! "
#
$% &!
'( !
'
) # %
*+
,
-)+
.
"
•
•
!"
•
#
$
•
%
&
'
(
•
%
)"*)+
),-/+
0 % '
•
./
(0
•
1
/
2 )"
)""
+
θ
Diisi 2 fasa
•
1
" ")
•
3
/" "+,
•
0 4
5 )
) 67"6)
•
0 4
5 +
) 677!!
1+
% %
+
/
%
)
+
/
(81
#5
)
•
9
(81
•
8
:
•
•
3
•
2
;
•
8
5
5
+
<
=
>
> 5
+
5
#5
+
•
9
(81
•
8
:
•
•
3
•
2
;
(81
•
>
> < 5
=
>
> <8
=
2+
-"
•
#
5
?
5 @ >/A
#5
)
•
? 0
B?0
•
B " ""6
" "6
; " "6
•
8
5
5
+
5
5
)
3+
#
•
1
•
8
•
8
•
B
•
5
•
:
5
4 #
!
'
) # %
)
%
5
5
///
+
8 4
5
5
5
!
#
+
(#
>
> <
=
> 5
5
7
D
>
> <@
=
<
=
<
=
6
1
<8
///8
5 !
////
////
5
,
%
/
•
@
D"
D)
D+
D!
<8
///8
////
////
5
•
@
8
1
<8
///8
////
////
5
•
#5
o
<8
///
8
////
////
5
5
)
o
5
+
<8
///8
////
////
5
o
#5
5
)
5
+
<8
///8
////
////
5
•
8
o
8
)
<8 ; =
<8
///8
////
////
5
o
8
)
<B=
<8
///8
////
////
5
o
8
)
<A
=
<8
///8
////
////
5
o
+
5/
5
)
File data terhitung (.inp)
•
#5
<D=
5
<8
///8
////
////
5 #
D
2
;
•
A
:
5
7
<#
=
>
> <8
=
•
C
/
5
/
<8
///8
/
///
////
5
•
B
5
5
<
=
5 <4 >
= # 5
5
5
(
5 4 >
5
!
+---+ | Phase: 1 | +---+
PHASE SCALE FACTOR = 0.236462E-03-.515320E-070.991738E-05 OVERALL TEMP. FACTOR = 0.000000 0.000000 0.000000
CELL PARAMETERS = 4.762982 0.000000 0.000564 4.762983 0.000000 0.000564 13.005280 0.000010 0.002151 90.000008 0.000000 0.000000 90.000008 0.000000 0.000000 120.000015 0.000000 0.000001
RECIPROCAL CELL = 0.242 0.242 0.077 90.000 90.000 60.000 CELL VOLUME = 255.510223 0.060120
SCALE * VOLUME = 0.060419 0.002534 MOLECULAR WEIGHT = 611.757
DENSITY = 3.974 ABSOLUTE PHASE VALUES:
INC = NEUTRONS ON SAMPLE/CM^2 ( in cm^-2) MASS = MASS OF PHASE IN BEAM (in g)
ls/R = RATIO OF DETECTOR HEIGHT TO SAMPLE-DETECTOR Then:
INC*MASS*ls/R = 10542.7
0.00000 0.00000 0.00000
PHASE 1: 81.63 4.63 77.29 4.28 PHASE 2: 9.58 0.76 16.18 1.27 PHASE 3: 8.79 1.59 6.53 1.17
+---+ | Hist | Rp | Rwp | Rexp |Durbin Unwght| Durbin Wght | N-P | +---+ | 1 | 17.09 | 23.23 | 14.15 | 1.066 | 1.119 | 710 | +---+ | SUMYDIF | SUMYOBS | SUMYCALC | SUMWYOBSSQ | GOF | CONDITION | +---+ | 0.6058E+04| 0.3545E+05| 0.3355E+05| 0.3545E+05| 0.2694E+01| 0.2237E+14 | +---+
