41
7. LAMPIRAN
Lampiran 1. Hasil Analisa Data menggunakan SPSS versi 10.0
for windows.
Tests of Normality
,156
28
,077
,964
28
,424
madu randu
madu hutan
madu randu
madu hutan
madu randu
madu hutan
madu randu
madu hutan
madu randu
madu hutan
madu randu
madu hutan
VISKOS
Statistic
df
Sig.
Statistic
df
Sig.
Kolmogorov-Smirnov
aShapiro-Wilk
This is a lower bound of the true significance.
*.
Lilliefors Significance Correction
a.
Descriptives
28 3,7239 ,21721 ,04105 3,6397 3,8082 3,35 3,98 28 3,7468 ,24180 ,04570 3,6530 3,8405 3,42 4,12 56 3,7354 ,22803 ,03047 3,6743 3,7964 3,35 4,12 28 13,9357 1,54350 ,29169 13,3372 14,5342 11,00 17,00 28 12,0536 2,49198 ,47094 11,0873 13,0199 8,00 18,00 56 12,9946 2,26270 ,30237 12,3887 13,6006 8,00 18,00 28 4,1913 1,57520 ,29768 3,5805 4,8021 1,20 6,58 28 5,3329 2,42092 ,45751 4,3942 6,2717 2,00 10,56 56 4,7621 2,10403 ,28116 4,1987 5,3256 1,20 10,56 28 75,5036 ,68068 ,12864 75,2396 75,7675 73,00 76,80 28 74,7964 1,06022 ,20036 74,3853 75,2075 72,20 75,80 56 75,1500 ,95213 ,12723 74,8950 75,4050 72,20 76,80 28 22,3357 ,64648 ,12217 22,0850 22,5864 21,20 24,60 28 22,9286 ,90793 ,17158 22,5765 23,2806 21,80 24,80 56 22,6321 ,83625 ,11175 22,4082 22,8561 21,20 24,80 28 5,303461 3,562198368 ******** 3,92218496 6,68473761 1,808864 12,02121 28 2,739549 2,355512883 ******** 1,82617674 3,65292183 ,798129 7,822298 56 4,021505 3,259807235 ******** 3,14852321 4,89448736 ,798129 12,02121 madu randu
madu hutan Total madu randu madu hutan Total madu randu madu hutan Total madu randu madu hutan Total madu randu madu hutan Total madu randu madu hutan Total
N Mean Std. DeviationStd. Error Lower BoundUpper Bound 95% Confidence Interval for
Mean
ANOVA
,007 1 ,007 ,138 ,711
2,852 54 ,053
2,860 55
49,594 1 49,594 11,544 ,001
231,994 54 4,296
281,588 55
7,001 1 7,001 8,820 ,004
42,859 54 ,794
49,860 55
4,921 1 4,921 7,922 ,007
33,541 54 ,621
38,462 55
,000 1 ,000 10,092 ,002
,000 54 ,000
,001 55
18,246 1 18,246 4,374 ,041
225,237 54 4,171
243,483 55 Between Groups
Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total PH
VISKOS
K_GULA
K_AIR
HPLC
DPPH
Sum of
Data madu randu selama penyimpanan
Tests of Normalityb,c,d,e,f,g,h
,250 4 , ,945 4 ,683 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 PH
VISKOS
DPPH
K_GULA
K_AIR
Statistic df Sig. Statistic df Sig.
Kolmogorov-Smirnova Shapiro-Wilk
Lilliefors Significance Correction a.
HPLC is constant when HARI = hari ke-0. It has been omitted. b.
HPLC is constant when HARI = hari ke-5. It has been omitted. c.
HPLC is constant when HARI = hari ke-10. It has been omitted. d.
HPLC is constant when HARI = hari ke-15. It has been omitted. e.
HPLC is constant when HARI = hari ke-20. It has been omitted. f.
HPLC is constant when HARI = hari ke-25. It has been omitted. g.
Descriptives
4 3,5800 ,00816 ,00408 3,5670 3,5930 3,57 3,59 4 3,5050 ,03512 ,01756 3,4491 3,5609 3,47 3,54 4 3,3825 ,02754 ,01377 3,3387 3,4263 3,35 3,41 4 3,9450 ,03512 ,01756 3,8891 4,0009 3,91 3,98 4 3,8400 ,01414 ,00707 3,8175 3,8625 3,83 3,86 4 3,9200 ,00816 ,00408 3,9070 3,9330 3,91 3,93 4 3,9000 ,00816 ,00408 3,8870 3,9130 3,89 3,91 28 3,7246 ,21764 ,04113 3,6403 3,8090 3,35 3,98 4 14,8750 1,65202 ,82601 12,2463 17,5037 13,00 17,00 4 14,5500 ,64031 ,32016 13,5311 15,5689 14,00 15,20 4 13,7500 1,32288 ,66144 11,6450 15,8550 12,50 15,50 4 14,5000 1,29099 ,64550 12,4457 16,5543 13,00 16,00 4 11,8750 ,62915 ,31458 10,8739 12,8761 11,00 12,50 4 13,0000 ,81650 ,40825 11,7008 14,2992 12,00 14,00 4 15,0000 1,82574 ,91287 12,0948 17,9052 13,00 17,00 28 13,9357 1,54350 ,29169 13,3372 14,5342 11,00 17,00 4 3,6718 ,19495 ,09747 3,3616 3,9820 3,50 3,91 4 4,6183 ,22027 ,11014 4,2678 4,9688 4,43 4,93 4 6,0974 ,33874 ,16937 5,5584 6,6365 5,82 6,58 4 1,5264 ,38627 ,19314 ,9118 2,1411 1,20 1,93 4 4,2360 1,50301 ,75150 1,8444 6,6277 2,05 5,49 4 3,3250 ,24108 ,12054 2,9414 3,7086 3,02 3,59 4 5,8636 ,11020 ,05510 5,6882 6,0389 5,74 5,96 28 4,1912 1,57508 ,29766 3,5805 4,8020 1,20 6,58 4 75,7750 ,26300 ,13150 75,3565 76,1935 75,50 76,00 4 75,8000 ,16330 ,08165 75,5402 76,0598 75,60 76,00 4 74,6500 1,23693 ,61847 72,6818 76,6182 73,00 75,60 4 75,8500 ,82260 ,41130 74,5411 77,1589 74,80 76,80 4 75,6500 ,19149 ,09574 75,3453 75,9547 75,40 75,80 4 75,8000 ,16330 ,08165 75,5402 76,0598 75,60 76,00 4 75,2000 ,16330 ,08165 74,9402 75,4598 75,00 75,40 28 75,5321 ,66670 ,12599 75,2736 75,7907 73,00 76,80 4 22,2000 ,16330 ,08165 21,9402 22,4598 22,00 22,40 4 22,3000 ,38297 ,19149 21,6906 22,9094 22,00 22,80 4 23,1500 1,03763 ,51881 21,4989 24,8011 22,40 24,60 4 21,9500 ,19149 ,09574 21,6453 22,2547 21,80 22,20 4 22,4000 ,16330 ,08165 22,1402 22,6598 22,20 22,60 4 22,1000 ,50332 ,25166 21,2991 22,9009 21,60 22,80 4 22,7250 ,09574 ,04787 22,5727 22,8773 22,60 22,80 28 22,4036 ,56991 ,10770 22,1826 22,6246 21,60 24,60 4 4,543271 ,000000000 ******** 4,54327100 4,54327100 4,543271 4,543271 4 9,014741 ,000000000 ******** 9,01474100 9,01474100 9,014741 9,014741 4 12,02121 ,000000000 ********12,0212130012,02121300 12,02121 12,02121 4 3,601214 ,000000000 ******** 3,60121400 3,60121400 3,601214 3,601214 4 3,796702 ,000000000 ******** 3,79670200 3,79670200 3,796702 3,796702 4 1,808864 ,000000000 ******** 1,80886400 1,80886400 1,808864 1,808864 4 2,338000 ,000000000 ******** 2,33800000 2,33800000 2,338000 2,338000 28 5,303429 3,562225993 ******** 3,92214224 6,68471633 1,808864 12,02121 hari ke-0
hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total
N Mean Std. Deviation Std. Error Lower BoundUpper Bound 95% Confidence Interval for
Mean
ANOVA
1,268
6
,211
408,099
,000
,011
21
,001
1,279
27
31,469
6
5,245
3,352
,018
32,855
21
1,565
64,324
27
58,945
6
9,824
25,662
,000
8,039
21
,383
66,984
27
4,824
6
,804
2,352
,068
7,178
21
,342
12,001
27
4,042
6
,674
2,993
,028
4,728
21
,225
8,770
27
342,615
6
57,103
1,1E+33
,000
,000
21
,000
342,615
27
Between Groups
Within Groups
Total
Between Groups
Within Groups
Total
Between Groups
Within Groups
Total
Between Groups
Within Groups
Total
Between Groups
Within Groups
Total
Between Groups
Within Groups
Total
Squares
df
Mean Square
F
Sig.
Post Hoc Tests
Homogeneous Subsets
PH
Duncan
a4
3,3825
4
3,5050
4
3,5800
4
3,8350
4
3,9000
4
3,9200
3,9200
4
3,9450
1,000
1,000
1,000
1,000
,217
,127
HARI
hari ke-10
hari ke-5
hari ke-0
hari ke-20
hari ke-30
hari ke-25
hari ke-15
Sig.
N
1
2
3
4
5
6
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
VISKOS
Duncan
a4
11,8750
4
13,0000
13,0000
4
13,7500
13,7500
4
14,5000
4
14,5500
4
14,8750
4
15,0000
,057
,057
HARI
hari ke-20
hari ke-25
hari ke-10
hari ke-15
hari ke-5
hari ke-0
hari ke-30
Sig.
N
1
2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
DPPH
Duncan
a4
1,5264
4
3,3250
4
3,6718
3,6718
4
4,2360
4,2360
4
4,6183
4
5,8636
4
6,0974
1,000
,061
,052
,599
HARI
hari ke-15
hari ke-25
hari ke-0
hari ke-20
hari ke-5
hari ke-30
hari ke-10
Sig.
N
1
2
3
4
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
K_GULA
Duncan
a4
74,6500
4
75,2000
75,2000
4
75,6000
75,6000
4
75,6500
4
75,7750
4
75,8000
4
75,8500
,050
,200
HARI
hari ke-10
hari ke-30
hari ke-25
hari ke-20
hari ke-0
hari ke-5
hari ke-15
Sig.
N
1
2
Subset for alpha = .05
K_AIR
Duncan
a4
22,0000
4
22,0000
4
22,1000
4
22,2000
4
22,2000
4
22,7250
22,7250
4
23,1500
,123
,301
HARI
hari ke-0
hari ke-15
hari ke-25
hari ke-5
hari ke-20
hari ke-30
hari ke-10
Sig.
N
1
2
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
HPLC
Duncana
4 1,808864
4 2,338000
4 3,601214
4 3,796702
4 4,543271
4 9,014741
4 12,02121
1,000 1,000 1,000 1,000 1,000 1,000 1,000
HARI hari ke-25 hari ke-30 hari ke-15 hari ke-20 hari ke-0 hari ke-5 hari ke-10 Sig.
N 1 2 3 4 5 6 7
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed. Uses Harmonic Mean Sample Size = 4,000.
Data madu hutan selama penyimpanan
Tests of Normalityb,c,d,e,f,g,h
,250 4 , ,945 4 ,683 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 PH
VISKOS
DPPH
KDR_AIR
KDR_GULA
Statistic df Sig. Statistic df Sig.
Kolmogorov-Smirnova Shapiro-Wilk
Lilliefors Significance Correction a.
HPLC is constant when HARI = hari ke-0. It has been omitted. b.
HPLC is constant when HARI = hari ke-5. It has been omitted. c.
HPLC is constant when HARI = hari ke-10. It has been omitted. d.
HPLC is constant when HARI = hari ke-15. It has been omitted. e.
HPLC is constant when HARI = hari ke-20. It has been omitted. f.
HPLC is constant when HARI = hari ke-25. It has been omitted. g.
Descriptives
4 3,5300 ,00816 ,00408 3,5170 3,5430 3,52 3,54
4 3,4400 ,01826 ,00913 3,4109 3,4691 3,42 3,46
4 3,5025 ,07274 ,03637 3,3867 3,6183 3,43 3,57
4 3,9300 ,01826 ,00913 3,9009 3,9591 3,91 3,95
4 3,8275 ,05679 ,02839 3,7371 3,9179 3,77 3,89
4 4,0200 ,09967 ,04983 3,8614 4,1786 3,92 4,12
4 3,9775 ,12393 ,06196 3,7803 4,1747 3,80 4,08
28 3,7468 ,24180 ,04570 3,6530 3,8405 3,42 4,12
4 13,7500 1,04083 ,52042 12,0938 15,4062 12,50 15,00
4 10,5000 1,29099 ,64550 8,4457 12,5543 9,00 12,00
4 13,1250 ,62915 ,31458 12,1239 14,1261 12,50 14,00
4 12,0000 ,81650 ,40825 10,7008 13,2992 11,00 13,00
4 9,0000 ,81650 ,40825 7,7008 10,2992 8,00 10,00
4 10,0000 ,81650 ,40825 8,7008 11,2992 9,00 11,00
4 16,0000 1,82574 ,91287 13,0948 18,9052 14,00 18,00
28 12,0536 2,49198 ,47094 11,0873 13,0199 8,00 18,00
4 4,4000 ,87856 ,43928 3,0020 5,7980 3,63 5,21
4 4,8925 ,60450 ,30225 3,9306 5,8544 4,36 5,46
4 9,8550 ,50889 ,25444 9,0452 10,6648 9,41 10,56
4 4,4600 2,38214 1,19107 ,6695 8,2505 2,33 6,88
4 3,6525 ,12010 ,06005 3,4614 3,8436 3,51 3,79
4 3,1300 1,25754 ,62877 1,1290 5,1310 2,00 4,34
4 6,9425 ,82443 ,41222 5,6306 8,2544 6,23 7,72
28 5,3332 2,42067 ,45746 4,3946 6,2719 2,00 10,56
4 75,4250 ,38622 ,19311 74,8104 76,0396 75,00 75,80
4 75,2250 ,53151 ,26575 74,3793 76,0707 74,60 75,80
4 74,8500 ,90000 ,45000 73,4179 76,2821 73,80 75,60
4 72,8500 ,75498 ,37749 71,6487 74,0513 72,20 73,60
4 74,4000 1,05830 ,52915 72,7160 76,0840 73,00 75,40
4 75,5750 ,17078 ,08539 75,3032 75,8468 75,40 75,80
4 75,2500 ,19149 ,09574 74,9453 75,5547 75,00 75,40
28 74,7964 1,06022 ,20036 74,3853 75,2075 72,20 75,80
4 22,6750 ,09574 ,04787 22,5227 22,8273 22,60 22,80
4 22,6000 ,51640 ,25820 21,7783 23,4217 22,00 23,20
4 22,7000 ,88694 ,44347 21,2887 24,1113 22,00 24,00
4 24,5000 ,38297 ,19149 23,8906 25,1094 24,00 24,80
4 23,4000 1,05830 ,52915 21,7160 25,0840 22,40 24,80
4 22,2000 ,23094 ,11547 21,8325 22,5675 22,00 22,40
4 22,6000 ,23094 ,11547 22,2325 22,9675 22,40 22,80
28 22,9536 ,89255 ,16868 22,6075 23,2997 22,00 24,80
4 1,32000 ,000000 ,000000 1,32000 1,32000 1,320 1,320 4 3,88700 ,000000 ,000000 3,88700 3,88700 3,887 3,887 4 7,82200 ,000000 ,000000 7,82200 7,82200 7,822 7,822
4 ,79800 ,000000 ,000000 ,79800 ,79800 ,798 ,798
4 1,15400 ,000000 ,000000 1,15400 1,15400 1,154 1,154 4 2,86500 ,000000 ,000000 2,86500 2,86500 2,865 2,865 4 1,33000 ,000000 ,000000 1,33000 1,33000 1,330 1,330 28 2,73943 2,355426 ,445134 1,82609 3,65277 ,798 7,822 hari ke-0
hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total hari ke-0 hari ke-5 hari ke-10 hari ke-15 hari ke-20 hari ke-25 hari ke-30 Total
N Mean Std. Deviation Std. Error Lower Bound Upper Bound 95% Confidence Interval for
Mean
Post Hoc Tests
Homogeneous Subsets
PH
Duncan
a4
3,4400
4
3,5025
4
3,5300
4
3,8275
4
3,9300
3,9300
4
3,9775
4
4,0200
,100
,052
,100
HARI
hari ke-5
hari ke-10
hari ke-0
hari ke-20
hari ke-15
hari ke-30
hari ke-25
Sig.
N
1
2
3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
ANOVA
1,475 6 ,246 49,819 ,000
,104 21 ,005
1,579 27
142,232 6 23,705 19,570 ,000
25,438 21 1,211
167,670 27
130,172 6 21,695 16,249 ,000
28,039 21 1,335
158,211 27
21,357 6 3,560 8,312 ,000
8,993 21 ,428
30,350 27
14,202 6 2,367 6,802 ,000
7,308 21 ,348
21,510 27
149,797 6 24,966 6,1E+33 ,000
,000 21 ,000
149,797 27
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
Between Groups Within Groups Total
VISKOS
Duncan
a4
9,0000
4
10,0000
4
10,5000
10,5000
4
12,0000
12,0000
4
13,1250
13,1250
4
13,7500
4
16,0000
,081
,068
,163
,431
1,000
HARI
hari ke-20
hari ke-25
hari ke-5
hari ke-15
hari ke-10
hari ke-0
hari ke-30
Sig.
N
1
2
3
4
5
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
DPPH
Duncan
a4
3,1300
4
3,6525
4
4,4000
4
4,4600
4
4,8925
4
6,9425
4
9,8550
,065
1,000
1,000
HARI
hari ke-25
hari ke-20
hari ke-0
hari ke-15
hari ke-5
hari ke-30
hari ke-10
Sig.
N
1
2
3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
KDR_AIR
Duncan
a4
22,2500
4
22,5500
22,5500
4
22,6000
22,6000
4
22,6750
22,6750
4
22,7000
22,7000
4
23,4000
4
24,5000
,346
,081
1,000
HARI
hari ke-25
hari ke-30
hari ke-5
hari ke-0
hari ke-10
hari ke-20
hari ke-15
Sig.
N
1
2
3
Subset for alpha = .05
KDR_GULA
Duncan
a4
72,8500
4
74,4000
4
74,8500
74,8500
4
75,2250
75,2250
4
75,2500
75,2500
4
75,4250
75,4250
4
75,5750
1,000
,058
,173
HARI
hari ke-15
hari ke-20
hari ke-10
hari ke-5
hari ke-30
hari ke-0
hari ke-25
Sig.
N
1
2
3
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
a.
HPLC
Duncan
a4
,79800
4
1,15400
4
1,32000
4
1,33000
4
2,86500
4
3,88700
4
7,82200
1,000
1,000
1,000
1,000
1,000
1,000
1,000
HARI
hari ke-15
hari ke-20
hari ke-0
hari ke-30
hari ke-25
hari ke-5
hari ke-10
Sig.
N
1
2
3
4
5
6
7
Subset for alpha = .05
Means for groups in homogeneous subsets are displayed.
Uses Harmonic Mean Sample Size = 4,000.
Lampiran 2. Hasil Kromatogram konsentrasi quercetin pada madu
Lampiran 3. Kotak penyimpanan madu dengan metode ASLT.
Lampiran 4. Gambar madu randu (kiri) dan madu hutan (kanan)
Lampiran 5. Cara perhitungan konsentrasi quercetin
Rumus perhitungan :
Konsentrasi quercetin =
sampel
Madu randu
Luas area standar quercetin 60 ppm = 2825540
Luas area peak sampel = 236372
Konsentrasi quercetin =
18
Madu hutan
Luas area standar quercetin 60 ppm = 2825540
Luas area peak sampel = 118512
Konsentrasi quercetin =
Lampiran 6. Konversi waktu penyimpanan
Kondisi normal (suhu kamar) madu dapat dihitung menggunakan persamaan
Arhennius seperti yang dikemukakan oleh Halid (1991) dan Koswara (2002).
Perhitungan tersebut dapat dilihat di bawah ini :
)
keterangan :
10 TQ
δ