$0 . '1~4 .915 7

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2 . ' .1153 .US5 .ItSl ... 57 .M5' .:tHO •• MI

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2 . 7 .'!lOS ."401 ."01 .9!JG8 .196' .Mll0 -"71 ."12 ."73 ."" ..

2 . I ."74 ." " .U7G .1117 ."11 .M7'

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" 7 ' .1910 .ttl' 2 . • . . . . 1 -"12 .M12 .II1l .HI" .. . 1,. •• IIS .n'5 .• IG .1101

(34)

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_ 2.' .0026 ,0025 .0024 .0023 ,0013 .0012 .0021 .0021 ,0020 .0019

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•• 2 . 1 .01 19 ,0114 .0 t'O ,01G6 .OHi2- ,Ot5(1 ,(11,$.1 ,0'50 .O,.t .ou.3

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1.8 . 0:1:,9 iilf02 .0344 .OJ3G .0329 , OJ L~ ,OJ;4 ,0307 .0)00 .029 ...

- 1 . 7 ,044G Il>\JG .e427 ,:)418 ,04'9 ,0401 .0392 .03001 . OJ7S . 0367

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1 . 6 OS"C .'J ~J7 .052:(. .O!.lG ("S05 .O-4!:S .04.)'; .00(75 .0"65 .0455

_ 1 • S _{. ~C.O} _.1),"S5.064';: .OGle' .OC; 1 a .Olioe; .au.:. . O~82 .O[;JO .0659

_ 1 .4 _.oeoc_{. 07'3}_.0171_.076/_{• .0749}_{.0135 ,0722 ,0708 ,0694 .OSII}

- I , ' .091.;' .0951 .011134 ,0'18 .0101 .0.85 .Ol!&;~ .0853 .0838 .0823

- , • 2. , 11 ';;' . 113 , .1 112 .1093 . 101$ . 1056 .lcul . l010 , t003 .0985

- 1 . 1 . 13S7 .1 335 . 1314 .1292 .1271 . t:z~ 1 .1l:l0 .12: 10 .lt90 . 1170

- 1. 0 . 15t37 .15G2 .1539 .1St 5 . 1492 .""69 " _4G .1 423 ,HOI . 1379

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.9 . 184 I 1814 . 1788 .17"2 .1736 . 1711 , 16;;;'5 .le.GO . 1",)5 .1611

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. 8 .2119 .2090 .20Gl .2033 , ;01)(';; ,1 " 7 . 1949 . 1922 .1 894 . 1867

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.242:.1 .2389 .:ZJ!>8 .2327 .lD7 .22'6 .2236 . 2206 .2177 . 21 .. 0

-- . G .Z·, f;J . 2709 .267,6 . 2643 .2G 1 I . 2576 . .lS';6 2514 .24133 .2451

-

. 5 .30'5 .3050 .JOI5 .2981 .294G .2912 .:Z8:17 .2843 .:Z010 ,2716

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.344a .:10\09 .3312 .3336 .3300 .3264 .3228 . 3192 .3156 . 312 I

-

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.3821 .37U3 ..3745 ..3707 .3"i9 . 3032 .3594 . 3557 . 3520 .3483

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.2 .4207 _4168 .4129 ,4090 .40$2 .4Q13 .39'''' .3s.36 .3897 .3859

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: 4602 .4582 ,4522 ."413 .4"'·U .4.01104 .4r64 ., ~.'7.5 .4;!16 ."247

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Lampiran 25

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Lampiran 26