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Pengaruh Temperatur Kalsinasi Pada Ekstraksi Silika Dari Abu Cangkang Kelapa Sawit

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File: C:\2020\DATA\ECH-300.SMP

Started :11/09/2015 7:13:08 Analysis Adsorptive :N2 Completed :14/09/2015 16:12:11 Analysis Bath Temp. :77.257 K Report Time :14/09/2015 7:38:21 Thermal Correction :No Sample Mass :0.3050 gWarm Free Space :25.7288 cm³ Measured

Cold Free Space :81.9857 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °CLow Pressure Dose :None Isotherm Linear Plot

SIO2 - Adsorption SIO2 - Desorption

Relative Pressure

0.009798 71.49968 0.996341 463.9799

0.029125 86.29842 0.986397 458.7902

0.057176 97.4559 0.977309 453.289

0.082912 104.7595 0.968518 449.2385

0.099599 108.795 0.958063 441.5128

0.119381 113.1938 0.932852 427.6534

0.139487 117.3405 0.904992 415.2422

0.159724 121.3005 0.877274 404.1742

0.179931 125.1794 0.850288 394.524

0.200131 128.9702 0.82551 386.5197

0.244191 137.1807 0.800266 379.1814

0.303063 148.5905 0.754841 365.4489

0.350105 158.4583 0.699447 338.2937

0.399961 169.9559 0.655842 296.4074

0.450287 182.6863 0.57313 239.1486

0.500379 196.6297 0.554505 230.2329

0.55012 212.2304 0.498024 206.891

0.600017 230.4077 0.454405 189.1147

0.649804 252.3323 0.393737 169.5922

0.699978 279.1239 0.352448 159.8215

0.745752 308.9076 0.305672 149.8134

0.805859 351.4478 0.254144 139.633

0.826617 363.9205 0.200678 129.5569

0.850981 375.5537 0.141334 118.2091

0.874563 384.5922 0.078811 104.2582

0.897243 393.4653

0.923802 405.6988

0.949563 420.6743

0.973346 438.5448

0.983102 447.9589

0.995622 456.6125

(3)

File: C:\2020\DATA\ECH-300.SMP

Started :11/09/2015 7:13:08 Analysis Adsorptive :N2 Completed :14/09/2015 16:12:11 Analysis Bath Temp. :77.257 K Report Time :14/09/2015 7:38:21 Thermal Correction :No Sample Mass :0.3050 gWarm Free Space :25.7288 cm³ Measured

Cold Free Space :81.9857 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °CLow Pressure Dose :None

BJH Adsorpsi Pore Size Distribution

Average Width 136.6822 0.014179 0.014179 0.414953 0.414953 86.37838 0.015774 0.029953 0.730451 1.145404 47.3277 0.031082 0.061035 2.626956 3.77236 30.65912 0.026807 0.087841 3.497362 7.269722

(4)

Started :14/09/2015 7:49:03 Analysis Adsorptive :N2 Completed :15/09/2015 12:19:52 Analysis Bath Temp. :77.267 K Report Time :15/09/2015 7:05:34 Thermal Correction :No Sample Mass :0.2350 g Warm Free Space:24.2568 cm³ Measured

Cold Free Space :78.1496 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

Isotherm Linear Plot

SIO2 - Adsorption SIO2 - Desorption

Relative Pressure

0.009688 61.59142 0.995144 447.0302

0.03121 77.31448 0.982884 441.6817

0.060277 88.42426 0.973902 435.8327

0.085027 95.37787 0.954929 424.7504

0.099647 98.9834 0.923809 410.4255

0.119407 103.4594 0.903036 402.4593

0.139392 107.7212 0.876876 393.4906

0.159527 111.8166 0.851088 385.3702

0.179591 115.7819 0.825631 378.1456

0.199908 119.7255 0.80085 371.8051

0.244772 128.4186 0.753437 359.6826

0.30143 139.8411 0.698762 335.9458

0.352563 150.9898 0.648864 288.2631

0.401041 162.4774 0.599359 249.0841

0.451504 175.2858 0.545728 219.7384

0.499529 188.9161 0.493925 198.1495

0.54986 205.15 0.444302 176.875

0.599509 223.9598 0.391842 160.671

0.649766 246.7072 0.35491 151.7933

0.699617 274.2414 0.304031 140.5161

0.749635 307.6294 0.250151 129.5115

0.798838 342.9726 0.202862 120.335

0.827138 359.2642 0.141296 108.2113

0.851673 369.5842 0.082457 94.8736

0.87492 377.3806

(5)

File:C:\2020\DATA\ECH-500.SMP

Started :14/09/2015 7:49:03 Analysis Adsorptive :N2 Completed :15/09/2015 12:19:52 Analysis Bath Temp. :77.267 K Report Time :15/09/2015 7:05:34 Thermal Correction :No Sample Mass :0.2350 g Warm Free Space:24.2568 cm³ Measured

Cold Free Space :78.1496 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

BJH Adsorpsi Pore Size Distribution

Average Width

241.5124 0.011962 0.011962 0.198112 0.198112

131.2857 0.014456 0.026418 0.440457 0.638569

86.07397 0.012325 0.038743 0.572744 1.211312

47.19616 0.027084 0.065826 2.29542 3.506732

30.48069 0.022348 0.088175 2.93279 6.439523

22.51849 0.017503 0.105677 3.109012 9.548535

17.88811 0.015253 0.12093 3.410657 12.95919

14.89033 0.014927 0.135856 4.009717 16.96891

12.71739 0.020616 0.156473 6.484402 23.45331

10.92915 0.033965 0.190437 12.43087 35.88418

8.971182 0.076954 0.267391 34.31147 70.19565

7.351761 0.074439 0.34183 40.50128 110.6969

6.19349 0.061841 0.40367 39.93912 150.636

5.320021 0.050954 0.454625 38.31148 188.9475

4.638948 0.041734 0.496359 35.98591 224.9334

4.086112 0.035402 0.531761 34.65559 259.589

3.636084 0.029131 0.560891 32.04615 291.6352

3.248448 0.026643 0.587534 32.80706 324.4422

2.912799 0.023441 0.610976 32.19082 356.6331

2.61055 0.021619 0.632595 33.12584 389.7589

2.31399 0.020322 0.652917 35.12972 424.8886

2.066639 0.013877 0.666794 26.85922 451.7478

1.920981 0.005824 0.672619 12.1276 463.8754

1.826106 0.005632 0.678251 12.33686 476.2123

(6)

Started :15/09/2015 7:45:17 Analysis Adsorptive :N2 Completed :15/09/2015 7:45:01 Analysis Bath Temp. :77.246 K Report Time :15/09/2015 15:59:21 Thermal Correction :No Sample Mass :0.1900 g Warm Free Space:25.9767 cm³ Measured

Cold Free Space :82.5904 cm³ Equilibration Interval:10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

Isotherm Linear Plot

SIO2 - Adsorption SIO2 - Desorption

Relative Pressure

0.01003 33.17376 0.99711 377.0766

0.030701 41.29888 0.990749 366.6811

0.059143 47.04626 0.974991 359.8925

0.077235 49.74762 0.954732 347.1838

0.099746 52.61896 0.924648 330.2734

0.119825 54.90581 0.903314 319.9489

0.139848 57.02176 0.876606 307.7925

0.159961 59.00787 0.850644 296.3747

0.180016 60.90864 0.826561 284.9547

0.200151 62.75785 0.800596 271.555

0.247716 67.02337 0.754026 239.8788

0.302264 71.90316 0.70588 193.2598

0.35324 76.73678 0.645881 147.1869

0.400277 81.61825 0.59838 125.7952

0.450164 87.49305 0.542133 108.663

0.500676 94.44343 0.506361 100.7168

0.550436 102.8611 0.454937 90.32428

0.600681 113.5164 0.398244 81.33079

0.650205 127.2798 0.349897 76.18548

0.700004 146.1564 0.303014 71.68985

0.749299 172.947 0.25045 66.91978

0.799322 212.4979 0.2004 62.40045

0.824218 235.3901 0.140529 56.67238

0.853217 261.3243 0.080557 49.75306

0.878192 279.8934

0.900638 293.9669

0.924453 308.6755

0.950535 326.2579

0.975529 346.8893

0.983727 355.5568

0.995868 365.0856

(7)

File:C:\2020\DATA\ECH-700.SMP

Started :15/09/2015 7:45:17 Analysis Adsorptive :N2 Completed :15/09/2015 7:45:01 Analysis Bath Temp. :77.246 K Report Time :15/09/2015 15:59:21 Thermal Correction :No Sample Mass :0.1900 g Warm Free Space:25.9767 cm³ Measured

Cold Free Space :82.5904 cm³ Equilibration Interval:10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

BJH Adsorpsi Pore Size Distribution

Average Width

(8)

Started :15/09/2015 16:11:00 Analysis Adsorptive :N2 Completed :16/09/2015 18:10:54 Analysis Bath Temp. :77.240 K Report Time :16/09/2015 7:24:10 Thermal Correction :No Sample Mass :0.2800 g Warm Free Space:25.7123 cm³ Measured

Cold Free Space :81.7593 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

Isotherm Linear Plot

SIO2 - Adsorption SIO2 – Desorption

Relative Pressure

0.011152 4.100603 0.992431 129.2093

0.032029 5.071684 0.97934 125.7058

0.066855 5.87981 0.968998 120.2861

0.079617 6.103362 0.949829 100.3231

0.099913 6.417791 0.924251 66.78152

0.12014 6.698195 0.896586 45.82331

0.14016 6.948123 0.873598 34.02169

0.159785 7.185942 0.851785 26.41426

0.179766 7.411308 0.825828 21.25293

0.199764 7.622845 0.803495 18.64492

0.249174 8.146273 0.75321 15.51915

0.300558 8.657114 0.703263 13.86915

0.350732 9.149714 0.652541 12.72316

0.399955 9.650325 0.600763 11.83561

0.449983 10.16782 0.550276 11.11288

0.499896 10.71215 0.500752 10.4865

0.549758 11.2977 0.450517 9.880975

0.599717 11.96249 0.400596 9.355215

0.649733 12.71752 0.350619 8.850689

0.699569 13.60701 0.300693 8.3513

0.749363 14.71981 0.250717 7.857176

0.799028 16.24785 0.200754 7.335342

0.8199 17.13452 0.121173 6.405588

0.849209 18.81537 0.069055 5.615526

0.873644 20.97894

0.89775 24.63322

0.920585 31.57259 0.951204 54.36078

0.966926 76.4219

(9)

:\2020\DATA\ECH-900.SMP

Started :15/09/2015 16:11:00 Analysis Adsorptive :N2 Completed :16/09/2015 18:10:54 Analysis Bath Temp. :77.240 K Report Time :16/09/2015 7:24:10 Thermal Correction :No Sample Mass :0.2800 g Warm Free Space:25.7123 cm³ Measured

Cold Free Space :81.7593 cm³ Equilibration Interval :10 s Ambient Temperature :22.00 °C Low Pressure Dose :None Automatic Degas :Yes

BJH Adsorpsi Pore Size Distribution

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