No KAS (g)
Anhidrid Maleat
Benzoil
Peroksida Styrena Kec. rotor
(rpm)
T
(oC)
T (min)
(phr) (g) (phr) (g) (mol
ratio/MA) (g)
1 30 - - - -
2 30 - - - 80 150 8
3 30 2 0.6 - - - - 80 150 8
4 30 4 1.2 - - - - 80 150 8
5 30 8 2.4 - - - - 80 150 8
6 30 16 4.8 - - - - 80 150 8
7 30 2 0.6 1 0.3 - - 80 150 8
8 30 4 1.2 1 0.3 - - 80 150 8
9 30 8 2.4 1 0.3 - - 80 150 8
10 30 16 4.8 1 0.3 - - 80 150 8
11 30 16 4.8 - - 0.5 2.55 80 150 8
12 30 16 4.8 - - 1.0 5.11 80 150 8
13 30 16 4.8 - - 2.0 10.22 80 150 8
14 30 16 4.8 1 0.3 0.5 2.55 80 150 8
15 30 16 4.8 1 0.3 1.0 5.11 80 150 8
16 30 16 4.8 1 0.3 2.0 10.22 80 150 8
17 30 16 4.8 1 0.3 - - 60 150 8
18 30 16 4.8 1 0.3 - - 70 150 8
19 30 16 4.8 1 0.3 - - 80 150 8
20 30 16 4.8 1 0.3 - - 80 150 6
21 30 16 4.8 1 0.3 - - 80 150 8
7
49
.49
8
26
.20
13
74.
59
14
59.
83
16
04.
74
29
34.
49
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8
A
bs
or
ba
nc
e
1000 2000
3000 4000
Wavenumbers (cm-1)
L
am
pi
ra
n 2. S
pe
kt
rum
F
T
-IR
K
ar
et A
la
m S
ikl
is
s
ega
r
(f
re
sh
7
49
.49
8
29
.04
13
74.
59
14
59.
83
15
99.
05
17
26.
91
29
34.
49
0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1
A
bs
or
ba
nc
e
1000 2000
3000 4000
ra
n 3. S
pe
kt
rum
F
T
-I
R
K
ar
et
A
la
m
S
ikl
is
ya
ng s
uda
h di
pr
os
es
di
d
al
am
P
enc
am
pur
I
nt
er
na
7
47
.62
8
29
.94
13
72.
09
14
57.
25
16
02.
02
17
78.
00
17
80.
84
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 4. S
pe
kt
rum
F
T
-I
R
KAS
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id M
al
ea
t 2 phr
, t
anpa
B
P
7
50
.46
8
29
.94
13
69.
26
14
57.
25
15
99.
18
17
26.
91
17
80.
84
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 5. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id
M
al
eat
4 phr
, t
anp
a B
P
7
39
.10
8
29
.94
13
72.
09
14
54.
41
16
02.
02
29
27.
61
0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 0.55
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 6. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id
M
al
eat
8 phr
, t
anp
a B
P
7
47
.62
8
69
.67
13
74.
93
14
54.
41
15
99.
18
17
18.
40
17
83.
68
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6 2.8 3.0 3.2
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 7. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id
M
al
ea
t 16 phr
, t
anp
a B
P
7
50
.56
8
27
.13
13
74.
47
14
56.
71
15
98.
51
17
20.
46
17
82.
85
29
34.
25
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 8. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id
M
al
ea
t 2 phr
, de
ng
an B
P
7
47
.62
8
29
.94
13
72.
09
14
57.
25
16
02.
02
17
21.
23
17
83.
68
29
38.
96
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 9. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n p
ena
m
ba
ha
n A
nhi
dr
id
M
al
ea
t 4 phr
,de
ng
an ke
h
adi
ra
n B
P
7
47
.62
8
32
.77
13
72.
09
14
57.
25
16
10.
53
17
21.
23
17
80.
84
29
36.
13
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6 2.8
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 10. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id
M
al
ea
t 8 phr
,de
ng
an ke
ha
di
ra
n B
P
7
47
.62
8
29
.94
13
74.
93
14
54.
41
15
99.
18
17
18.
40
17
86.
52
29
36.
13
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.7
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 11. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id
M
al
ea
t 16 phr
,de
ng
an k
eha
di
ra
n B
P
7
02
.20
7
50
.46
8
38
.45
13
72.
09
14
54.
41
15
99.
18
17
21.
23
17
83.
68
18
54.
64
29
33.
29
0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 0.55
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 12. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id
M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
2:
1)
t
anpa
B
P
6
98
.34
7
58
.01
8
29
.04
13
74.
59
14
54.
14
15
99.
05
17
21.
23
17
80.
90
18
57.
62
29
34.
49
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3
A
bs
or
ba
nc
e
1000 2000
3000 4000
ra
n 13. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
1:
1)
t
anpa
B
P
6
99
.36
7
61
.81
8
38
.45
13
72.
09
14
57.
25
16
10.
53
17
21.
23
17
83.
68
18
54.
64
29
33.
29
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 14. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
1:
2)
t
anpa
B
P
7
05
.04
7
50
.46
8
41
.29
13
72.
09
14
57.
25
16
10.
53
17
18.
40
17
83.
68
18
57.
48
29
33.
29
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 15. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
2:
1)
de
nga
n B
P
7
05
.04
7
53
.29
9
49
.15
13
74.
93
14
60.
09
16
02.
02
17
83.
68
18
54.
64
29
33.
29
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 16. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
1:
1)
de
nga
n B
P
7
05
.04
7
53
.29
9
29
.28
13
69.
26
14
57.
25
16
02.
02
17
80.
84
18
54.
64
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 17. S
pe
kt
rum
F
T
-IR
K
A
S
de
nga
n pe
n
am
ba
ha
n A
nhi
dr
id M
al
ea
t
da
n kom
onom
er
S
tir
ena
,
ra
si
o m
ol
A
M
/S
t =
1:
2)
de
nga
n B
P
7
50
.46
8
29
.94
13
69.
26
14
57.
25
15
99.
18
17
26.
91
17
80.
84
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 18. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n k
ec
ep
at
an
rot
or
60 r
7
39
.10
8
29
.94
13
72.
09
14
54.
41
16
02.
02
29
27.
61
0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 0.55
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 19. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n k
ec
ep
at
an
rot
or
70 r
7
47
.62
8
29
.94
13
74.
93
14
54.
41
15
99.
18
17
18.
40
17
86.
52
29
36.
13
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.7
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 20. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n k
ec
ep
at
an
rot
or
80 r
7
49
.49
8
29
.04
13
74.
59
14
59.
83
15
99.
05
17
26.
91
29
34.
49
0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1
A
bs
or
ba
nc
e
1000 2000
3000 4000
ra
n 21. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n
w
akt
u 6 m
eni
7
47
.62
8
29
.94
13
74.
93
14
54.
41
15
99.
18
17
18.
40
17
86.
52
29
36.
13
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.7
A
bs
or
ba
nc
e
1000 2000
3000
Wavenumbers (cm-1)
ra
n 22. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n
w
akt
u 8 m
eni
7
47
.62
8
69
.67
13
74.
93
14
54.
41
15
99.
18
17
18.
40
17
83.
68
29
33.
29
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0 2.2 2.4 2.6 2.8 3.0 3.2
A
bs
or
ba
nc
e
1000 2000
3000
ra
n 23. S
pe
kt
rum
F
T
-I
R
KAS
pr
oduk pe
n
ca
ngkoka
n A
M
d
enga
n
w
akt
u 12 m
eni
1 - - - - -
2 7,328 - 0,807 - 0,110126
3 13,191 - 2,76 - 0,209234
4 20,701 - 5,919 - 0,285928
5 3,33 - 1,564 - 0,46967
6 12,422 - 14,577 - 1,173483
7 8,451 1,843 - 0,218081
8 12,49 - 6,509 - 0,521137
9 16,385 - 16,354 - 0,998108
10 8,508 - 10,478 - 1,231547
11 3,162 0,804 4,049 0,254269 1,280519
12 6,082 1,738 10,512 0,285761 1,728379
13 4,588 2,141 12,169 0,466652 2,652354
14 6,633 2,373 18,331 0,357757 2,763606
15 7,132 3,843 20,949 0,538839 2,937325
16 8,515 7,933 29,835 0,93165 3,503817
17 13,213 - 2,801 - 0,211988
18 3,4 - 0,76 - 0,223529
19 8,508 - 10,478 - 1,231547
20 4,889 - 1,869 - 0,382287
21 12,389 - 14,541 - 1,173702
ra
n 25
. T
he
rmogr
am T
G
A
K
ar
et A
la
m S
ikl
is
s
ega
r
(f
re
sh
Universitas
ra
n 27
. T
he
rmogr
am D
S
C
K
ar
et A
la
m S
ikl
is
s
ega
r
(f
re
sh
Universitas
ra
n 29
. T
he
rmogr
am T
G
A
K
ar
et A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 30. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 31
. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 32
. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 33. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 34
. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 35
. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 36
. T
he
rmogr
am D
S
C
K
ar
et A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
ra
n 37. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
2 phr
de
ra
n 38. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
4 phr
de
nga
n B
P
ra
n 39
. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
8 phr
de
ra
n 40. T
he
rm
ogr
am
T
G
A
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
16 phr
de
nga
n B
P
ra
n 41. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
2 phr
de
nga
ra
n 42. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
4
phr
de
nga
n B
P
ra
n 43. T
he
rm
ogr
am
D
S
C
K
ar
et
A
la
m
S
ikl
is
pe
na
m
ba
ha
n
A
M
8 phr
de
ra
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