29 CHAPTER III
SPECIFICATION EQUIPMENTS
1.1Oleic Acid Storage Tank
Code : T-01
Duties : Store raw materials oleic acid as 1,575.31
kg/hour
Type : Vertical cylindrical tank with torispherical dished
head
Quantity : 1 Piece
Volume : 1,415.43 m3
Material : Carbon steel SA 212 Grade B
Storage conditions : Pressure : 1 atm
Temperature : 35oC
Dimensions :
The diameter of the tank : 12.17 m
Height tank : 12.17 m
Thick tank : Coarse 1 : 0.4375 in
Coarse 2 : 0.375 in
Coarse 3 : 0.3125 in
Coarse 4 : 0.25 in
Coarse 5 : 0.25 in
Coarse 6 : 0.1875 in
Thick Head : 0.5 in
Total high : 14.3864 m
Price : US $ 340,548.30
1.2Storage Tank Butanol
Code : T-02
30
Type : Vertical cylindrical tank with torispherical dished
head
Quantity : 1 piece
Volume : 446.14 m3
Material : Carbon steel SA 212 Grade B
Storage conditions : Pressure : 1 atm
Temperature : 35oC
Dimensions :
The diameter of the tank : 8.28 m
Height tank : 8.28 m
Thick tank : Coarse 1 : 0.25 in
Coarse 2 : 0.25 in
Coarse 3 : 0.1875 in
Coarse 4 : 0.1875 in
Coarse 5 : 0.1875 in
Thick-Head : 0.3125 in
Overall high :9.79 m
Price : US $ 215,985.33
1.3 Tank of Butyl Oleate
Code : T-05
Duties : store the product butyl oleate as 1,893.94 kg/hour
Type : Vertical cylinder with torispherical dished head
Quantity : 1 piece
Volume : 826.27 m3
Material : Carbon steel SA 212 Grade B
Storage conditions : Pressure : 1 atm
Temperature : 35oC
Dimensions :
The diameter of the tank : 10.17 m
31
Thick tank : Coarse 1 : 0.25 in
Coarse 2 : 0.25 in
Coarse 3 : 0.25 in
Coarse 4 : 0.25 in
Coarse 5 : 0.1875 in
Coarse 6 : 0.1875 in
Thick-Head : 0.4375 in
Overall high : 12.02 m
Price : US $ 270,838.75
1.4 Sulfuric Acid Tank
Code : T-03
Duties : To save as much sulfuric acid 47.46 kg/hour
Type : Vertical cylindrical tank with torispherical dished head
Quantity : 1 piece
Volume : 20.69 m3
Material : Carbon steel SA 212 Grade B
Storage conditions : Pressure : 1 atm
Temperature : 35oC
Dimensions :
The diameter of the tank : 2.98 m
High-tank : 2.98 m
Thick tank : Coarse 1 : 0.1875 in
Coarse 2 : 0.1875 in
Thick Head : 0.1875 in
Overall height : 3.51 m
Price : US $ 6,856.68
1.5 Tank Sodium Hydroxide
32
Duties : To save sodium Hydroxide as much as 96.22 kg/hour
Type : Upright cylindrical tank covered with the top
torispherical dished head
Quantity : 1 piece
Volume : 55.47 m3
Material : Carbon steel SA 212 Grade B
Storage conditions : Pressure : 1 atm
Temperature : 35oC
Dimensions :
The diameter of the tank : 4.13 m
High-Tank : 4.13 m
Thick Tank : Coarse 1 : 0.1875 in
Coarse 2 : 0.1875 in
Thick Head : 0.1875 in
Overall height : 4.88 m
Price : US $ 20,627.17
1.6 Reactor
Code : R
Duties : Reacting oleic acid and butanol to produce butyl oleate
with the help of Sulfuric Acid
Type : Continueous Stirred Tank Reactor (CSTR)
Quantity : 1 piece
Volume : 23.39 m3
Material : Carbon Steel SA 212 Grade B
Condition : Pressure : 1 atm
Temperature : 100oC
Dimensions :
The diameter of the tank : 2.82 m
High-tank : 3.46 m
33 Dimensions head :
Shape : Elliptical
Thick head : 0.1875 in
High head : 0.46 m
Mixer :
Type : Turbine with 6 blades with 4 baffles
Quantity : 1 piece
Diameter : 0.94 m
Speed : 67.68 rpm
Power : 7.5 hp
Cooling jacket :
Ingredients : Water
Diameter : 3.06 m
Inlet temperature : 30oC
Outlet temperature : 40oC
High-jacket : 2.59 m
Price : US $ 253,697.05
1.7 Netralizer
Code : N
Duties : Neutralize sulfuric acid catalyst with sodium hydroxide
Quantity : 1 piece
Temperature : 47.28oC
Pressure : 1 atm
Diameter : 1.70 m
Height : 1.70 m
Volume : 4.95 m3
Type : Continueous Stirred Tank Reactor (CSTR)
Type of head : Torispherical dished head
Construction Materials : Steel SA-283 Grade C
34
Type : Blade disk turbine with 6 standard
Speed : 106.19 rpm
Diameter : 0.57 m
Power of motor : 3 hp
Price : US $ 21,255.70
3.8. Decanter
Code : D
Function : Separating butyl oleate and H2O
Operation : Continuous
Quantity : 1 piece
Temperature : 47.28°C
Pressure : 1 atm
Diameter : 1.16 m
Lenght : 3.47 m
Volume : 3.03 m3
Type : Horizontal Cylinders
Construction Material : Stainless steel SA-167 (type of 304)
Price : US $ 5,713.90
3.9 . Mixer Tank 01
Code : MT-01
Function : Mixing oleic acid from the recycle of Flash drums and
fresh bait
Operation : Continuous
Quantity : 1 piece
Temperature : 35°C
Pressure : 1 atm
Diameter : 0.75 m
Height : 0.75 m
35
Type : Vertical cylindrical tank stirred
Type of head : Torispherical dished head
Material of construction : Steel SA-283 Grade C
Mixer :
Type : Turbine blade with 6 and 4 baffles
Speed : 270.05rpm
Diameter : 0.75 m
Power of motor : 0.75 hp
Price : US $ 11,542.07
3.10.Mixer Tank 02
Code : MT-02
Function : Butanol from the recycle of Distillation Tower and fresh
bait.
Operation : Continuous
Quantity : 1 piece
Temperature : 35°C
Pressure : 1 atm
Diameter : 0.93 m
Height : 0.93 m
Volume : 0.84 m3
Type : Vertical cylindrical tank stirred
Type of head : Torispherical dished head
Material of construction : Steel SA-283 Grade C
Mixer
Type : Turbine blade with 6 and 4 baffles
Speed : 176.67 rpm
Diameter : 0.32 m
Power of motor : 0.75 hp
36
Ingredients : Water
Diameter : 0.93 m
Inlet temperature : 25oC
Outlet temperature : 50oC
High-jacket : 0.82 m
Price : US $ 11,542.07
3. 11. Distillation Tower
Code : DT
Duties : Separating butanol from the mixture after exit
decanter
Type : Tower sieve tray
Number plate : 36 plate
Material : Low Alloy Steel SA 203 Grade C 2 1/2 Ni
Dimensions :
Diameter Top : 0.78 m
Diameter Bottom : 1.26
Height : 17.121 m
Shell Thickness : 0.1875 in
Dimensions Head
Type : Torispherical Dished Head
Thick Head : 0.1875 in
High Head : 0.28 m
Operating Conditions:
Top : Temperature : 118.33oC Pressure : 1 atm
Bottom : Temperature : 146.0937oC Pressure : 1 atm
37 3. 12. Flash Drum
Code : FD
Duties : Purify Butyl Oleate as the product of oleic acid
Type : Vessel Vertical
Quantity : 1 piece
Volume : 2.27 m3
Material : Steel SA-212 Grade B
Condition : Pressure : 1 atm
Temperature : 196.78oC
Dimensions :
Tank Diameter : 1.95 m
High-tank : 7.8 m
Shell thickness : 0.1875 in
Dimensi Head :
Type : Elliptical
Thick Head : 0.1875 m
Price : US $ 68,566.77
3.13. Heat Exchanger
Code : HE-01
Function : Increasing the flow temperature of 10 to MD of
temperature 47.28°C to 121.82°C
Type : Double pipe heat exchanger
Heating Load : 1,045,682.80 kJ/hour
Heat transfer area : 7.19 m2
Pipe Length : 3.6 m
specifications :
Anulus,
OD pipe : 4.55 in
38
Pressure drop : 0,0015 psi
Inner pipe,
OD pipe : 3.5 in
ID : 3,068 in
Pressure drop : 0,0119 psi
UC : 14.26 Btu/hour.ft2.oF
UD : 13.67 Btu/hour.ft2.oF
Rd : 0,003 Hour.ft2.oF /Btu
Construction Material : Inner (SS), Anulus (CS)
Total : 1
Price : US $ 31,997.83
3.14. Heat Exchanger 02
Code : HE-02
Function : Increasing the temperature from the bottom of the
distillation tower to flash drums of temperature 146.09oC
to 196.7oC .
Type : Double pipe heat exchanger
Heating Load : 319,927.91 kJ/hour
Heat transfer area : 3.97 m2
Lenght of pipe : 3.6 m
Specification :
Anulus,
OD pipe : 2.38 in
ID : 2.067 in
Pressure drop : 0,0014 psi
39
OD pipe : 1.66 in
ID : 1.38 in
Pressure drop : 0,1043 psi
UC : 85.18 Btu/hour.ft2.oF
UD : 67.84 Btu/hour.ft2.oF
Rd : 0.003 hour.ft2.oF /Btu
Construction Material : Inner (SS), Anulus (CS)
Total : 1
Price : US $ 23,998.37
3.15. Heat Exchanger 03
Code : HE-03
Function : Raising the temperature of mixing in the mixer 1 (flow 1
+ recycle at flow 14) to the reactor temperature 69.20oC to
100oC.
Type : Double pipe heat exchanger
Heating Load : 115,872.63 kJ/hour
Heat transfer area : 0.78 m2
Pipe Lenght : 36 m
Specification :
Anulus,
OD pipa : 4.5 in
ID : 4.026 in
Pressure drop : 0.0000489 psi
Inner pipe,
OD pipa : 3.5 in
40
Pressure drop : 0.0029 psi
UC : 18.95 Btu/hour.ft2.oF
UD : 17.93 Btu/hour.ft2.oF
Rd : 0.003 Hour.ft2.oF /Btu
Construction Material : Inner (SS), Anulus (CS)
Total : 1
Price : US $ 8,570.85
3.16 Cooler 01
Code : Co-01
Duties : Decreasing reactor outlet temperature before entering the
neutralizer of the temperature of 100oC to 40oC as much
as 5,237.06 kg/hour with water cooling medium.
Type : Double Pipe Heat Exchanger
Cooling Load : 1,013,420.48 kJ/hour
Heat transfer area : 6.66 m2
Pipe Lenght : 3.6 m
Specification :
Anulus,
OD pipe : 4.5 in
ID : 4.026 in
Pressure drop : 0.21 psi
Inner pipe,
OD pipe : 3.5 in
ID : 3.068 in
Pressure drop : 0.11 psi
UC : 74.76 Btu/hour.ft2.oF
UD : 61.06 Btu/hour.ft2.oF
Rd : 0.003 Hour.ft2.oF /Btu
41
Total : 1
Price : US $ 34,283.39
3.17. Cooler 02
Code : Co-02
Duties :.Decreasing flash drum outlet temperature as the product
of temperature 196,80oC to 35oC as much as 1,893.93
kg/hour with water cooling medium.
Type : Double Pipe Heat Exchanger
Cooling Load : 746,495.33 kJ/hour
Heat transfer area : 4.41 m2
Pipe Lenght : 3.6 m
Specification :
Anulus,
OD pipe : 2.38 in
ID : 2.067 in
Pressure drop : 0.22 psi
Inner pipe,
OD pipe : 1.66 in
ID : 1.38 in
Pressure drop : 6.69 psi
UC : 136.91 Btu/hour.ft2.oF
UD : 97.05 Btu/hour.ft2.oF
Rd : 0.003 Hour.ft2.oF /Btu
Construction Material : Inner (SS), Anulus (CS)
Total : 1
Price : US $ 23,998.37
1.18. Reboiler
42
Function :.Vaporize bottom liquid distillation tower as
2,165.39 kg/h
Type : Double Pipe
Heating Load : 2,174,811.45 kJ/hour
Heat transfer area : 3.31 m2
Pipe Lenght : 3.6 m
Specification :
Anulus,
OD pipe : 4.5 in
ID : 4.026 in
Pressure drop : 0.0057 psi
Inner pipe,
OD pipe : 3.5 in
ID : 3.068 in
Pressure drop : 0.0025 psi
UC : 62.01 Btu/hour.ft2.oF
UD : 52.28 Btu/hour.ft2.oF
Rd : 0.003 hour.ft2.oF/Btu
Construction Material : Inner (SS), Anulus (CS)
Total : 1
Price : US $ 19,427.25
3.19.Condensor 1
Code : Cd-01
Function :.For condensing distillation tower top products as much
as 2892.73 kg/hour.
Type : Shell and Tube
43
Heat transfer area : 27.96 m2
Fluid flow
Shell : gas Tube : Water
Specifications tube
Number of tube : 70 pieces
Lenght : 16 ft
OD, BWG, pitch : ¾ in, 16, 1 in (triangular)
Total flow : 8 pass
Shell Specification
ID : 15.25 in
Baffle spacing : 5 in
Total flow : 1 pass
Price : US $ 39,997.28
3.20.Condensor 2
Code : Cd-02
Function :.For condensing distillate or products of flash drum.
Type : Shell and Tube
Heating Load : 493,805.93 kJ/hour
Heat transfer area : 3.38 m2
Fluid flow
Shell : gas Tube : Water
Specifications tube
Number of tube : 70 pieces
Lenght : 16 ft
OD, BWG, pitch : ¾ in, 16, 1 in (triangular)
Total flow : 8 pass
Specifications shell
ID : 15,25 in
Baffle spacing : 5 in
44
Price : US $ 20,570.03
3.21.Accumulator 01
Code : Acc-01
Duties : Collect as much condensate from the distillation tower as
much as 2892.73 kg/hour
Type : Horizontal drum
Quantity : 1 piece
Operating conditions
Temperature : 118.3oC
Pressure : 1 atm
Dimensions of tank
Shell : Lenght : 1.7 m
Diameter : 0.87 m Thickness : ¼ in
Head :Type : Torispherical dished head
Thickness : 36 in
Material : Stainless steel SA-212 Grade B
Price : US $ 7,428.07
3.22.Accumulator 02
Code : Acc-02
Duties : Collect as much condensate from the flash drum 1893.94
kg/hour
Type : Horizontal drum
Quantity : 1 piece
Operating conditions
Temperature : 196.8oC
Pressure : 1 atm
Dimensions of tank
45 Diameter : 0.75 m
Thickness : ¼ in
Head :Type : Torispherical dished head
Thickness : 32 in
Material : Stainless steel SA 212 Grade B
Price : US $ 4,913.95
3.23.Pump-01
Code : P-01
Duties : Pumping from the tanker butanol to the tank of material
butanol
Capacity : 46.09 m3/hour
Total Head : 8.31 m
Type :Centrifugal Single Stage 3500 rpm
Motor Standar : 2 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 19,884.36
3.24.Pump-02
Code : P-02
Duties : Transporting raw materials oleic acid from the truck to the
tank Oleic acid reservoir.
Capacity : 46.09 m3/hour
Total Head : 3,00 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 2 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
46 3.25.Pump-03
Code : P-03
Duties : Flowing from the truck to the tank NaOH
Capacity : 46.09 m3/hour
Total Head : 4.16 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 2 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 19,884.36
3.26.Pump-04
Code : P-04
Duties : Flowing from the truck to the tank Oleic acid
Capacity : 46.09 m3/hour
Total Head : 12.19 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 5 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 19,884.36
3.27.Pump-05
Code : P-05
Duties : Flowing butanol material to the mixer 02
Capacity : 0.81 m3/hour
Total Head : 0.97 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
47
Price : US $ 6,628.12
3.28.Pump-06
Code : P-06
Duties :Transporting materials sulfuric acid into the reactor
Capacity : 0.04 m3/hour
Total Head : 2.98 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 6,628.12
3.29.Pump-07
Code : P-07
Duties : To pumping NaOH from NaOH tank to netralizer
Capacity : 0.10 m3/hour
Total Head : 1.70 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 6,628.12
3.40.Pump-08
Code : P-08
Duties : Pumping oleic acid from oleic acid tank to the mixer 01
Capacity : 2.57 m3/hour
Total Head : 0.79 m
Type : Centrifugal Single Stage 3500 rpm
48
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 7,656.62
3.41.Pump-09
Code : P-09
Duties : Pumping of raw materials to the output of the mixer 02 to
reactor
Capacity : 6.03 m3/hour
Total Head : 4.41 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 10,170.74
3.42.Pump-10
Code : P-10
Duties : Pumping the output of the mixer 01 to reactor
Capacity : 3.17 m3/hour
Total Head : 4.41 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 8,570.85
3.43.Pump-11
Code : P-11
Duties : Pumping the output of the reactor to netralizer
49
Total Head : 0.09 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 11,656.35
3.44.Pump-12
Code : P-12
Duties : Pumping output netralizer to decanter
Capacity : 9.14 m3/hour
Total Head : 2.35 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 11,656.35
3.45.Pump-13
Code : P-13
Duties : Pumping down the decanter to the output of the WTU
Capacity : 0.29 m3/hour
Total Head : 3.69 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 6,628.12
3.46.Pump-14
50
Duties : Pumping on the decanter to the output of the distillation
tower
Capacity : 8.97 m3/hour
Total Head : 4.66 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.5 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 11,656.35
3.47.Pump-15
Code : P-15
Duties : Pumping output below the results of distillation tower to
Flash drums
Capacity : 4.02 m3/hour
Total Head : 7.93 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.5 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 10,170.74
3.48.Pump-16
Code : P-16
Duties : Pumping output results on distillation tower is in
accumulator to the mixer 02
Capacity : 5.77 m3/hour
Total Head : 0.99 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
51
Amount :1
Price : US $ 10,170.74
3.49.Pump-17
Code : P-17
Duties : Pumping output over existing flash drum in accumulator to
the product storage tank
Capacity : 3.21 m3/hour
Total Head : 10.19 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 8,570.85
3.50.Pump-18
Code : P-18
Duties : Pumping down the output of the mixer to flash drum 01
Capacity : 0.50 m3/hour
Total Head : 0.77 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 0.25 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
Price : US $ 6,628.12
3.51.Pump-19
Code : P-18
Duties : Powering butyl oleate products in the storage tank products
to the distribution trucks.
52
Total Head : 10.19 m
Type : Centrifugal Single Stage 3500 rpm
Motor Standar : 5 Hp
Material : Carbon Steel SA 285 Grade C
Amount :1
